Method of bonding perfluoroelastomeric materials to a surface
The invention includes a method of bonding a perfluoroelastomer material to first surface that includes: (a) contacting a first surface with a bonding agent comprising a curable perfluoropolymer and a curing agent; (b) curing the bonding agent to form a perfluoroelastomer material that is bonded to the first surface. In the practice of such method, the bonding agent may be a solution prepared by dissolving the curable perfluoroelastomer and the curing agent in a solvent. In an embodiment of the invention, the perfluoroelastomer material formed in step (b) is a coating layer or, alternatively, the first surface is a surface of a perfluoroelastomer member and the perfluoroelastomer material formed is a perfluoroelastomer weld.
1. A method of bonding a perfluoroelastomer member to a surface, comprising:
(a) contacting a first surface of a perfluoroelastomer member with a bonding agent comprising: a curable perfluoropolymer, and a curing agent;
(b) placing the bonding agent also in contact with a second surface; and
(c) curing the bonding agent to form a perfluoroelastomer weld between the first and second surface, wherein upon curing the perfluoroelastomer weld comprises essentially the same perfluoroelastomer as the perfluoroelastomer member, wherein the perfluoroelastomer members are cured elastomeric materials.
2. The method of claim 1 , further comprising post-curing the perfluoroelastomer weld.
3. The method of claim 2 , wherein the perfluoroelastomer weld is about 95% cured.
4. The method of claim 1 , wherein the perfluoroelastomer member and the weld form a part and the method further comprises post-curing the part.
5. The method of claim 4 , wherein the part is a seal.
6. The method of claim 4 , wherein the part is homogeneous.
7. The method of claim 1 , wherein the perfluoroelastomer weld is homogeneous with the perfluoroelastomer member.
8. The method of claim 1 , wherein the first and second surfaces are on the same perfluoroelastomer member.
9. The method of claim 1 , wherein in step (a) the perfluoroelastomer member is about 75% to about 95% cured.
10. The method of claim 1 , wherein step (b) further comprises: placing the first surface and the second surface within a fixture; and positioning the first surface, the bonding agent and the second surface within the fixture, such that the first surface, the bonding agent and the second surface are in contact.
11. The method of claim 1 , wherein step (c) further comprises heating the bonding agent for a sufficient period of time to effectively cure the bonding agent.
12. The method of claim 1 , wherein step (c) further comprises heating the perfluoroelastomer bonding agent to about 300° F.
13. The method of claim 1 , wherein the bonding agent further comprises a solvent and the bonding agent is contacted with the first surface by coating the first surface with the bonding agent.
14. The method of claim 13 , wherein the solvent is a fluorinated solvent.
15. The method of claim 1 , wherein the curing agent is at least one of a bisphenol or a derivative thereof, a tetraphenyltin, a triazine, and a peroxide-based curing system.
16. The method of claim 1 , wherein the bonding agent is produced by the steps comprising:
compounding a perfluoroelastomer formulation to form a compound; and
dissolving the compound in a solvent to form a solution, wherein the bonding agent is contacted with the first surface by coating the first surface with the bonding agent and the bonding agent is contacted with the first surface by coating the first surface with the bonding agent.
17. The method of claim 16 , wherein the step of dissolving comprises: forming the compound into pieces;
adding about 70% to about 95% by weight solvent to the pieces of the compound, and
grinding the pieces while dissolving the pieces on a ball mill.
18. The method of claim 16 , wherein the solvent is added in an amount of about 90% to about 95% by weight of the solution.
19. A method of bonding a perfluoroelastomer seal to a gland, comprising:
placing a bonding agent comprising a curable perfluoropolymer and curing agent within gaps formed between a perfluoroelastomer seal and a gland; and
curing the bonding agent; wherein upon curing, the perfluoropolymer forms essentially the same perfluoroelastomer as the perfluoroelastomer seal.