Preparation method of porous ceramic, porous ceramic, and electronic cigarette
The present invention relates to a preparation method of a porous ceramic, the porous ceramic, and a use thereof in the electronic cigarette. The method of preparing a porous ceramic includes: mixing amorphous silica, aluminum oxide and iron oxide uniformly to obtain a mixture; sintering the mixture at a temperature of 1000° C. to 1400° C. for 0.5 hour to 3 hours to obtain a precursor; grinding the precursor to obtain precursor powder; mixing the precursor powder, sodium silicate, and porogen uniformly to obtain a premix; mixing and extruding the premix with water to obtain a molded body; and heat preserving the molded body at a temperature of 200° C. to 600° C. for 1 hour to 6 hours, and sintering the molded body at a temperature of 700° C. to 1200° C. for 0.5 hour to 3 hours to obtain the porous ceramic.
1. A method of preparing a porous ceramic, comprising the steps of:
mixing amorphous silica, aluminum oxide, and iron oxide uniformly to obtain a mixture, wherein the amount of the amorphous silica in the mixture is from 80% to 90% by mass, the amount of the aluminum oxide in the mixture is from 1% to 10% by mass, the amount of iron oxide in the mixture is from 1% to 10% by mass;
sintering the mixture at a temperature of 1000° C. to 1400° C. for 0.5 hour to 3 hours to obtain a precursor;
grinding the precursor to obtain a precursor powder;
mixing the precursor powder, sodium silicate, and porogen uniformly to obtain a premix, wherein the amount of the precursor powder in the premix is from 60% to 90% by mass, the amount of sodium silicate in the premix is from 0% to 20% by mass, the amount of porogen in the premix is from 10% to 40% by mass;
mixing and extruding the premix with water to obtain a molded body;
heat preserving the molded body at a temperature of 200° C. to 600° C. for 1 hour to 6 hours; and
sintering the molded body at a temperature of 700° C. to 1200° C. for 0.5 hour to 3 hours to obtain the porous ceramic.
2. The method according to claim 1 , wherein after the precursor is ground, the precursor is passed through a 50-mesh standard sieve to obtain the precursor powder.
3. The method according to claim 1 , wherein the porogen is at least one selected from the group consisting of sucrose, starch, wood fiber, and short carbon fiber.
4. The method according to claim 3 , wherein a particle size of the sucrose and starch ranges from 10 μm to 150 μm; a diameter of the wood fiber and short carbon fiber ranges from 50 μm to 300 μm; a length of the wood fiber and short carbon fiber ranges from 300 μm to 3000 μm.
5. The method according to claim 1 , wherein a mass ratio of the premix and the water is 3:1 to 6:1.
6. The method according to claim 1 , wherein the extruding is performed under a pressure of 0.5 MPa to 20 MPa.
7. The method according to claim 6 , wherein heat preserving the molded body at the temperature of 200° C. to 600° C. further comprises heating the molded body to the temperature of 200° C. to 600° C. with a heating rate of 1° C./min to 10° C./min.