IP Library Granted Patent US 9,505,933
Granted Patent B2
US 9,505,933 · App. 13/998,217 · Granted Nov 29, 2016

Composite pigments

Inventors: Zhenzhong Zhang (Sandersville, GA); Yaping Li (Evans, GA)
Assignee: Thiele Kaolin Company
C09C1/0081C09C1/0084C09C1/021C09C1/3653C09C1/402C01P2004/61C01P2004/62C01P2004/80C01P2006/12C01P2006/60
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Quick Facts
Patent No.
US 9,505,933
App. No.
13/998,217
Granted
Nov 29, 2016
Kind
B2
Abstract

Composite pigments are provided which comprise a mineral pigment (such as kaolin clay, titanium dioxide, talc, mica or a mixture of two or more of these mineral pigments) and calcium carbonate precipitated in-situ on the surfaces of the particles of the mineral pigment.

Claims (18)

1. A process for the manufacture of a high brightness composite pigment which comprises a mineral pigment and calcium carbonate, wherein the process comprises the steps of:

(a) obtaining a slurry of particles of the mineral pigment;

(b) adding slaked lime to the slurry to form a mixture;

(c) passing carbon dioxide gas through the mixture to precipitate calcium carbonate on surfaces of the mineral pigment particles;

(d) stopping passage of the carbon dioxide gas when the mixture has a pH of about 7.0; and

(e) repeating steps (b)-(d) a plurality of times to produce the composite pigment,

wherein the composite pigment has a reduced amount of particles of less than 0.2 microns compared to the starting mineral pigment and an equivalent or increased amount of particles of 1-2 microns compared to the starting mineral pigment.

2. A process as defined by claim 1 wherein the mineral pigment is kaolin clay, titanium dioxide, talc, mica or a mixture of two or more of these mineral pigments.

3. A process as defined by claim 1 wherein the mineral pigment is kaolin clay.

4. A process as defined by claim 3 wherein the kaolin clay is hydrous kaolin clay.

5. A process as defined by claim 3 wherein the kaolin clay is delaminated kaolin clay.

6. A process as defined by claim 3 wherein the kaolin clay is calcined kaolin clay.

7. A process as defined by claim 3 wherein the kaolin clay is a blend of hydrous kaolin clay and calcined kaolin clay.

8. A process as defined by claim 1 wherein the amount of calcium carbonate in the composite pigment is from about 5.0 to about 90.0 weight percent based on the weight of the dry composite pigment.

9. A process as defined by claim 1 wherein the amount of calcium carbonate in the composite pigment is from about 10.0 to about 60.0 weight percent based on the weight of the dry composite pigment.

10. A process as defined by claim 1 wherein the amount of calcium carbonate in the composite pigment is from about 20.0 to about 40.0 weight percent based on the weight of the dry composite pigment.

11. A process as defined by claim 1 wherein the calcium carbonate is uniformly precipitated on the surfaces of the mineral pigment.

12. A process as defined by claim 1 wherein the composite pigment additionally comprises titanium dioxide, talc, mica or a mixture of these materials.

Assignments (3)
RELEASE OF SECURITY INTEREST Recorded Jul 2, 2026
From: BANK OF AMERICA, N.A.
To: THIELE KAOLIN COMPANY
Reel/Frame 075161/0158 →
NOTICE OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Apr 6, 2017
From: THIELE KAOLIN COMPANY
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 042171/0362 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 23, 2013
From: ZHANG, ZHENZHONG; LI, YAPING
To: THIELE KAOLIN COMPANY
Reel/Frame 032064/0723 →
Continuity (1)
Related Publication 20150096469A1 · Apr 9, 2015