IP Library Granted Patent US 9,773,594
Granted Patent B2
US 9,773,594 · App. 14/370,138 · Granted Sep 26, 2017

Non-rare earth magnetic nanoparticles

Inventors: Everett E. Carpenter (Richmond, VA); Zachary J. Huba (Glen Allen, VA); Kyler J. Carroll (San Diego, CA); Ahmed Farghaly (Richmond, VA); Shiv N. Khanna (Richmond, VA); Meichun Qian (Richmond, VA); Massimo Bertino (Richmond, VA)
Assignee: VIRGINIA COMMONWEALTH UNIVERSITY
H01F1/11C01B31/303H01F1/0063B82Y25/00
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Quick Facts
Patent No.
US 9,773,594
App. No.
14/370,138
Granted
Sep 26, 2017
Kind
B2
Abstract

Continuous flow synthetic methods are used to make single phase magnetic metal alloy nanoparticles that do not contain rare earth metals. Soft and hard magnets made from the magnetic nanoparticles are used for a variety of purposes, e.g. in electric motors, communication devices, etc.

Claims (10)

1. A method of synthesizing single phase non-rare earth metal carbide nanoparticles, comprising:

introducing continuously one or more fluid solutions comprising a salt of a metal into a continuous flow reactor;

in the continuous flow reactor, subjecting said one or more fluid solutions to conditions which allow said salt of the metal to form said single phase non-rare earth metal carbide nanoparticles, wherein said subjecting step includes for a period of time maintaining said one or more fluid solutions at a pressure and temperature sufficient to convert the one or more fluid solutions to a supercritical fluid (SCF); and

recovering said single phase non-rare earth metal carbide nanoparticles,

wherein said single phase non-rare earth metal carbide nanoparticles consist of a material selected from the group consisting of Co 2 C and Co 3 C.

2. A method of synthesizing single phase non-rare earth metal carbide nanoparticles, comprising:

introducing continuously one or more fluid solutions comprising a salt of a metal into a continuous flow reactor:

in the continuous flow reactor, subjecting said one or more fluid solutions to conditions which allow said salt of the metal to form said single phase non-rare earth metal carbide nanoparticles, wherein said subjecting step includes for a period of time maintaining said one or more fluid solutions at a pressure and temperature sufficient to convert the one or more fluid solutions to a supercritical fluid (SCF): and

recovering said single phase non-rare earth metal carbide nanoparticles,

wherein said single phase non-rare earth metal carbide nanoparticles consist of a material selected from the group consisting of Fe 3 C, Fe 5 C 2 , and Fe 7 C 3 .

Assignments (3)
CONFIRMATORY LICENSE Recorded Nov 17, 2023
From: VIRGINA COMMONWEALTH UNIVERSITY
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 065616/0046 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 16, 2016
From: CARPENTER, EVERETT E.; HUBA, ZACHARY J.; CARROLL, KYLER J.; FARGHALY, AHMED; KHANNA, SHIV N.; QIAN, MEICHUN; BERTINO, MASSIMO
To: VIRGINIA COMMONWEALTH UNIVERSITY
Reel/Frame 039452/0774 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 13, 2014
From: CARPENTER, EVERETT E.; HUBA, ZACHARY J.; CARROLL, KYLER J.; FARGHALY, AHMED
To: VIRGINIA COMMONWEALTH UNIVERSITY
Reel/Frame 033522/0419 →
Continuity (4)
Provisional Application 61582963 · Jan 4, 2012
Provisional Application 61662053 · Jun 20, 2012
Provisional Application 61703460 · Sep 20, 2012
Related Publication 20150001437A1 · Jan 1, 2015