IP Library Granted Patent US 10,407,757
Granted Patent B2
US 10,407,757 · App. 14/214,282 · Granted Sep 10, 2019

Sintered nanocrystalline alloys

Inventors: Christopher A. Schuh (Wayland, MA); Mansoo Park (Boston, MA)
Assignee: Massachusetts Institute of Technology
C22C27/04B22F1/0044B22F3/10C22C1/045C22C27/06B22F3/1035B22F2998/10C22C2200/04
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Quick Facts
Patent No.
US 10,407,757
App. No.
14/214,282
Granted
Sep 10, 2019
Kind
B2
Abstract

Provided in one embodiment is a method, comprising: sintering a plurality of nanocrystalline particulates to form a nanocrystalline alloy, wherein at least some of the nanocrystalline particulates may include a non-equilibrium phase comprising a first metal material and a second metal material, and the first metal material may be soluble in the second metal material. The sintered nanocrystalline alloy may comprise a bulk nanocrystalline alloy.

Claims (34)

1. A sintered nanocrystalline alloy comprising W and Cr, wherein the W is present in an amount of at least about 60 at %, the Cr is present in an amount greater than or equal to 0.3 at %, the nanocrystalline alloy has a relative density of at least about 90%, and the nanocrystalline alloy comprises grains having a largest dimension smaller than about 1000 nm.

2. The alloy of claim 1 , wherein the nanocrystalline alloy comprises the W and the Cr in a solid solution.

3. The alloy of claim 2 , wherein the nanocrystalline alloy further comprises Ti.

4. The alloy of claim 1 , wherein the nanocrystalline alloy is substantially thermodynamically stable at a temperature that is greater than or equal to about 1,000° C.

5. The alloy of claim 1 , wherein the nanocrystalline alloy has a relative density of at least about 98%.

6. The alloy of claim 1 , wherein the nanocrystalline alloy further comprises at least one of Pd, Pt, Ni, Co, Fe, Ti, V, and Sc.

7. The alloy of claim 1 , wherein the nanocrystalline alloy has an average grain size of less than about 100 nm.

8. The alloy of claim 1 , wherein the Cr is present in an amount greater than or equal to 1 at %.

9. The alloy of claim 1 , wherein the Cr is present in an amount greater than or equal to 5 at %.

10. The alloy of claim 2 , wherein the Cr is present in an amount greater than or equal to 10 at %.

11. The alloy of claim 1 , wherein the Cr is present in an amount greater than or equal to 15 at %.

12. The alloy of claim 1 , wherein the Cr is present in an amount of 0.3 at % to 40 at %.

13. The alloy of claim 1 , wherein the Cr is present in an amount of 1 at % to 30 at %.

14. The alloy of claim 1 , wherein the W is present in an amount of at least about 70 at %.

15. The alloy of claim 1 , wherein the W is present in an amount of at least about 60 at % and less than or equal to about 95 at %.

16. The alloy of claim 1 , wherein the W is present in an amount of at least about 70 at % and less than or equal to about 95 at %.

17. A bulk nanocrystalline alloy, comprising:

a first metal material that includes W; and

a second metal material that includes Cr,

wherein the bulk nanocrystalline alloy has an average grain size of less than about 100 nm, the W is present in an amount of at least about 60 at %, and the Cr is present in an amount greater than or equal to 0.3 at %.

18. The bulk nanocrystalline alloy of claim 17 , wherein the bulk nanocrystalline alloy has a relative density of at least about 90%.

19. The bulk nanocrystalline alloy of claim 18 , wherein the bulk nanocrystalline alloy has a relative density of at least about 95%.

20. The bulk nanocrystalline alloy of claim 19 , wherein the bulk nanocrystalline alloy has a relative density of at least about 98%.

21. The bulk nanocrystalline alloy of claim 17 , wherein the bulk nanocrystalline alloy is substantially thermodynamically stable at a temperature of about 1,000° C.

22. The bulk nanocrystalline alloy of claim 17 , wherein the W and the Cr are in a solid solution.

23. The bulk nanocrystalline alloy of claim 17 , wherein the Cr is present in an amount greater than or equal to 1 at %.

24. The bulk nanocrystalline alloy of claim 17 , wherein the Cr is present in an amount greater than or equal to 5 at %.

25. The bulk nanocrystalline alloy of claim 17 , wherein the Cr is present in an amount greater than or equal to 10 at %.

26. The bulk nanocrystalline alloy of claim 17 , wherein the Cr is present in an amount greater than or equal to 15 at %.

27. The bulk nanocrystalline alloy of claim 17 , wherein the Cr is present in an amount of 0.3 at % to 40 at %.

28. The bulk nanocrystalline alloy of claim 17 , wherein the Cr is present in an amount of 1 at % to 30 at %.

29. The bulk nanocrystalline alloy of claim 17 , wherein the W is present in an amount of at least about 70 at %.

30. The bulk nanocrystalline alloy of claim 17 , wherein the W is present in an amount of at least about 60 at % and less than or equal to about 95 at %.

31. The bulk nanocrystalline alloy of claim 17 , wherein the W is present in an amount of at least about 70 at % and less than or equal to about 95 at %.

Assignments (4)
CONFIRMATORY LICENSE Recorded Feb 25, 2016
From: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
To: DEFENSE THREAT REDUCTION AGENCY; DEPT. OF DEFENSE, UNITED STATES GOVERNMENT
Reel/Frame 037915/0765 →
CONFIRMATORY LICENSE Recorded Feb 17, 2016
From: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
To: DEFENSE THREAT REDUCTION AGENCY; DEPT. OF DEFENSE, UNITED STATES GOVERNMENT
Reel/Frame 037844/0894 →
CONFIRMATORY LICENSE Recorded Jun 18, 2015
From: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
To: DEFENSE THREAT REDUCTION AGENCY; DEPT. OF DEFENSE; UNITED STATES GOVERNMENT
Reel/Frame 035937/0327 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 19, 2014
From: SCHUH, CHRISTOPHER A.; PARK, MANSOO
To: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
Reel/Frame 032472/0550 →
Continuity (2)
Provisional Application 61784743 · Mar 14, 2013
Related Publication 20140271325A1 · Sep 18, 2014