IP Library › Granted Patent US 9,365,921
Granted Patent B2
US 9,365,921 · App. 14/314,566 · Granted Jun 14, 2016

Method for fabricating light-emitting element using chamber with mass spectrometer

Inventors: Shunpei Yamazaki (Tokyo, JP); Satoshi Seo (Kanagawa, JP); Tsunenori Suzuki (Kanagawa, JP)
Assignee: Semiconductor Energy Laboratory Co., Ltd.
C23C14/12C23C14/243C23C14/548H01L51/001H01L51/56
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Quick Facts
Patent No.
US 9,365,921
App. No.
14/314,566
Granted
Jun 14, 2016
Kind
B2
Abstract

A light-emitting element and its fabrication method are provided. The light-emitting element includes an EL layer between a pair of electrode, and the EL layer is formed by evaporation of an organic compound. The evaporation is conducted so that the partial pressure of a component with a specific molecular weight in a film-formation chamber, which is monitored by a mass spectrometer, does not exceed a specific value during the evaporation. This method allows the formation of a light-emitting element having an improved lifetime.

Claims (36)

1. A method for fabricating a semiconductor device, the method comprising:

forming a film by evaporating an organic compound in a film-formation chamber,

wherein a partial pressure of a component in the film-formation chamber is monitored during the evaporation by using a mass spectrometer, and

wherein the component exhibits a m/z in a range from 46 to 200.

2. The method according to claim 1 ,

wherein the component exhibits the m/z in a range from 46 to 130.

3. The method according to claim 1 ,

wherein the component exhibits the m/z of 46, 84, 86, or 92.

4. The method according to claim 1 ,

wherein the organic compound is deposited when the partial pressure is in a range from 1.0×10 −12 Pa to 5.0×10 −8 Pa.

5. The method according to claim 4 ,

wherein the deposition is stopped when the partial pressure is higher than 5.0×10 −8 Pa.

6. The method according to claim 1 ,

wherein the semiconductor device is a light-emitting element.

7. A method for fabricating a semiconductor device, the method comprising:

forming a film by co-evaporating a plurality of organic compounds in a film-formation chamber,

wherein a partial pressure of a component in the film-formation chamber is monitored during the evaporation by using a mass spectrometer, and

wherein the component exhibits a m/z in a range from 46 to 200.

8. The method according to claim 7 ,

wherein the component exhibits the m/z in a range from 46 to 130.

9. The method according to claim 7 ,

wherein the component exhibits the m/z of 46, 84, 86, or 92.

10. The method according to claim 7 ,

wherein the plurality of organic compounds are deposited when the partial pressure is in a range from 1.0×10 −12 Pa to 5.0×10 −8 Pa.

11. The method according to claim 10 ,

wherein the deposition is stopped when the partial pressure is higher than 5.0×10 −8 Pa.

12. The method according to claim 7 ,

wherein the plurality of organic compounds includes a first organic compound and a second organic compound, and

wherein the co-evaporation is performed so that the first organic compound is dispersed in the second organic compound in the film.

13. The method according to claim 12 ,

wherein the first organic compound exhibits a thermally activated delayed fluorescence.

14. The method according to claim 12 ,

wherein the plurality of organic compounds further includes a third organic compound which forms an exciplex with the second organic compound, and

wherein the first organic compound is a phosphorescent substance.

15. The method according to claim 7 ,

wherein the semiconductor device is a light-emitting element.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 25, 2014
From: YAMAZAKI, SH; SEO, SATOSHI; SUZUKI, TSUNENORI
To: SEMICONDUCTOR ENERGY LABORATORY CO., LTD.
Reel/Frame 033176/0879 →
Priority Claims (4)
JP 2013-135919 · Jun 28, 2013 · national
JP 2013-179326 · Aug 30, 2013 · national
JP 2013-179343 · Aug 30, 2013 · national
JP 2013-179351 · Aug 30, 2013 · national
Continuity (1)
Related Publication 20150004722A1 · Jan 1, 2015