IP Library Granted Patent US 9,035,066
Granted Patent B2
US 9,035,066 · App. 14/062,969 · Granted May 19, 2015

Method of using 4,5,6,7-tetrahydroimidazo[4,5-C]pyridine compounds

Inventors: Edward Savory (Cambridgeshire, GB); Michael Higginbottom (Cambridgeshire, GB); Kathryn Oliver (Hertfordshire, GB); Viet-Anh Anne Horgan (Surrey, GB)
Assignee: Proximagen Limited
C07D471/04A61K31/437
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Quick Facts
Patent No.
US 9,035,066
App. No.
14/062,969
Granted
May 19, 2015
Kind
B2
Abstract

The present invention relates to compounds of formula (I), and their pharmaceutically acceptable salts, solvates, hydrates, geometrical isomers, tautomers, optical isomers or N-oxides, which are inhibitors of SSAO activity. The invention further relates to pharmaceutical compositions comprising these compounds and to the use of these compounds for the treatment of medical conditions wherein inhibition of SSAO activity is beneficial, such as inflammatory diseases and immune disorders.

Claims (86)

1. A method for the treatment of arthritis, which comprises administering to a mammal in need of such treatment an effective amount of a compound of formula (I),

or a pharmaceutically acceptable salt, geometrical isomer, tautomer, optical isomer, or N-oxide thereof, wherein:

R 1 is selected from:

(a) hydrogen,

(b) C 1-6 -alkyl, and

(c) —NR 4A R 4B ;

R 2 is selected from:

(a) hydrogen,

(b) C 1-6 -alkyl,

(c) halo-C 1-6 -alkyl,

(d) hydroxy-C 1-6 -alkyl,

(e) C 1-6 -alkoxy-C 1-6 -alkyl,

(f) halo-C 1-6 -alkoxy-C 1-6 -alkyl,

(g) N(R 4A R 4B )—C 1-6 -alkyl,

(h) —C(O)NR 4A R 4B , and

(i) —C(O)O—C 1-6 -alkyl; and

R 3 is selected from:

(a) C 1-6 -alkyl,

(b) halo-C 1-6 -alkyl,

(c) hydroxy-C 1-6 -alkyl,

(d) C 1-6 -alkoxy-C 1-6 -alkyl,

(e) halo-C 1-6 -alkoxy-C 1-6 -alkyl,

(f) N(R 4A R 4B )—C 1-6 -alkyl,

(g) C 6-10 -aryl-C 1-4 -alkyl,

(h) heteroaryl-C 1-4 -alkyl,

(i) C 6-10 -aryloxy-C 1-4 -alkyl,

(j) heteroaryloxy-C 1-4 -alkyl,

(k) C 3-8 -cycloalkyl,

(l) C 3-8 -cycloalkyl-C 1-4 -alkyl,

(m) heterocyclyl, and

(n) heterocyclyl-C 1-4 -alkyl,

wherein any aryl or heteroaryl residue is optionally substituted with one more substituents independently selected from halogen, hydroxy, cyano, nitro, CF 3 , C 1-4 -alkyl, C 1-4 -alkoxy and —NR 4A R4B, and wherein any cycloalkyl or heterocyclyl residue is optionally substituted with one or more substituents independently selected from halogen, hydroxy, C 1-4 -alkyl, C 1-4 -alkoxy and —NR 4A R 4B ;

R 4A and R 4B are each independently selected from:

(a) hydrogen,

(b) C 1-6 -alkyl, and

(c) C 1-6 -acyl.

2. The method according to claim 1 , wherein R 1 is H.

3. The method according to claim 1 , wherein R 2 is selected from hydrogen, —C(O)O—C 1-3 -alkyl, and —C(O)NR 4A′ R 4B′ and wherein R 4A′ and R 4B′ are independently selected from hydrogen and C 1-2 -alkyl.

4. The method according to claim 1 , wherein R 2 is selected from:

(a) hydrogen,

(b) —C(O)O—C 1-6 -alkyl, and

(c) —C(O)NR 4A R 4B .

5. The method according to claim 1 , wherein R 2 is hydrogen, —C(O)OMe, —C(O)NH 2 , or —C(O)NHMe.

6. The method according to claim 1 , wherein R 3 is selected from halo-C 1-2 -alkyl, halo-C 1-2 -alkoxy-C 1-2 -alkyl, phenyl-C 1-2 -alkyl, phenoxy-C 1-2 -alkyl, C 5-6 -heteroaryl-C 1-2 -alkyl, C 5-6 -heteroaryloxy-C 1-2 -alkyl, heterocyclyl, and heterocyclyl-C 1-2 -alkyl and wherein any phenyl, heteroaryl, or heterocyclyl residue is optionally substituted with one or two substituents independently selected from halogen and C 1-2 -alkyl.

7. The method according to claim 1 , wherein R 3 is selected from halo-C 1-4 -alkyl, halo-C 1-4 -alkoxy-C 1-4 -alkyl, di(C 1-4 -alkyl)-amino-C 1-4 -alkyl, C 6-10 -aryl-C 1-4 -alkyl, C 6-10 -aryloxy-C 1-4 -alkyl, heteroaryl-C 1-4 -alkyl, heteroaryloxy-C 1-4 -alkyl, heterocyclyl, and heterocyclyl-C 1-4 -alkyl, wherein any aryl, heteroaryl, or heterocyclyl residue is optionally substituted with one or two substituents independently selected from halogen and C 1-4 -alkyl.

