IP Library Granted Patent US 9,741,945
Granted Patent B1
US 9,741,945 · App. 14/319,675 · Granted Aug 22, 2017

Tunable photoluminescent metal-organic-frameworks and method of making the same

Inventors: Tina M. Nenoff (Albuquerque, NM); Dorina Florentina Sava Gallis (Albuquerque, NM); Lauren E.S. Rohwer (Albuquerque, NM)
Assignee: National Technology & Engineering Solutions of Sandia, LLC
H01L51/0079H01L51/0089
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Quick Facts
Patent No.
US 9,741,945
App. No.
14/319,675
Granted
Aug 22, 2017
Kind
B1
Abstract

The present disclosure is directed to new photoluminescent metal-organic frameworks (MOFs). The newly developed MOFs include either non rare earth element (REE) transition metal atoms or limited concentrations of REE atoms, including: Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ga, Ge, Y, Ru, Ag, Cd, Sn, Sb, Ir, Pb, Bi, that are located in the MOF framework in site isolated locations, and have emission colors ranging from white to red, depending on the metal concentration levels and/or choice of ligand.

Claims (5)

1. A metal-organic-framework material having the formula selected from a group consisting of X(BTB) 7/3 (H 2 O) 2 .(DEF) 6 , X(BTB)(H 2 O).(H 2 O)(DEF), X(TTB) 2/3 (OA).(DMF) 2.5 , X(TTB)(DEF)(H 2 O).(DEF) 5 , and X(TCBB)(DMA) 4.5 (MeOH), where X is one or more non-rare earth element transition metal atoms or rare earth element atoms.

2. The material of claim 1 , wherein the metal atom is an ion of one or more elements selected from a group consisting of In, Eu, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ga, Ge, Y, Ru, Ag, Cd, Sn, Sb, Ir, Pb and Bi.

3. The material of claim 1 , wherein the metal-organic-framework material selected from a group consisting essentially of InEu(BTB) 7/3 (H 2 O) 2 .(DEF) 6 , Eu(BTB)(H 2 O).(H 2 O)(DEF), In(TTB) 2/3 (OA).(DMF) 2.5 , Eu(TTB)(DEF)(H 2 O).(DEF) 5 , and Eu(TCBB)(DMA) 4.5 (MeOH).

4. A solid state lighting device comprising one or more materials of claim 1 .

5. A light emitting diode comprising one or more of the materials of claim 1 .

Assignments (3)
CHANGE OF NAME Recorded Sep 5, 2017
From: SANDIA CORPORATION
To: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
Reel/Frame 043761/0254 →
CONFIRMATORY LICENSE Recorded Sep 16, 2014
From: SANDIA CORPORATION
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 033753/0584 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 18, 2014
From: NENOFF, TINA M.; SAVA GALLIS, DORINA FLORENTINA; ROHWER, LAUREN E.S.
To: SANDIA CORPORATION
Reel/Frame 033557/0312 →
Continuity (1)
Provisional Application 61842645 · Jul 3, 2013