High-temperature strain cell for tomographic imaging
This disclosure provides systems, methods, and apparatus related to the high temperature mechanical testing of materials. In one aspect, a method includes providing an apparatus. The apparatus may include a chamber. The chamber may comprise a top portion and a bottom portion, with the top portion and the bottom portion each joined to a window material. A first cooled fixture and a second cooled fixture may be mounted to the chamber and configured to hold the sample in the chamber. A plurality of heating lamps may be mounted to the chamber and positioned to heat the sample. The sample may be placed in the first and the second cooled fixtures. The sample may be heated to a specific temperature using the heating lamps. Radiation may be directed though the window material, the radiation thereafter interacting with the sample and exiting the chamber through the window material.
1. An apparatus comprising:
a chamber, the chamber comprising a top portion and a bottom portion, the top portion and the bottom portion each joined to a window material, the window material separating the top portion and the bottom portion and configured to transmit radiation used to characterize a sample, the top portion of the chamber defining a first port configured for a first cooled fixture, the bottom portion of the chamber defining a second port configured for a second cooled fixture, the first cooled fixture and the second cooled fixture configured to hold the sample in the chamber, the top portion of the chamber and the bottom portion of the chamber further defining a plurality of heating lamp ports, the plurality of heating lamp ports configured for a plurality heating lamps, the plurality of heating lamps positioned to heat the sample.
2. The apparatus of claim 1 , wherein the chamber is configured to maintain a vacuum.
3. The apparatus of claim 1 , wherein the window material is selected from a group consisting of aluminum, beryllium, pyrolytic carbon, and glassy carbon.
4. The apparatus of claim 1 , wherein the window material is about 200 microns to 400 microns thick.
5. The apparatus of claim 1 , wherein the window material has an inner diameter of about 8 centimeters to 26 centimeters.
6. The apparatus of claim 1 , wherein the window material has a substantially cylindrical shape.
7. The apparatus of claim 1 , wherein the window material separates the top portion and the bottom portion of the chamber by up to about 2 centimeters.
8. The apparatus of claim 1 , wherein the chamber defines a volume having a substantially spherical shape.
9. The apparatus of claim 1 , wherein the plurality of heating lamp ports comprises six heating lamps ports arranged in a hexapole arrangement.
10. The apparatus of claim 1 , further comprising:
the plurality of heating lamps.
11. The apparatus of claim 10 , wherein the plurality of heating lamps includes halogen lamps.
12. The apparatus of claim 10 , further comprising:
a plurality of gaskets, a gasket disposed between the top portion or the bottom portion of the chamber and each of the plurality of heating lamps, each of the plurality of gaskets configured to create a seal between the chamber and each of the plurality of heating lamps.
13. The apparatus of claim 1 , further comprising:
the first cooled fixture; and
the second cooled fixture.
14. The apparatus of claim 13 , further comprising:
a motor positioned to apply a force to the first cooled fixture that is transmitted to the sample.
15. The apparatus of claim 14 , further comprising:
a force measuring device positioned between the motor and the chamber, wherein the force measuring device is configured to measure the force applied to the sample by the motor.
16. The apparatus of claim 13 , further comprising:
a displacement measuring device positioned between the motor and the chamber, wherein the displacement measuring device is configured to measure a displacement of the first cooled fixture.
17. A method comprising:
providing an apparatus, the apparatus including:
a chamber, the chamber comprising a top portion and a bottom portion, the top portion and the bottom portion each joined to a window material, the window material separating the top portion and the bottom portion and configured to transmit radiation used to characterize a sample;
a first cooled fixture and a second cooled fixture mounted to the chamber and configured to hold the sample in the chamber; and
a plurality of heating lamps mounted to the chamber and positioned to heat the sample;
placing the sample in the first and the second cooled fixtures;
heating the sample to a specific temperature using the heating lamps; and
directing the radiation though the window material, the radiation thereafter interacting with the sample and exiting the chamber through the window material.
18. The method of claim 17 , further comprising:
applying a force to the first cooled fixture that is transmitted to the sample.
19. The apparatus of claim 18 , wherein the force is a compressive force.
20. The apparatus of claim 18 , wherein the force is a tensile force.