IP Library Granted Patent US 9,115,089
Granted Patent B2
US 9,115,089 · App. 14/298,610 · Granted Aug 25, 2015

Methyl/fluoro-pyridinyl-methoxy substituted pyridinone-pyridinyl compounds and fluoro-pyrimidinyl-methoxy substituted pyridinone-pyridinyl compounds

Inventors: Susan L. Hockerman (Kirkwood, MO); Joseph B. Monahan (St. Louis, MO); Shaun R. Selness (Chesterfield, MO)
Assignee: CONFLUENCE LIFE SCIENCES, INC.
C07D213/69A61K31/444A61K31/506A61K45/06C07D401/14
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Quick Facts
Patent No.
US 9,115,089
App. No.
14/298,610
Granted
Aug 25, 2015
Kind
B2
Abstract

The present disclosure provides methyl/fluoro-pyridinyl-methoxy substituted pyridinone-pyridinyl compounds and fluoro-pyrimidinyl-methoxy substituted pyridinone-pyridinyl compounds useful in the treatment of p38 kinase mediated diseases, such as lymphoma and auto-inflammatory disease, including rheumatoid arthritis, having the structure of Formula (I): wherein R 1 , R 2 , R 3 , R 4 , R 5 and X are as defined in the detailed description; pharmaceutical compositions comprising at least one of the compounds; and methods for treating p38 kinase mediated diseases using the compound.

Claims (134)

1. A compound of Formula (I):

or a pharmaceutically acceptable salt thereof, wherein:

X is CH or N;

R 1 is selected from the group consisting of H, C 1 -C 6 alkyl, fluoro, chloro, bromo, cyano, or —CF 3 ;

R 2 is selected from the group consisting of H, methyl, cyano, or fluoro;

R 3 is selected from the group consisting of:

R 4 is selected from the group consisting of H, methyl, OH, and O—CH 3 ;

R 5 is H or C 1 -C 3 alkyl;

m is 1 or 2;

n is 0 or 1;

p is 1; and

q is 0 or 1.

2. The compound of claim 1 , wherein the compound has the structure of Formula (II):

or a pharmaceutically acceptable salt thereof, wherein:

X is CH or N;

R 1 is selected from the group consisting of H, C 1 -C 6 alkyl, fluoro, chloro, bromo, cyano, or —CF 3 ;

R 2 is selected from the group consisting of H, methyl, cyano, or fluoro;

R 3 is

R 4 is selected from the group consisting of H, methyl, OH, and —OCH 3 ;

R 5 is H or C 1 -C 3 alkyl;

m is 1 or 2; and

n is 0 or 1.

3. The compound of claim 2 , wherein R 3 is selected from the group consisting of 3,5-difluoropyridin-2-yl, 3-fluoropyridin-2-yl, 5-fluoro-3-methylpyridin-2-yl, 6-fluoropyridin-2-yl, 6-fluoro-4-methylpyridin-2-yl, 3-fluoro-5-methylpyridin-2-yl, and 5-fluoropyridin-2-yl.

4. The compound of claim 3 , wherein the compound has the structure of Formula (III):

or a pharmaceutically acceptable salt thereof, wherein:

X is CH or N;

R 1 is chloro or bromo; and

R 2 is —H or methyl.

5. The compound of claim 4 , wherein the compound is selected from the group consisting of:

3-bromo-4-((3,5-difluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-chloro-4-((3,5-difluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2″,2″-terpyridin]-2-one;

3-bromo-4-((3,5-difluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((3,5-difluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-bromo-4-((3,5-difluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-chloro-4-((3,5-difluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((3,5-difluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((3,5-difluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one.

6. The compound of claim 3 , wherein the compound is selected from the group consisting of:

3-chloro-4-((5-fluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((3-fluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((5-fluoro-3-methylpyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((6-fluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((6-fluoro-4-methylpyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((3-fluoro-5-methylpyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-bromo-4-((5-fluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((5-fluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((5-fluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-chloro-4-((5-fluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-bromo-4-((5-fluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((5-fluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((5-fluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((3-fluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((3-fluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((3-fluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-chloro-4-((3-fluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-bromo-4-((3-fluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((3-fluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((3-fluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((5-fluoro-3-methylpyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((5-fluoro-3-methylpyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((5-fluoro-3-methylpyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-chloro-4-((5-fluoro-3-methylpyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-bromo-4-((5-fluoro-3-methylpyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((5-fluoro-3-methylpyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((5-fluoro-3-methylpyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((6-fluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((6-fluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((6-fluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-chloro-4-((6-fluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-bromo-4-((6-fluoropyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((6-fluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((6-fluoropyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((6-fluoro-4-methylpyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((6-fluoro-4-methylpyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((6-fluoro-4-methylpyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-chloro-4-((6-fluoro-4-methylpyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-bromo-4-((6-fluoro-4-methylpyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((6-fluoro-4-methylpyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((6-fluoro-4-methylpyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((3-fluoro-5-methylpyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((3-fluoro-5-methylpyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((3-fluoro-5-methylpyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-chloro-4-((3-fluoro-5-methylpyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-bromo-4-((3-fluoro-5-methylpyridin-2-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((3-fluoro-5-methylpyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one; and

3-bromo-4-((3-fluoro-5-methylpyridin-2-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one.

