IP Library Granted Patent US 9,181,368
Granted Patent B2
US 9,181,368 · App. 14/074,426 · Granted Nov 10, 2015

High activity, low molecular weight olefin polymerization process

Inventors: Harold W. Boone (Houston, TX); Kevin A. Frazier (Midland, MI); Daniel D. VanderLende (Sugar Land, TX); Paul C. Vosejpka (Midland, MI)
Assignee: Dow Global Technologies LLC
C08F210/14C07F7/00C08F10/00C08F4/65908C08F4/65912C08F110/06C08F210/06C08F210/16C08F210/18Y10S526/905
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Quick Facts
Patent No.
US 9,181,368
App. No.
14/074,426
Granted
Nov 10, 2015
Kind
B2
Abstract

Group 4 metal complexes comprising a polyvalent, heteroaryl donor ligand and their use as components of olefin polymerization catalysts, especially suited for preparing propylene copolymer products having high isotacticity and low molecular weight, are disclosed.

Claims (7)

1. An interpolymer of propylene, ethylene, and optionally, a diene, and wherein the interpolymer comprises 65 percent or more polymerized propylene, and wherein the interpolymer is made by a process comprising the following:

copolymerizing propylene, ethylene, and optionally a diene, at a temperature from 100 to 130° C., a pressure from 100 KPa to 10 MPa, and a propylene/hydrogen flow ratio (g propylene/hr:g H 2 /hr) from 5000 to 50,000 in the presence of a metal complex corresponding to the formula:

wherein, X is an anionic ligand group; and

covalent bonds are represented by lines and coordination interactions are represented by arrows; and

wherein said interpolymer has a Mw from 50,000 to 150,000, a molecular weight distribution Mw/Mn from 2.0 to 10, a density from 0.860 to 0.885, an ethylene content from 5 to 15 weight percent, an isotacticity (percent mm) of at least 90, ΔH fusion from 25 to 55 J/g; a Tc between 50° C. and 58.7° C., and a B-value from 1.03 to 1.09.

2. The interpolymer of claim 1 , wherein the interpolymer has a melt flow rate (MFR) from 10 to 500 g/10 min.

3. The interpolymer of claim 1 , wherein the interpolymer has a molecular weight distribution (Mw/Mn) from 2.0 to less than 3.0.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 10, 2014
From: BOONE, HAROLD W.; FRAZIER, KEVIN A.; VANDERLENDE, DANIEL D.; VOSEJPKA, PAUL C.
To: DOW GLOBAL TECHNOLOGIES INC.
Reel/Frame 033282/0192 →
CHANGE OF NAME Recorded Jul 10, 2014
From: DOW GLOBAL TECHNOLOGIES INC.
To: DOW GLOBAL TECHNOLOGIES LLC
Reel/Frame 033289/0332 →
Continuity (4)
Continuation 13349860 · Jan 13, 2012
Division 12088108
Provisional Application 60721295 · Sep 28, 2005
Related Publication 20140066585A1 · Mar 6, 2014