IP Library Granted Patent US 9,480,702
Granted Patent B2
US 9,480,702 · App. 14/366,603 · Granted Nov 1, 2016

Use of chemically modified heparin derivates in sickle cell disease

Inventors: Hans-Peter Ekre (Stockholm, SE); Anna Leitgeb (Saltsjöbaden, SE); Mats Wahlgren (Stocksund, SE); Dagmar Pikas (Uppsala, SE)
Assignee: DILAFORETTE AB
A61K31/727A61K45/06C08B37/0063C08B37/0075C08B37/0078
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Quick Facts
Patent No.
US 9,480,702
App. No.
14/366,603
Granted
Nov 1, 2016
Kind
B2
Abstract

The present invention relates to chemically modified heparin for use in the treatment of sickle cell disease, with an antifactor II activity of less than 10 IU/mg, an antifactor Xa activity of less than 10 IU/mg and an average molecular weight (Mw) between about 6.5 and 9.5 kDa.

Claims (17)

1. A method of treating sickle cell disease, comprising:

administering to a patient having sickle cell disease a therapeutically effective amount of a chemically modified heparin having an antifactor IIa activity and an antifactor Xa activity, wherein the antifactor IIa activity is less than 10 IU/mg and the antifactor Xa activity is up to 10 IU/mg, the chemically modified heparin having a weight average molecular weight from about 6.5 to about 9.5 kDa, wherein the chemically modified heparin comprises polysaccharide chains having:

(i) at least 90% of the sulfate groups of the corresponding native heparin;

(ii) a reduction in chemically intact saccharide sequences providing an antithrombin-mediated anticoagulant effect, when compared to the polysaccharide chains of native heparin, and a reduction in unsulfated iduronic and/or glucuronic acid units when compared to native heparin; and

(iii) a predominant disaccharide having the chemical structure:

wherein R′ is a threonate residue and n is an integer of from 2 to 25, such that it comprises from 2 to 25 disaccharide units corresponding to molecular weights from 1.2 to 15 kDa.

2. The method according to claim 1 , wherein at least 30% of the polysaccharide chains have a molecular weight of at least 8 kDa.

3. The method according to claim 1 , wherein the polysaccharide chains have glycol-split residues of the chemical structure:

4. The method according to claim 1 , wherein 3-15% of the polysaccharide chains have a molecular mass of at least 15 kDa.

5. The method according to claim 1 , wherein from 25-47% of the polysaccharide chains have a molecular mass of at least 9 kDa.

6. The method according to claim 1 , wherein from 40-60% of the polysaccharide chains have a molecular mass of at least 7 kDa.

7. The method according to claim 1 , wherein from 60-80% of the polysaccharide chains have a molecular mass of at least 5 kDa.

8. The method according to claim 1 , wherein at least 85% of the polysaccharide chains have a molecular mass of at least 3 kDa.

9. The method according to claim 1 , wherein at least 95% of the polysaccharide chains have a molecular mass of at least 2 kDa.

10. The method according to having claim 1 , wherein the chemically modified heparin has, in a 1 H-NMR spectrum, no unidentified signals in the ranges 0.10-2.00 ppm, 2.10-3.10 ppm and 5.70-8.00 ppm larger than 4 percent when compared to the height of the signal present in native heparin at 5.42 ppm.

11. The method according to claim 1 , wherein the predominantly occurring polysaccharide chains have from 6 to 16 disaccharide units with molecular weights from about 3.6 to about 9.6 kDa.

12. The method according to claim 1 , the treatment is of vaso-occlusive crisis in sickle cell disease.

Assignments (3)
CHANGE OF NAME Recorded Oct 31, 2016
From: DILAFORETTE AB
To: MODUS THERAPEUTICS AB
Reel/Frame 040543/0075 →
CHANGE OF NAME Recorded Oct 20, 2016
From: DILAFORETTE AB
To: MODUS THERAPEUTICS AB
Reel/Frame 040429/0889 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 5, 2014
From: EKRE, HANS-PETER; PIKAS, DAGMAR; LINDAHL, ULF; HOLMER, ERIK; ERIKSSON, PER-OLOV; LEITGEB, ANNA; WAHLGREN, MATS
To: DILAFORETTE AB
Reel/Frame 033676/0447 →
Continuity (2)
Continuation In Part PCTSE2011051538 · Dec 19, 2011
Related Publication 20140364369A1 · Dec 11, 2014