IP Library Granted Patent US 9,541,558
Granted Patent B2
US 9,541,558 · App. 14/017,744 · Granted Jan 10, 2017

Cysteine hydrazide nicotinamide for glycomics and glycoproteomics uses

Inventors: William M. Clemons (Pasadena, CA); Kyoung-Soon Jang (Pasadena, CA); Roger Nani (Pasadena, CA); Sergiy Levin (North Wales, PA); Sarah Reisman (San Marino, CA)
Assignee: California Institute of Technology
G01N33/6848G01N33/6842Y10T436/143333
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Quick Facts
Patent No.
US 9,541,558
App. No.
14/017,744
Granted
Jan 10, 2017
Kind
B2
Abstract

A cysteine hydrazide nicotinamide (Cyhn) reagent designed for the enrichment of bacterial glycoproteins is provided. Methods for purification of free oligosaccharides and their analysis are also provided.

Claims (8)

1. A compound having a structure of Formula (II):

or a salt thereof, wherein:

n is an integer from 1-10;

R is a nitrogen-containing ring capable of forming a salt;

wherein the nitrogen-containing ring is a ring selected from the group consisting of pyridyl, pyridazinyl, pyrazinyl, quinoxalyl, indolizinyl, quinazolinyl, purinyl, quinolinyl, pyrimidinyl, pyrrolyl, pyrazolyl, tetrazolyl, imidazolyl, triazolyl, indolyl, piperidinyl, piperazinyl, and pyrrolidinyl; and

R 1 is H or saccharide.

2. The compound according to claim 1 , wherein R is pyridyl.

3. The compound according to claim 1 , wherein n=1.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 18, 2014
From: CLEMONS, WILLIAM M.; JANG, KYOUNG-SOON; NANI, ROGER; LEVIN, SERGIY; REISMAN, SARAH
To: CALIFORNIA INSTITUTE OF TECHNOLOGY
Reel/Frame 032708/0416 →
CONFIRMATORY LICENSE Recorded Sep 17, 2013
From: CALIFORNIA INSTITUTE OF TECHNOLOGY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 031288/0231 →
Continuity (3)
Provisional Application 61697096 · Sep 5, 2012
Provisional Application 61712703 · Oct 11, 2012
Related Publication 20140072981A1 · Mar 13, 2014