IP Library Granted Patent US 10,518,323
Granted Patent B2
US 10,518,323 · App. 14/432,646 · Granted Dec 31, 2019

Copper power and method for producing same

Inventors: Yoichi Kamikoriyama (Saitama, JP); Shigeki Nakayama (Saitama, JP)
Assignee: MITSUI MINING & SMELTING CO., LTD.
B22F1/00B22F3/10B22F9/20B22F9/24C22B15/0063C22C9/00H01B1/026H01B1/22H01B13/00H05K1/097B22F1/0018H05K2203/1157Y10T428/12014
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,518,323
App. No.
14/432,646
Granted
Dec 31, 2019
Kind
B2
Abstract

Disclosed is copper powder having an average primary particle size D of 0.15 to 0.6 μm, having a ratio of D to D BET , D/D BET , of 0.8 to 4.0 wherein D BET is a sphere-equivalent average particle diameter calculated from a BET specific surface area, and having no layer for preventing agglomeration on the surface thereof. The copper powder is suitably produced by a method which includes a step of mixing (1) hydrazine and (2) a reactant mixture including a monovalent or divalent copper source and a liquid medium which includes water and an organic solvent having water miscibility and capable of reducing the surface tension of water, to reduce the copper source to form copper particles.

Claims (7)

1. Copper powder having a crystallite size of 37 nm or smaller, an average primary particle size D of 0.15 to 0.6 μm, having a ratio of D to D BET (D/D BET ) of 0.8 to 4.0, wherein D BET is a sphere-equivalent average particle diameter calculated from a BET specific surface area, and having no layer for preventing agglomeration on the surface thereof.

2. The copper powder according to claim 1 , having a total content of carbon, phosphorus, silicon, titanium, and zirconium of 0.10 mass % or less.

3. The copper powder according to claim 2 , having a total content of sodium, sulfur, and chlorine of 0.10 mass % or less.

4. The copper powder according to claim 2 , having a sintering onset temperature of 170° to 240° C.

5. The copper powder according to claim 1 , having a total content of sodium, sulfur, and chlorine of 0.10 mass % or less.

6. The copper powder according to claim 5 , having a sintering onset temperature of 170° to 240° C.

7. The copper powder according to claim 1 , having a sintering onset temperature of 170° to 240° C.

Assignments (2)
CHANGE OF NAME Recorded Mar 31, 2026
From: MITSUI MINING AND SMELTING COMPANY, LIMITED
To: MITSUI KINZOKU COMPANY, LIMITED
Reel/Frame 075357/0342 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 31, 2015
From: KAMIKORIYAMA, YOICHI; NAKAYAMA, SHIGEKI
To: MITSUI MINING & SMELTING CO., LTD.
Reel/Frame 035301/0690 →
Priority Claims (1)
JP 2012-257281 · Nov 26, 2012 · national
Continuity (1)
Related Publication 20150266090A1 · Sep 24, 2015