IP Library Granted Patent US 9,394,507
Granted Patent B2
US 9,394,507 · App. 14/406,338 · Granted Jul 19, 2016

Biodiesel emulsion for cleaning bituminous coated equipment

Inventors: Gerald Reinke (La Crosse, WI); Gaylon Baumgardner (Jackson, MI); David Cramer (La Crosse, WI)
Assignees: ALM Holding Company; Ergon Asphalt & Emulsions Inc.
C11D3/38B08B3/102C11D1/886C11D3/18C11D3/365
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Quick Facts
Patent No.
US 9,394,507
App. No.
14/406,338
Granted
Jul 19, 2016
Kind
B2
Abstract

Methods of cleaning equipment such as hand tools dirtied by bituminous mixture. A biodiesel emulsion comprising biodiesel, water and emulsifier(s), is applied to the surface of the equipment for a period of time (e.g., at least about 15 minutes) and optionally agitated. The biodiesel emulsion produces cleaning properties comparable to straight biodiesel, at a cost reduction, due to the replacement of biodiesel with water.

Claims (20)

1. A method of cleaning equipment dirtied by bituminous material, the method comprising:

forming a stable, water in oil emulsion comprising biodiesel, 1 to 4 wt-% lecithin-based emulsifier based on the biodiesel weight, and water;

exposing the dirtied equipment to the emulsion for a period of time and agitating either the emulsion or the equipment; and

removing clean equipment from the emulsion.

2. The method of claim 1 , wherein the lecithin-based emulsifier comprises biodiesel, a first lecithin-based emulsifier, a second lecithin-based emulsifier, and water.

3. The method of claim 2 , wherein the first lecithin-based emulsifier has a low HLB.

4. The method of claim 3 wherein the first lecithin-based emulsifier has a 2 to 6 HLB.

5. The method of claim 3 , wherein the second lecithin-based emulsifier has a higher HLB than the first lecithin-based emulsifier.

6. The method of claim 2 , wherein the first lecithin-based emulsifier is present at a level of 1 to 2 wt-% based on the biodiesel weight.

7. The method of claim 1 , wherein the emulsion comprises at least 10 vol-% water.

8. The method of claim 1 , wherein the emulsion comprises at least 20 vol-% water.

9. The method of claim 1 , wherein the emulsion comprises at least 40 vol-% water.

10. The method of claim 1 , wherein the step of forming a stable, water in oil emulsion comprises:

combining the emulsifier with the biodiesel to form an intermediate mixture at a first location, and

combining the water with the intermediate mixture at a second location.

11. A method of cleaning equipment dirtied by bituminous material, the method comprising:

forming a stable, water in oil emulsion comprising biodiesel, 1 to 4 wt-% lecithin-based emulsifier based on the biodiesel weight, and at least 10 volume % water;

immersing the dirtied equipment in the emulsion for a period of time; and

removing clean equipment from the emulsion, the clean equipment being comparably clean to equipment immersed in pure biodiesel.

12. The method of claim 11 , wherein the step of immersing the dirtied equipment in the emulsion for a period of time comprises soaking the dirtied equipment in the emulsion for at least 15 minutes.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 26, 2016
From: CRAMER, DAVID; BAUMGARDNER, GAYLON; REINKE, GERALD
To: ALM HOLDING COMPANY; ERGON ASPHALT & EMULSIONS INC.
Reel/Frame 038385/0680 →
Continuity (2)
Provisional Application 61657268 · Jun 8, 2012
Related Publication 20150152358A1 · Jun 4, 2015