IP Library Granted Patent US 9,738,534
Granted Patent B2
US 9,738,534 · App. 14/415,017 · Granted Aug 22, 2017

Porous silica powder

Inventors: Hiroshi Kobayashi (Kyoto, JP); Kouji Fujimura (Kyoto, JP); Kanta Nakano (Kyoto, JP)
Assignee: Shinwa Chemical Industries Ltd.
C01B33/18B01D53/02B01J20/103B01J20/283B01J20/28004B01J20/28011B01J20/28016B01J20/28059B01J20/28071B01J20/28085B01J20/3028B01J20/3078B01J20/3085C08K7/26B01D2253/106B01J2220/80C01B33/12C01P2004/51C01P2006/12C01P2006/14C01P2006/16
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Quick Facts
Patent No.
US 9,738,534
App. No.
14/415,017
Granted
Aug 22, 2017
Kind
B2
Abstract

An object of the present invention is to provide a porous silica powder suitable for, for example, a gas chromatography support, and the porous silica powder has an average pore diameter of 0.5 to 10 μm as determined by a mercury intrusion method, a volume of pores having a 100 nm or smaller pore diameter of 0.2 cm 3 /g or less as determined by a nitrogen gas adsorption method, a specific surface area of 0.5 to 100 m 2 /g as determined by a nitrogen gas adsorption method, and a particle size distribution of 10 to 1000 μm.

Claims (13)

1. A porous silica powder consisting of silica particles with a particle size of 100 μm-1000 μm,

and having an average pore diameter of 0.8 to 5.0 μm,

a volume of pores with a 100 nm or smaller pore diameter of 0.001 to 0.1 cm 3 /g,

a specific surface area of 0.7 to 50.0 m 2 /g.

2. The porous silica powder according to claim 1 , having a bulk specific gravity of 0.2 to 0.7 g/mL.

3. The porous silica powder according to claim 1 , obtained by pulverizing or granulating porous silica formed from a reaction mixture comprising acid, a water-soluble polymer, and organosilicate.

4. The porous silica powder according to claim 3 , obtained by forming the porous silica from the reaction mixture using a sol-gel method, and firing the porous silica before or after pulverization or granulation.

5. A gas chromatography support, comprising the porous silica powder of claim 1 .

6. An adsorbent for a liquid component or a gas component, comprising the porous silica powder of claim 1 .

7. The porous silica powder according to claim 2 , obtained by pulverizing or granulating porous silica formed from a reaction mixture comprising acid, a water-soluble polymer, and organosilicate.

8. A gas chromatography column comprising:

a gas chromatography support comprising the porous silica powder of claim 1 , wherein a surface of the gas chromatography support is coated with a non-volatile liquid; and

a tube filled with the gas chromatography support.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 15, 2015
From: KOBAYASHI, HIROSHI; FUJIMURA, KOUJI; NAKANO, KANTA
To: SHINWA CHEMICAL INDUSTRIES LTD.
Reel/Frame 034727/0673 →
Priority Claims (1)
JP 2012-186757 · Aug 27, 2012 · national
Continuity (1)
Related Publication 20150166353A1 · Jun 18, 2015