IP Library Granted Patent US 9,543,496
Granted Patent B2
US 9,543,496 · App. 14/215,947 · Granted Jan 10, 2017

Creation of high-pinning microstructures in post production YBCO coated conductors

Inventors: Ulrich Welp (Lisle, IL); Dean J. Miller (Darien, IL); Wai-Kwong Kwok (Downers Grove, IL); Martin W. Rupich (Framingham, MA); Steven Fleshler (Brookline, MA); Alexis P. Malozemoff (Lexington, MA)
Assignee: UChicago Argonne, LLC
H01L39/126H01L39/143H01L39/2483Y10T428/24413
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Quick Facts
Patent No.
US 9,543,496
App. No.
14/215,947
Granted
Jan 10, 2017
Kind
B2
Abstract

A method comprising irradiating a polycrystalline rare earth metal-alkaline earth metal-transition metal-oxide superconductor layer with protons having an energy of 1 to 6 MeV. The irradiating process produces an irradiated layer that comprises randomly dispersed defects with an average diameter in the range of 1-10 nm.

Claims (12)

1. A method, comprising:

irradiating a polycrystalline rare earth metal-alkaline earth metal-transition metal-oxide superconductor layer comprising at least one selected from the group consisting of metal oxide precipitates, columnar defects, and stacking faults with protons having an energy of 1 to 6 MeV, such that the irradiated layer comprises uniformly distributed randomly dispersed defects with an average diameter in the range of 1-10 nm and the at least one selected from the group consisting of metal oxide precipitates, columnar defects, and stacking faults.

2. The method of claim 1 , wherein the rare earth metal-alkaline earth metal-transition metal-oxide superconductor layer comprises a material with the general formula:

(RE)Ba 2 Cu 3 O 7

where RE is at least one rare earth metal.

3. The method of claim 2 , wherein RE comprises Yttrium.

4. The method of claim 1 , wherein the irradiation has a fluence of at least 1.5×10 16 p/cm 2 .

5. The method of claim 1 , further comprising maintaining the layer at a temperature of less than 200° C. throughout the irradiation.

6. The method of claim 1 , further comprising cooling the layer during the irradiation.

7. The method of claim 1 , wherein the layer is disposed over a textured substrate.

8. The method of claim 1 , wherein the irradiated layer exhibits a superconducting critical current density measured in a c-axis applied magnetic field of at least 1.5 T at a temperature of 27 K at least 10% greater than a reference material of the same chemical composition that does not include the randomly dispersed defects.

9. The method of claim 1 , wherein a metallic protective layer is disposed over the polycrystalline rare earth metal-alkaline earth metal-transition metal-oxide superconductor layer, and irradiating the polycrystalline rare earth metal-alkaline earth metal-transition metal-oxide superconductor layer comprises passing the protons through the metallic protective layer.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 13, 2015
From: WELP, ULRICH; MILLER, DEAN J.; KWOK, WAI-KWONG
To: UCHICAGO ARGONNE, LLC
Reel/Frame 036072/0862 →
CONFIRMATORY LICENSE Recorded Nov 18, 2014
From: UCHICAGO ARGONNE, LLC
To: ENERGY, UNITED STATES DEPARTMENT OF
Reel/Frame 034368/0574 →
Continuity (1)
Related Publication 20150263259A1 · Sep 17, 2015