7. The compound of claim 1 , wherein the compound has the structure of Formula (IV):

or a pharmaceutically acceptable salt thereof, wherein:

X is CH or N;

R 1 is selected from the group consisting of H, C 1 -C 6 alkyl, fluoro, chloro, bromo, cyano, or —CF 3 ;

R 2 is selected from the group consisting of H, methyl, cyano, or fluoro;

R 4 is selected from the group consisting of H, methyl, OH, and —OCH 3 ;

R 5 is H or C 1 -C 3 alkyl;

m is 1 or 2; and

n is 0 or 1.

8. The compound of claim 7 , wherein the compound has the structure of Formula (V):

or a pharmaceutically acceptable salt thereof, wherein:

X is CH or N;

R 1 is chloro or bromo; and

R 2 is —H or methyl.

9. The compound of claim 8 , wherein the compound is selected from the group consisting of:

3-chloro-4-((4-fluoropyridin-3-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-bromo-4-((4-fluoropyridin-3-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((4-fluoropyridin-3-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((4-fluoropyridin-3-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-chloro-4-((4-fluoropyridin-3-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-bromo-4-((4-fluoropyridin-3-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((4-fluoropyridin-3-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one; and

3-bromo-4-((4-fluoropyridin-3-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one.

10. The compound of claim 1 , wherein the compound has the structure of Formula (VI):

or a pharmaceutically acceptable salt thereof, wherein:

X is CH or N;

R 1 is selected from the group consisting of H, C 1 -C 6 alkyl, fluoro, chloro, bromo, cyano, or —CF 3 ;

R 2 is selected from the group consisting of H, methyl, cyano, or fluoro;

R 4 is selected from the group consisting of H, methyl, OH, and —OCH 3 ;

R 5 is H or C 1 -C 3 alkyl;

p is 1; and

q is 0 or 1.

11. The compound of claim 10 , wherein the compound has the structure of Formula (VII):

or a pharmaceutically acceptable salt thereof, wherein:

X is CH or N;

R 1 is chloro or bromo; and

R 2 is —H or methyl.

12. The compound of claim 11 , wherein the compound is selected from the group consisting of:

3-chloro-4-((5-fluoropyrimidin-4-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-bromo-4-((5-fluoropyrimidin-4-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)pyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((5-fluoropyrimidin-4-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-bromo-4-((5-fluoropyrimidin-4-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-5′,6-dimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one;

3-chloro-4-((5-fluoropyrimidin-4-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-bromo-4-((5-fluoropyrimidin-4-yl)methoxy)-2′-(2-(2-hydroxypropan-2-yl)-5-methylpyrimidin-4-yl)-5′,6-dimethyl-2H-[1,4′-bipyridin]-2-one;

3-chloro-4-((5-fluoropyrimidin-4-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one; and

3-bromo-4-((5-fluoropyrimidin-4-yl)methoxy)-6″-(2-hydroxypropan-2-yl)-3″,5′,6-trimethyl-2H-[1,4′:2′,2″-terpyridin]-2-one.

13. A pharmaceutical composition comprising a therapeutically effective amount of a compound of claim 1 or a pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable carrier.

14. The pharmaceutical composition of claim 13 , further comprising a therapeutically effective amount of an active pharmaceutical ingredient selected from the group consisting of anti-inflammatory drugs, anti-atherosclerotic drugs, immunosuppressive drugs, immunomodulatory drugs, cytostatic drugs, angiogenesis inhibitors, kinase inhibitors, cytokine blockers and inhibitors of cell adhesion molecules.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 15, 2018
From: ACLARIS LIFE SCIENCES, INC.
To: ACLARIS THERAPEUTICS, INC.
Reel/Frame 046153/0695 →
MERGER Recorded Nov 16, 2017
From: CONFLUENCE LIFE SCIENCES, INC.
To: ACLARIS LIFE SCIENCES, INC.
Reel/Frame 044477/0208 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 25, 2014
From: HOCKERMAN, SUSAN L.; MONAHAN, JOSEPH B.; SELNESS, SHAUN R.
To: CONFLUENCE LIFE SCIENCES, INC.
Reel/Frame 033393/0275 →
Continuity (2)
Provisional Application 61832736 · Jun 7, 2013
Related Publication 20140364442A1 · Dec 11, 2014