IP Library Granted Patent US 10,005,674
Granted Patent B2
US 10,005,674 · App. 14/327,720 · Granted Jun 26, 2018

Silica support structure for a zeolite membrane

Inventors: Michael Tsapatsis (Minneapolis, MN); Kumar Varoon Agrawal (Minneapolis, MN); Lorraine Francis (Minneapolis, MN)
Assignee: Regents of the University of Minnesota
C01B33/18C01B33/12D10B2101/02
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Quick Facts
Patent No.
US 10,005,674
App. No.
14/327,720
Granted
Jun 26, 2018
Kind
B2
Abstract

A process for making a mechanically strong, high permeance, and relatively inexpensive support structure for zeolite membranes is described. In an example implementation, a process includes forming a silica powder from silica fibers, mixing the silica powder and a polymer solution to form a mixture, forming the mixture into a shaped mixture, and sintering the shaped mixture to form a silica support.

Claims (7)

1. A silica support, comprising:

a porous layer of interconnected silica particles suitable for supporting a zeolite membrane;

wherein the layer has a nitrogen permeance in a range of approximately 3×10 −5 to 8×10 −5 mol/m 2 sPa; and

wherein the layer of interconnected silica particles comprises interconnected anisotropic silica fibers.

2. The silica support of claim 1 , wherein the layer of interconnected silica particles has inter-particle gaps that are less than 10 μm.

3. The silica support of claim 1 , wherein each anisotropic silica fiber has an aspect ratio in the range of approximately 2 to 10.

4. The silica support of claim 1 , wherein the silica support has a bi-axial flexural strength of 18.2±0.5 MPa as measured by a ring-on-ring test using two Viton O-rings.

Assignments (4)
CONFIRMATORY LICENSE Recorded Nov 20, 2023
From: UNIVERSITY OF MINNESOTA
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 065629/0993 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 12, 2018
From: TSAPATSIS, MICHAEL; AGRAWAL, KUMAR VAROON; FRANCIS, LORRAINE
To: REGENTS OF THE UNIVERSITY OF MINNESOTA
Reel/Frame 045518/0913 →
CONFIRMATORY LICENSE Recorded Jun 22, 2016
From: REGENTS OF THE UNIVERSITY OF MINNESOTA
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 038982/0571 →
CONFIRMATORY LICENSE Recorded Jun 17, 2015
From: REGENTS OF THE UNIVERSITY OF MINNESOTA
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 035851/0865 →
Continuity (2)
Provisional Application 62018142 · Jun 27, 2014
Related Publication 20150376019A1 · Dec 31, 2015