IP Library Granted Patent US 9,174,932
Granted Patent B2
US 9,174,932 · App. 14/229,152 · Granted Nov 3, 2015

CaSR agonists

Inventors: Masayuki Sugiki (Kawasaki, JP); Toru Okamatsu (Kawasaki, JP); Sayaka Asari (Kawasaki, JP); Yayoi Kawato (Kawasaki, JP); Toshihiro Hatanaka (Kawasaki, JP); Tetsuo Yano (Kawasaki, JP); Yukie Seki (Kawasaki, JP); Naohiro Miyamura (Kawasaki, JP); Hiroaki Nagasaki (Kawasaki, JP); Yuzuru Eto (Kawasaki, JP); Reiko Yasuda (Kawasaki, JP)
Assignee: AJINOMOTO CO., INC.
C07C237/04A23L1/228A23L1/22657A23L1/3051C07C309/51C07F9/3834C07F9/4018C07F9/4021
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Quick Facts
Patent No.
US 9,174,932
App. No.
14/229,152
Granted
Nov 3, 2015
Kind
B2
Abstract

By searching various kinds of compounds having CaSR agonistic activity, the present invention provides CaSR agonistic agents, pharmaceutical compositions, preventive or therapeutic agents for diarrhea and kokumi-imparting agents each of which comprise the compound. More specifically, the present invention provides CaSR agonistic agents, pharmaceutical compositions, preventive or therapeutic agents for diarrhea and kokumi-imparting agents each of which comprise a glutamic acid derivative having CaSR agonistic activity or pharmaceutically acceptable salts thereof.

Claims (54)

1. A compound of formula (I) or a pharmaceutically acceptable salt thereof:

wherein R1, R3, and R5 are each independently selected from the group consisting of a hydrogen atom, a halogen atom, a hydroxyl group, —NH 2 , an optionally substituted alkyl group having 1 to 6 carbon atoms, and an optionally substituted alkoxy group having 1 to 6 carbon atoms;

R4 is selected from the group consisting of a halogen atom, a hydroxyl group, —NH 2 , and an optionally substituted alkoxy group having 1 to 6 carbon atoms;

R2 is selected from the group consisting of a sulfonic acid group,

R6 and R 7 are each independently a hydrogen atom or an optionally substituted alkyl group having 1 to 6 carbon atoms; and

X is a methylene group or an oxygen atom;

and excluding

a compound wherein X is a methylene group, and R2 is

2. The compound or pharmaceutically acceptable salt thereof according to claim 1 ,

wherein R1, R3, and R5 are each independently selected from the group consisting of a hydrogen atom, a halogen atom, a hydroxyl group, —NH 2 , an optionally substituted alkyl group having 1 to 3 carbon atoms, and an optionally substituted alkoxy group having 1 to 3 carbon atoms;

R2 is selected from the group consisting of a sulfonic acid group,

and

R6 and R 7 are each independently a hydrogen atom or a methyl group.

3. The compound or pharmaceutically acceptable salt thereof according to claim 1 ,

wherein R1, R3, and R5 are each independently selected from the group consisting of a hydrogen atom, a a chlorine atom, a bromine atom, a hydroxyl group, —NH 2 , a methyl group, and a methoxy group;

R2 is selected from the group consisting of a sulfonic acid group,

R6 is a hydrogen atom or a methyl group;

R 7 is a hydrogen atom; and

X is a methylene group.

4. The compound or pharmaceutically acceptable salt thereof according to claim 1 ,

wherein R2 is a sulfonic acid group, a carboxylic acid group, or a phosphonic acid group.

5. A compound of formula (I) or a pharmaceutically acceptable salt thereof:

wherein R2 and R5 are each independently selected from the group consisting of a hydrogen atom, a halogen atom, a hydroxyl group, —NH 2 , an optionally substituted alkyl group having 1 to 6 carbon atoms, and an optionally substituted alkoxy group having 1 to 6 carbon atoms;

R4 is selected from the group consisting of a halogen atom, a hydroxyl group, —NH 2 , and an optionally substituted alkoxy group having 1 to 6 carbon atoms;

either of R1 or R3 is a sulfonic acid group and the other is selected from the group consisting of a hydrogen atom, a halogen atom, a hydroxyl group, an unsubstituted amino group, an optionally substituted alkyl group having 1 to 6 carbon atoms, and an optionally substituted alkoxy group having 1 to 6 carbon atoms;

R6 is a hydrogen atom or an optionally substituted alkyl group having 1 to 6 carbon atoms; and

X is a methylene group or an oxygen atom.

6. The compound or pharmaceutically acceptable salt thereof according to claim 5 , wherein R4 is a halogen atom.

7. A pharmaceutical composition comprising the compound or pharmaceutically acceptable salt thereof according to claim 1 .

8. A pharmaceutical composition comprising the compound or pharmaceutically acceptable salt thereof according to claim 5 .

9. The compound or pharmaceutically acceptable salt thereof of claim 1 , which is N 5 -(5-chloro-2-hydroxy-3-sulfophenyl)-L-glutamine.

10. The compound or pharmaceutically acceptable salt thereof of claim 1 , wherein X is methylene.

11. A compound or pharmaceutically acceptable salt thereof, which is

N 5 -(5-chloro-2-hydroxy-3-sulfophenyl)-L-glutamine,

N 5 -(2-hydroxy-3-sulfophenyl)-L-glutamine,

3-(L-(-glutamylamino)-2-hydroxybenzoic acid,

3-bromo-5-(L-(-glutamylamino)benzoic acid,

N 5 -(3-phosphonophenyl)-L-glutamine,

N 5 -(3-chloro-4-methyl-5-sulfophenyl)-L-glutamine,

5-chloro-3-(L-(-glutamylamino)benzoic acid,

O-{[(3-chloro-4-methyl-5-sulfophenyl)amino]carbonyl}-L-serine,

3-{[(2S)-2-amino-2-carboxyethoxycarbonyl]amino}-5-chloro-2-hydroxybenzensulfonic acid, or

O-{[(3-chloro-2-methyl-5-sulfophenyl)amino]carbonyl}-L-serine.

12. The compound or pharmaceutically acceptable salt thereof of claim 1 , wherein X is an oxygen atom.

13. The compound or pharmaceutically acceptable salt thereof of claim 1 , which is

O-{[(3-chloro-4-methyl-5-sulfophenyl)amino]carbonyl}-L-serine,

3-{[(2S)-2-amino-2-carboxyethoxycarbonyl]amino}-5-chloro-2-hydroxybenzensulfonic acid, or

O-{[(3-chloro-2-methyl-5-sulfophenyl)amino]carbonyl}-L-serine.

14. The compound or pharmaceutically acceptable salt thereof of claim 11 , which is

3-(L-(-glutamylamino)-2-hydroxybenzoic acid,

3-bromo-5-(L-(-glutamylamino)benzoic acid,

N 5 -(3-phosphonophenyl)-L-glutamine, or

5-chloro-3-(L-(-glutamylamino)benzoic acid.

15. The compound or pharmaceutically acceptable salt thereof according to claim 1 , wherein R4 is a halogen atom.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 21, 2016
From: AJINOMOTO CO., INC.
To: EA PHARMA CO., LTD.
Reel/Frame 039094/0087 →
Priority Claims (1)
JP 2008-258003 · Oct 3, 2008 · national
Continuity (3)
Continuation 13079273 · Apr 4, 2011
Continuation PCTJP2009067342 · Oct 5, 2009
Related Publication 20140303122A1 · Oct 9, 2014