IP Library Granted Patent US 9,200,272
Granted Patent B2
US 9,200,272 · App. 14/197,489 · Granted Dec 1, 2015

Extraction buffer and method for isolating high-quality RNA from cells exposed to metal chloride solutions and clay mineral suspensions

Inventors: Andrea Loes (Scottsdale, AZ); Shelley Haydel (Mesa, AZ)
Assignee: Arizona Board of Regents on behalf of Arizona State University
C12N15/1006C07H1/00C07H1/06C07H1/08C07H21/02C07H21/04
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Quick Facts
Patent No.
US 9,200,272
App. No.
14/197,489
Granted
Dec 1, 2015
Kind
B2
Abstract

An RNA extraction buffer, an RNA extraction method, and an RNA extraction kit are described which enable functional, rapid, efficient, and high-quality RNA isolation from samples containing high concentrations of aqueous metal cations, clays, silica, or silicate minerals.

Claims (6)

1. A method for isolating RNA from bacterial cells exposed to one or more of clay mixtures, clay minerals, silicate minerals, phyllosilicates, and aqueous solutions including metal cations, comprising the steps of:

lysing at least one of said bacterial cells; and

extracting RNA separately from DNA with a mixture comprising a sodium phosphate buffer with a pH of about 4.5 to about 6.0, about 1.0 M to about 2.0 M NaCl, about 0.2% hexadecyltrimethylammonium bromide (CTAB), and a chelating agent.

2. The method of claim 1 , wherein the NaCl concentration is about 1.4 M.

3. The method of claim 1 , wherein the chelating agent is about 50 mM EDTA.

4. The method of claim 1 , wherein the extracting step further comprises using said buffer further including about 0.05% diethyl pyrocarbonate for about 12 hours, with diethyl pyrocarbonate subsequently inactivated by autoclaving, and about 1 mM 1,4-dithio-DL-threitol added immediately prior to use.

Assignments (2)
CONFIRMATORY LICENSE Recorded Dec 4, 2014
From: ARIZONA BOARD OF REGENTS, A BODY CORPORATE OF THE STATE OF ARIZONA ACTING FOR AND ON BEHALF OF ARIZONA STATE UNIVERSITY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 034525/0666 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 7, 2014
From: LOES, ANDREA; HAYDEL, SHELLEY
To: ARIZONA BOARD OF REGENTS ON BEHALF OF ARIZONA STATE UNIVERSITY
Reel/Frame 033486/0747 →
Continuity (2)
Provisional Application 61775257 · Mar 8, 2013
Related Publication 20140256929A1 · Sep 11, 2014