IP Library Granted Patent US 9,861,958
Granted Patent B2
US 9,861,958 · App. 14/307,031 · Granted Jan 9, 2018

Multifunctional cerium-based nanomaterials and methods for producing the same

Inventors: Matthew J. O'Keefe (Rolla, MO); Carlos E. Castano Londono (Rolla, MO); William G. Fahrenholtz (Rolla, MO)
Assignee: The Curators of The University of Missouri
B01J23/10B01J27/1804B01J35/004B01J37/0217B01J37/0219B01J37/0225B01J37/28B01J37/345C22C21/10C22C21/12C22C23/02C23C22/48C23C22/56C23C22/57C23C22/73C23C22/78C23C22/83C25B1/003B01J35/002B01J35/0006B01J35/0013B01J35/0033B01J37/0226B01J37/035B01J37/06
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Quick Facts
Patent No.
US 9,861,958
App. No.
14/307,031
Granted
Jan 9, 2018
Kind
B2
Abstract

Embodiments relate to a cerium-containing nano-coating composition, the composition including an amorphous matrix including one or more of cerium oxide, cerium hydroxide, and cerium phosphate; and crystalline regions including one or more of crystalline cerium oxide, crystalline cerium hydroxide, and crystalline cerium phosphate. The diameter of each crystalline region is less than about 50 nanometers.

Claims (15)

1. A cerium-containing nano-coating composition, the composition comprising:

an amorphous matrix including one or more of cerium oxide, cerium hydroxide, and cerium phosphate; and

crystalline regions including one or more of crystalline cerium oxide, crystalline cerium hydroxide, and crystalline cerium phosphate;

wherein the crystalline regions are embedded in the amorphous matrix, wherein the thickness of the amorphous matrix with embedded crystalline regions is at least 100 nanometers and the diameter of each crystalline region is less than 50 nanometers.

2. The composition of claim 1 , wherein cerium is present as both trivalent cerium (Ce(III)) and tetravalent cerium (Ce(IV)).

3. The composition of claim 2 , wherein the ratio of the Ce(III) species to the Ce(IV) species is between 0.1 to 1.0.

4. The composition of claim 2 , wherein the Ce(IV) species and Ce(III) species comprise a reversible redox couple.

5. The composition of claim 4 , wherein the Ce(IV)/Ce(III) redox couple is reversible at constant environmental conditions.

6. The composition of claim 2 , wherein Ce(III) content is increasable by up to 33 atomic percent via photocatalytic reduction of Ce(IV) species at ambient conditions.

7. The composition of claim 1 , wherein the composition is capable of self-healing surface cracks.

8. The composition of claim 1 , wherein an achievable band gap differential is 2.0 eV to 4.0 eV.

9. The composition of claim 8 , wherein the band gap is increasable by exposing the composition to sunlight at ambient temperatures and pressures.

10. The composition of claim 1 , wherein the composition is capable of absorbing light having a range of threshold absorption wavelengths up to 590 nanometers.

11. The composition of claim 1 , wherein the composition is capable of photocatalytically splitting water at ambient temperatures and pressures.

12. The composition of claim 1 , wherein the embedded crystalline regions are homogenously distributed in the amorphous matrix.

Assignments (2)
CONFIRMATORY LICENSE Recorded May 16, 2019
From: MISSOURI UNIVERSITY/SCIENCE & TECHNOLOGY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 049220/0007 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 30, 2014
From: O'KEEFE, MATTHEW J.; CASTANO LONDONO, CARLOS E.; FAHRENHOLTZ, WILLIAM G.
To: THE CURATORS OF THE UNIVERSITY OF MISSOURI
Reel/Frame 033208/0700 →
Continuity (2)
Provisional Application 61836007 · Jun 17, 2013
Related Publication 20140371059A1 · Dec 18, 2014