IP Library Granted Patent US 9,339,785
Granted Patent B2
US 9,339,785 · App. 14/132,262 · Granted May 17, 2016

Methods and systems for acoustically-assisted hydroprocessing at low pressure

Inventors: James J. Strohm (West Richland, WA); Benjamin Q. Roberts (Richland, WA); Kayte M. Denslow (Richland, WA)
Assignee: Battelle Memorial Institute
B01J19/10C10G15/08C10G31/00C10G45/02C10G45/22C10G47/32
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Quick Facts
Patent No.
US 9,339,785
App. No.
14/132,262
Granted
May 17, 2016
Kind
B2
Abstract

Hydroprocessing can be performed at low pressure using acoustic energy. For example, hydroprocessing a feedstock having one or more hydrocarbon compounds carried in, or mixed with, a transport gas involves flowing the feedstock through a reaction zone in a reactor that has a bulk pressure less than 68 atm and applying acoustic energy through the reaction zone. The hydrocarbon compounds are chemically reacted with a hydrogen source in the presence of a catalyst, wherein the reacting occurs in the reaction zone.

Claims (19)

1. A method of hydroprocessing a feedstock comprising one or more hydrocarbon compounds carried in, or mixed with, a transport gas, the method comprising:

flowing the feedstock through a reaction zone in a reactor, the reaction zone having a bulk pressure less than 3 atm;

applying acoustic energy through the reaction zone; and

chemically reacting the hydrocarbon compounds with a hydrogen source in the presence of a catalyst, said reacting occurring in the reaction zone.

2. The method of claim 1 , wherein the hydrocarbon compounds comprise solid particulates.

3. The method of claim 1 , wherein the hydrocarbon compounds comprise liquid fluid.

4. The method of claim 1 , wherein the hydrocarbon compounds comprise vapor.

5. The method of claim 1 , wherein said applying acoustic energy further comprises inducing non-linear acoustic effects.

6. The method of claim 1 , wherein the reaction zone has a bulk pressure approximately equivalent to atmospheric pressure.

7. The method of claim 1 , wherein the hydrocarbon compounds comprise derivatives or distillate cuts of oils, tars, or asphaltenes.

8. The method of claim 7 , wherein the oil, tars, or asphaltenes comprise petroleum, coal-derived oils, biomass-derived oils, oil sands, oils shale.

9. The method of claim 1 , wherein the hydrogen source is selected from the group consisting of hydrogen, methane, natural gas, light hydrocarbons (≦C4), and combinations thereof.

10. The method of claim 1 , having a liquid hourly space velocity (LHSV) greater than 0.1 hr−1.

11. The method of claim 1 , wherein the reaction zone has a bulk temperature from 120° C. to 450° C.

12. The method of claim 1 , wherein said reacting comprises a reaction selected from the group consisting of hydrogenation, hydrocracking, hydrodesulfurization, hydrodenitrogenation, hydrodeoxygenation, hydrodemetalization, and combinations thereof.

13. A method of hydroprocessing a feedstock comprising one or more hydrocarbon compounds carried in or mixed with a transport gas, the method comprising:

flowing the feedstock through a reaction zone in a reactor, the reaction zone having a bulk pressure less than 3 atm;

applying acoustic energy through the reaction zone, the acoustic energy having frequencies and sound pressure levels sufficient to induce non-linear effects; and

chemically reacting the hydrocarbon compounds with a hydrogen source in the presence of a catalyst, said reacting occurring in the reaction zone.

Assignments (2)
CONFIRMATORY LICENSE Recorded Feb 21, 2014
From: BATTELLE MEMORIAL INSTITUTE, PACIFIC NORTHWEST DIVISION
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 032262/0361 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 18, 2013
From: STROHM, JAMES J.; ROBERTS, BENJAMIN Q.; DENSLOW, KAYTE M.
To: BATTELLE MEMORIAL INSTITUTE
Reel/Frame 031807/0578 →
Continuity (1)
Related Publication 20150165413A1 · Jun 18, 2015