IP Library Granted Patent US 9,416,357
Granted Patent B2
US 9,416,357 · App. 14/358,596 · Granted Aug 16, 2016

Method for isolating total RNA from cells

Inventors: Mark B. Stead (Moorpark, CA); Sidney R. Kushner (Athens, GA)
Assignee: University of Georgia Research Foundation, Inc.
C12N15/1003B01D15/08C07H21/02
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Quick Facts
Patent No.
US 9,416,357
App. No.
14/358,596
Granted
Aug 16, 2016
Kind
B2
Abstract

Provided herein are methods for isolating cellular ribonucleic acid (RNA) from cells. The method includes suspending cells in an extraction solution comprising formamide; incubating the cells and formamide mixture; and pelleting cell debris, DNA, and protein to form an RNA-containing supernatant. Also provided herein are kits for isolating RNA and solutions for extracting RNA from a cell.

Claims (20)

1. A method for isolating cellular ribonucleic acid (RNA), comprising:

(a) suspending cells in an extraction solution comprising formamide in an amount of at least 40% by volume of the extraction solution;

(b) incubating the cells and formamide mixture of step (a); and

(c) pelleting cell debris, DNA, and protein to form an RNA-containing supernatant.

2. The method of claim 1 , further comprising adding zirconium beads prior to incubating the mixture.

3. The method of claim 1 , further comprising pelleting the cells prior to suspending the cells in the extraction solution.

4. The method of claim 1 , wherein the extraction solution further comprises a reducing agent, an anionic detergent, a chelating agent, or a mixture thereof.

5. The method of claim 4 , wherein the reducing agent comprises β-mercaptoethanol or dithiothreitol.

6. The method of claim 5 , wherein the β-mercaptoethanol is present in the extraction solution in an amount of less than 5% by volume of the extraction solution.

7. The method of claim 5 , wherein the β-mercaptoethanol is present in the extraction solution in an amount of less than 2% by volume of the extraction solution.

8. The method of claim 5 , wherein the dithiothreitol is present in the extraction solution at a concentration of from 50 μM to 1 M.

9. The method of claim 4 , wherein the anionic detergent comprises sodium dodecyl sulfate.

10. The method of claim 4 , wherein the anionic detergent is present in the extraction solution in an amount of less than 5% by weight/volume of the extraction solution.

11. The method of claim 4 , wherein the anionic detergent is present in the extraction solution in an amount of less than 0.05% by weight/volume of the extraction solution.

12. The method of claim 4 , wherein the chelating agent comprises EDTA.

13. The method of claim 4 , wherein the chelating agent is present in the extraction solution at a concentration of from 0.5 mM to 50 mM.

14. The method of claim 4 , wherein the chelating agent is present in the extraction solution at a concentration of 18 mM.

15. The method of claim 1 , wherein the extraction solution is substantially free from quaternary amine surfactants.

16. The method of claim 1 , wherein the incubating step is performed at a temperature of from 10° C. to 140° C.

17. The method of claim 1 , wherein the incubating step is performed at a temperature of 95° C.

Assignments (3)
CONFIRMATORY LICENSE Recorded Jun 9, 2016
From: UNIVERSITY OF GEORGIA
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 038926/0417 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 26, 2015
From: KUSHNER, SIDNEY R
To: UNIVERSITY OF GEORGIA RESEARCH FOUNDATION, INC.
Reel/Frame 035266/0621 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 15, 2014
From: STEAD, MARK B.
To: UNIVERSITY OF GEORGIA RESEARCH FOUNDATION, INC.
Reel/Frame 033738/0388 →
Continuity (2)
Provisional Application 61560561 · Nov 16, 2011
Related Publication 20150218550A1 · Aug 6, 2015