IP Library Granted Patent US 10,175,391
Granted Patent B2
US 10,175,391 · App. 14/434,699 · Granted Jan 8, 2019

Planarization of optical substrates

Inventors: Christopher Stolz (Lathrop, CA); Jim Folta (Livermore, CA); Paul B. Mirkarimi (Danville, CA); Regina Soufli (Berkeley, CA); Christopher C. Walton (Oakland, CA); Justin Wolfe (Modesto, CA); Carmen Menoni (Fort Collins, CO); Dinesh Patel (Fort Collins, CO)
Assignee: Lawrence Livermore National Security, LLC
G02B3/00C03C17/3417C23C14/08C23C14/34C23C14/3442C23F4/00C03C2218/33Y10T428/265
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Quick Facts
Patent No.
US 10,175,391
App. No.
14/434,699
Granted
Jan 8, 2019
Kind
B2
Abstract

Planarization of defects in laser mirror and other optical component manufacture is disclosed. The planarization is performed by first depositing a relatively thick planarization layer, then carrying out a sequential deposition and etch process. The technique takes advantage of the non-uniform material removal rate as a function of etchant incident angle, and effectively buries the inclusion in a thick film with a near planar top surface. The process enables faster, more reliable manufacture of a non-defective high fluence multilayer mirror particularly suitable for high energy laser applications.

Claims (20)

1. A method of making an optical component in which a substrate surface has at least a one micron size nodular defect, the method comprising:

depositing a planarization layer over the nodular defect;

depositing an ion beam etchable layer over the planarization layer;

etching away a portion of the ion beam etchable layer;

depositing a layer of a metal oxide over the ion beam etchable layer; and

repeating the steps of depositing an ion beam etchable layer, etching away a portion of the ion beam etchable layer, and depositing a layer of the metal oxide, until the nodular defect is reduced in size a predetermined amount.

2. The method of claim 1 wherein:

the optical component comprises a mirror;

the ion beam etchable layer comprises silicon dioxide (SiO 2 ); and

the layer of the metal oxide comprises hafnium dioxide.

3. The method of claim 2 wherein the planarization layer comprises silicon dioxide (SiO 2 ).

4. The method of claim 1 wherein the step of depositing an ion beam etchable layer comprises depositing at least a one micron thick layer of silicon dioxide.

5. The method of claim 4 wherein the step of etching away a portion of the ion beam etchable layer comprises removing 25% to 75% of the layer of silicon dioxide.

6. The method of claim 5 wherein the step of etching away a portion of the ion beam etchable layer comprises removing about half of the layer of silicon dioxide.

7. The method of claim 4 wherein the layer of silicon dioxide is at least two microns thick.

8. The method of claim 1 wherein the step of depositing at least one of the planarization layer or the ion beam etchable layer comprises sputtering silicon dioxide.

9. The method of claim 8 wherein sputtering silicon dioxide comprises ion beam sputtering silicon dioxide.

10. The method of claim 1 wherein the step of etching away a portion of the ion beam etchable layer comprises ion beam etching.

11. The method of claim 1 wherein the step of depositing a layer of a metal oxide comprises sputtering hafnium dioxide.

12. The method of claim 11 wherein sputtering hafnium dioxide comprises ion beam sputtering hafnium dioxide.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 15, 2020
From: MENONI, CARMEN; PATEL, DINESH
To: COLORADO STATE UNIVERSITY RESEARCH FOUNDATION
Reel/Frame 053217/0565 →
CONFIRMATORY LICENSE (SEE DOCUMENT FOR DETAILS) Recorded May 19, 2020
From: LAWRENCE LIVERMORE NATIONAL SECURITY, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 052707/0495 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 18, 2015
From: STOLZ, CHRISTOPHER J.; FOLTA, JAMES A.; MIRKARIMI, PAUL B.; SOUFLI, REGINA; WALTON, CHRISTOPHER CHARLES; WOLFE, JUSTIN
To: LAWRENCE LIVERMORE NATIONAL SECURITY, LLC
Reel/Frame 036352/0954 →
Continuity (2)
Provisional Application 61713332 · Oct 12, 2012
Related Publication 20150276993A1 · Oct 1, 2015