IP Library Granted Patent US 9,771,499
Granted Patent B2
US 9,771,499 · App. 14/092,110 · Granted Sep 26, 2017

Adhesive having structural integrity and insulative properties

Inventors: Tianjian Huang (Hillsborough, NJ); Robert Sandilla (Wexford, PA); Daniel Waski (Elmhurst, IL); Kristina Thompson (Clinton, NJ); John Meccia (Ringoes, NJ)
Assignee: HENKEL IP & HOLDING GMBH
C09J11/08B32B1/02B32B3/28B32B7/12D21H19/10D21H19/24D21H19/54D21H21/52D21H27/10D21H27/36C08K9/10C08L3/02C08L2205/025C09J2205/11D21H21/54Y10T428/1376Y10T428/24711Y10T428/249972
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Quick Facts
Patent No.
US 9,771,499
App. No.
14/092,110
Granted
Sep 26, 2017
Kind
B2
Abstract

An adhesive composition that provides improved structural integrity and insulative properties when applied to a substrate is provided. The adhesive composition includes an emulsion-based polymer, a plurality of microspheres; and optionally, water and plasticizer.

Claims (22)

1. An adhesive composition to decrease the basis weight of a substrate comprising:

(a) about 50 to about 70 weight percent of an emulsion polymer selected from the group consisting of vinyl acetate-ethylene copolymer, polyvinyl acetate-polyvinyl alcohol copolymer, dextrin-stabilized polyvinyl acetate copolymer, polyvinyl acetate copolymers, and mixtures thereof;

(b) about 0.1 to about 10 weight percent of a plurality of expandable microspheres that are expandable in the presence of heat and/or radiation; and

(c) water; and

wherein the total adhesive composition weight percent is calculated without component (c) water;

wherein the emulsion polymer has a solids level of from about 40 weight percent to about 60 weight percent, based on the emulsion polymer;

wherein the adhesive composition is a water-based resin emulsion.

2. The adhesive composition of claim 1 , wherein said expandable microspheres comprise polymeric microspheres have an initial expansion temperature (Texp) and a maximum expansion temperature (Tmax).

3. The adhesive composition of claim 1 , wherein said plurality of expandable microspheres are present in an amount of from about 0.5 weight percent to about 5 weight percent.

4. The adhesive composition of claim 1 , further comprising a plasticizer and/or a preservative.

5. The adhesive composition of claim 2 , wherein said expandable microspheres has a Texp of about 80° C. to about 90° C. and a (Tmax) about 120° C. to about 140° C.

6. The adhesive composition of claim 1 , wherein the adhesive further comprises a crosslinker, filler, pigment, dye, stabilizer, rheology modifier, polyvinyl alcohol, humectant and mixtures thereof.

7. The adhesive composition of claim 1 , wherein the adhesive further comprises an accelerator that is a multivalent water-soluble salt.

8. An expanded adhesive composition prepared by

(1) forming an unexpanded adhesive, which is a water-based resin emulsion comprising:

(a) about 50 to about 70 weight percent of an emulsion polymer, having a solids level of from about 40 to about 60 weight percent based on the emulsion polymer, selected from the group consisting of vinyl acetate-ethylene copolymer, polyvinyl acetate-polyvinyl alcohol copolymer, dextrin-stabilized polyvinyl acetate copolymer, polyvinyl acetate copolymers, and mixtures thereof

(b) about 0.1 to about 10 weight percent of a plurality of expandable microspheres; and

(c) water; and

wherein the total adhesive weight percent is calculated without component (c) water;

(2) expanding the expandable microspheres with heat and/or radiation; and

(3) drying the water from the water-based resin emulsion;

wherein the dry volume of the expanded adhesive composition is at least 400% greater than the dry volume of the unexpanded adhesive.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2022
From: HENKEL IP & HOLDING GMBH
To: HENKEL AG & CO. KGAA
Reel/Frame 059357/0267 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 21, 2016
From: HENKEL CORPORATION
To: HENKEL IP & HOLDING GMBH
Reel/Frame 038048/0769 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 15, 2016
From: HUANG, TIANJIAN; SANDILLA, ROBERT; WASKI, DANIEL; THOMPSON, KRISTINA; MECCIA, JOHN
To: HENKEL CORPORATION
Reel/Frame 037734/0552 →
Continuity (7)
Continuation In Part 13775348 · Feb 25, 2013
Continuation PCTUS2011050965 · Sep 9, 2011
Continuation 14092110
Continuation In Part 13826451 · Mar 14, 2013
Provisional Application 61381642 · Sep 10, 2010
Provisional Application 61706447 · Sep 27, 2012
Related Publication 20140087109A1 · Mar 27, 2014