R-T-B-M-C sintered magnet and production method and an apparatus for manufacturing the R-T-B-M-C sintered magnet
The present invention discloses an R-T-B-M-C sintered magnet and a method for manufacturing the R-T-B-M-C sintered magnet from an R-T-B-M-C alloy powder including the lubricant. The present invention also discloses an apparatus for manufacturing the R-T-B-M-C sintered magnet from the R-T-B-M-C alloy powder including the lubricant. The apparatus includes an alloy powder feeding mechanism for distributing the R-T-B-M-C alloy powder including the lubricant, a filling mechanism including a mold for receiving the R-T-B-M-C alloy powder including the lubricant, a press mechanism for compressing the R-T-B-M-C alloy powder including the lubricant and a stacking mechanism for storing the mold including the R-T-B-M-C alloy powder including the lubricant.
1. A method for preparing the R-T-B-M-C sintered rare earth magnet from an R-T-B-M-C alloy powder using a mold, said method comprising the steps of;
mixing the R-T-B-M-C alloy powder having a predetermined particle size with a lubricant under an inert gas environment to produce an R-T-B-M-C alloy powder including the lubricant, wherein
R is at least one rare earth element selected from Y and Sc, a weight content of R is at least 25 weight percent (wt. %) and not greater than 40 wt. %,
T is at least one element selected from Fe and Co, a weight content of T is at least 60 wt. % and not greater than 74 wt. %,
M is at least one element selected from Ti, Ni, Nb, Al, V, Mn, Sn, Ca, Mg, Pb, Sb, Zn, Si, Zr, Cr, Cu, Ga, Mo, W and Ta, a weight content of M is not greater than 2 wt. %,
B is boron, a weight content of B is at least 0.8 wt. % and not greater than 1.2 wt. %,
C is carbon, a weight content of C is at least 0.03 wt. % and not greater than 0.15 wt. %,
a weight content of the lubricant is at least 0.05 wt. % and not greater than 2 wt. %,
filling the mold with the R-T-B-M-C alloy powder including the lubricant and oscillating the mold so the R-T-B-M-C alloy powder including the lubricant achieves a filling density of between 2.8 g/cm 3 and 3.8 g/cm 3 under the inert gas environment,
engaging a cover on the mold to compress the R-T-B-M-C alloy powder including the lubricant in the mold under a predetermined pressure between 0.2 MPa and 2 MPa,
orienting the R-T-B-M-C alloy powder including the lubricant in the mold by applying a magnetic field to the R-T-B-M-C alloy powder including the lubricant under the inert gas environment to form a compact,
sintering the compact in the mold,
subjecting the sintered compact to a heat treatment.
2. The method for preparing the R-T-B-M-C sintered rare earth magnet as set forth in claim 1 wherein the lubricant is at least one or a mixture selected from a salt of stearic acid, oleic acid, boric acid, methyl acetate and caprylic acid methyl ester.
3. The method for preparing the R-T-B-M-C sintered rare earth magnet as set forth in claim 1 wherein the magnetic field used in said orienting step is a DC pulsed magnetic field having a magnetic field strength of at least 3.5T.
4. The method for preparing the R-T-B-M-C sintered rare earth magnet as set forth in claim 1 wherein the predetermined particle size of the R-T-B-M-C has an average particle size of less than 8 μm.