8. The method according to claim 1 , wherein R 3 is selected from 2,2,2-trichloroethyl, 2-chloro-2,2-difluoroethyl, 2,2,2-trifluoroethoxyethyl, dimethylaminoethyl, benzyl, pyridinylmethyl, pyrazinylmethyl, thiazolylmethyl, isoxazolylmethyl, phenoxyethyl, pyridinyloxyethyl, tetrahydrofuranyl, tetrahydrofuranylmethyl, pyrrolidinyl, pyrrolidinylmethyl, and oxetanylmethyl, wherein any phenyl, heteroaryl or heterocyclyl residue is optionally monosubstituted with halogen or methyl.

9. The method according to claim 1 , wherein the compound is selected from the group consisting of:

(a) 2,2,2-Trichloroethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(b) 2-Chloro-2,2-difluoroethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]-pyridine-5-carboxylate;

(c) Benzyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(d) 3-Chlorobenzyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(e) 4-Chlorobenzyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(f) Pyridin-2-ylmethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(g) Pyridin-3-ylmethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(h) Pyridin-4-ylmethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(i) (5-Chloropyridin-2-yl)methyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]-pyridine-5-carboxylate;

(j) Pyrazin-2-ylmethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(k) Benzyl (4S,6S)-6-(aminocarbonyl)-4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo-[4,5-c]pyridine-5-carboxylate;

(l) Benzyl (4S,6S)-4-isopropyl-6-[(methylamino)carbonyl]-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(m) 5-Benzyl 6-methyl (4S,6S)-4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]-pyridine -5,6-dicarboxylate;

(n) 2-Phenoxyethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(o) 2-(4-Chlorophenoxy)ethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(p) (3S)-Tetrahydrofuran-3-yl (4S)-4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]-pyridine-5-carboxylate;

(q) Tetrahydrofuran-3-ylmethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(r) (3-Methyloxetan-3-yl)methyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]-pyridine-5-carboxylate;

(s) 2-(Dimethylamino)ethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(t) (2R)-Tetrahydrofuran-2-ylmethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(u) 1,3-Thiazol-2-ylmethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(v) (5-Methylisoxazol-3-yl)methyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]-pyridine-5-carboxylate;

(x) [(2S)-1-Methylpyrrolidin-2-yl]methyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo-[4,5-c]pyridine-5-carboxylate;

(y) (3R)-1-methylpyrrolidin-3-yl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]-pyridine-5-carboxylate;

(z) Oxetan-2-ylmethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate;

(aa) 2-(Pyridin-3-yloxy)ethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]pyridine-5-carboxylate; and

(bb) 2-(2,2,2-Trifluoroethoxy)ethyl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]-pyridine-5-carboxylate, and

pharmaceutically acceptable salts thereof.

10. The method according to claim 1 wherein the compound is in a pharmaceutical formulation containing a pharmaceutically acceptable diluent or carrier.

11. The method according to claim 1 wherein the arthritis is rheumatoid arthritis.

12. The method according to claim 1 wherein the arthritis is juvenile rheumatoid arthritis.

13. The method according to claim 1 wherein the arthritis is osteoarthritis.

14. The method according to claim 1 wherein the arthritis is psoriatic arthritis.

15. The method according to claim 1 wherein the mammal is a human.

16. The method according to claim 9 wherein the compound is in a pharmaceutical formulation containing a pharmaceutically acceptable diluent or carrier.

17. The method according to claim 9 wherein the arthritis is rheumatoid arthritis.

18. The method according to claim 9 wherein the arthritis is juvenile rheumatoid arthritis.

19. The method according to claim 9 wherein the arthritis is osteoarthritis.

20. The method according to claim 9 wherein the arthritis is psoriatic arthritis.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 15, 2022
From: BENEVOLENTAI CAMBRIDGE LIMITED
To: PROXIMAGEN, LLC
Reel/Frame 059265/0350 →
CHANGE OF ADDRESS Recorded Mar 22, 2019
From: BENEVOLENTAI CAMBRIDGE LIMITED
To: BENEVOLENTAI CAMBRIDGE LIMITED
Reel/Frame 048676/0176 →
CHANGE OF NAME Recorded Dec 17, 2018
From: PROXIMAGEN LIMITED
To: BENEVOLENTAI CAMBRIDGE LIMITED
Reel/Frame 047799/0165 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 25, 2013
From: SAVORY, EDWARD; HIGGINBOTTOM, MICHAEL; OLIVER, KATHRYN; HORGAN, VIET-ANH ANNE
To: PROXIMAGEN LTD
Reel/Frame 031475/0817 →
Continuity (4)
Continuation 13567146 · Aug 6, 2012
Division 13062318
Provisional Application 61106734 · Oct 20, 2008
Related Publication 20140121219A1 · May 1, 2014