IP Library Granted Patent US 9,024,256
Granted Patent B2
US 9,024,256 · App. 14/453,235 · Granted May 5, 2015

Electron microscope

Inventors: Chong-Yu Ruan (Okemos, MI); Martin Berz (DeWitt, MI); Zhensheng Tao (Lansing, MI)
Assignee: Board of Trustees of Michigan State University
H01J37/263H01J37/073H01J37/045H01J37/065H01J37/228H01J37/26H01J2237/0432H01J2237/06333H01J37/1471H01J37/28H01J2237/2802
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Quick Facts
Patent No.
US 9,024,256
App. No.
14/453,235
Granted
May 5, 2015
Kind
B2
Abstract

An electron microscope is provided. In another aspect, an electron microscope employs a radio frequency which acts upon electrons used to assist in imaging a specimen. Furthermore, another aspect provides an electron beam microscope with a time resolution of less than 1 picosecond with more than 10 5 electrons in a single shot or image group. Yet another aspect employs a super-cooled component in an electron microscope.

Claims (67)

1. An electron microscope comprising:

an electron gun operably emitting electrons;

a radio frequency cavity within which a radio frequency is operably emitted to act upon the electrons;

a pulse shaper adapted to shape a laser pulse received within the radio frequency cavity; and

an imager operably using the electrons to at least one of: (a) create a magnified specimen image, or (b) produce diffraction patterns, after the electrons pass through the radio frequency cavity.

2. The electron microscope of claim 1 , wherein the radio frequency cavity is adjacent the electron gun so as to act together in emitting the electrons, further comprising a bunching radio frequency cavity spaced away from and downstream of the electron gun.

3. The electron microscope of claim 2 , further comprising a laser emitting a laser beam at the electron gun to assist in the emission of the electrons therefrom, and another laser beam also being emitted into a specimen chamber located downstream of the bunching radio frequency cavity.

4. The electron microscope of claim 1 , further comprising an objective lens acting with the radio frequency cavity to control a density and focal distance of the electrons.

5. The electron microscope of claim 4 , wherein the objective lens is an electromagnetic lens and the radio frequency cavity longitudinally compresses and widens at least a 10 5 quantity of the electrons per pulse.

6. The electron microscope of claim 1 , further comprising shaping the laser pulse with the pulse shaper which is controlled by a computer.

7. The electron microscope of claim 6 , further comprising a cooling member super-cooling the radio frequency cavity to 10 Kelvin or less, and the radio frequency cavity being a machinable and super-conducting material.

8. The electron microscope of claim 1 , wherein a quantity of the electrons is more than 10 5 with a time resolution less than 1 picosecond, per pulse.

9. The electron microscope of claim 1 , wherein the electron beam scans a specimen in a raster scan pattern, and the secondarily scattered electrons or beam-induced photons are collected to form an image.

10. The electron microscope of claim 1 , wherein the image is created by transmission electron microscopy such that the electrons pass through a specimen and project onto the imager which is at least one of: (a) a fluorescent screen, or (b) a CCD camera.

11. The electron microscope of claim 1 , wherein the radio frequency cavity is retrofit onto a previously assembled microscope electron beam column.

12. The electron microscope of claim 1 , further comprising a microscope control circuit which comprises an amplifier and a phase shifter connected to the radio frequency cavity, and signals from a laser oscillator being synchronized to the amplifier in a phase-locked loop.

13. The electron microscope of claim 1 , further comprising an electron beam column located between the radio frequency cavity and the electron gun, the radio frequency cavity bunching the electrons prior to imaging.

14. The electron microscope of claim 1 , wherein the electron gun includes a DC gun.

15. An electron microscope comprising:

a radio frequency, femtosecond electron gun assembly operably emitting electrons within a radio frequency wave;

a bunching cavity located downstream of the electron gun assembly and having a radio frequency wave in the bunching cavity for assisting in creating a group of at least a 10 5 quantity of the electrons with a time resolution of less than 1 picosecond, with a pattern of the electrons being wider than longer when they leave the bunching cavity; and

a lens assisting in focusing the electrons.

16. The electron microscope of claim 15 , wherein the electron gun assembly further comprises a super-conducting radio frequency cavity which is super-cooled to less than or equal to 10 Kelvin.

17. The electron microscope of claim 15 , further comprising radio frequency waves of 400 MHz-3 GHz and 100 W-5 kW increase the width-to-length ratio of the at least 10 5 group of electrons between the electron gun and an imager, and the lens being an objective lens that laterally compresses the width of the group of electrons.

18. The electron microscope of claim 15 , wherein a specimen image is created by scanning electron microscopy.

19. The electron microscope of claim 15 , wherein a specimen image is created by transmission electron microscopy.

20. The electron microscope of claim 15 , wherein the radio frequency cavity is retrofit onto a previously assembled microscope electron beam column.

21. An electron microscope comprising:

an electron gun operably emitting a series of electrons;

a housing surrounding at least a portion of the electron gun, the housing being made from a super-conducting material;

a super-cooler attached to the housing to operably cause an internal surface of the housing to have a temperature less than or equal to 10 Kelvin; and

an imager operably using the electrons to create a specimen image.

22. The electron microscope of claim 21 , further comprising a radio frequency wave emitted inside the housing.

23. The electron microscope of claim 22 , further comprising a shaped laser beam pulse received within the housing, and the super-conducting material comprises niobium.

24. The electron microscope of claim 22 , further comprising:

a bunching radio frequency cavity spaced away from the housing;

at least one condenser lens located between the bunching radio frequency cavity and the electron gun; and

an adjustable objective lens located between the bunching radio frequency cavity and the imager.

25. The electron microscope of claim 21 , wherein the super-cooler includes a cryo jacket which causes the internal surface of the housing to have a temperature less than 10 Kelvin.

26. The electron microscope of claim 21 , wherein a quantity of the electrons is more than 10 5 with a time resolution less than 1 picosecond, per image.

27. The electron microscope of claim 21 , wherein the electron beam scans a specimen in a raster scan pattern, and the secondarily scattered electrons or beam-induced photons are collected to form an image.

28. The electron microscope of claim 21 , wherein the image is created by transmission electron microscopy such that the electrons pass through a specimen and project onto the imager which is at least one of: (a) a fluorescent screen, or (b) a CCD camera.

29. An electron microscope comprising an electron gun and an imager, wherein a time resolution for at least 10 5 electrons emitted by the electron gun is less than 1 picosecond per image created by the imager.

30. The electron microscope of claim 29 , further comprising radio frequency waves being emitted adjacent the electron gun.

31. The electron microscope of claim 30 , further comprising a shaped laser beam pulse acting with the electron gun to emit the electrons in a beam toward the imager.

32. The electron microscope of claim 30 , further comprising:

a bunching radio frequency spaced away from the electron gun;

at least one condenser lens located between the bunching radio frequency and the electron gun; and

an adjustable objective lens located between the bunching radio frequency and the imager.

33. The electron microscope of claim 29 , further comprising radio frequency waves of 400 MHz-3 GHz and 100 W-5 kW compress a longitudinal length of the at least 10 5 electrons between the electron gun and the imager.

34. The electron microscope of claim 29 , further comprising super-cooling an internal surface of a radio frequency cavity to 10 Kelvin or less, and the radio frequency cavity being a machinable and super-conducting material.

35. The electron microscope of claim 29 , wherein the image is created by the imager using scanning electron microscopy.

36. The electron microscope of claim 29 , wherein the image is created by the imager using transmission electron microscopy.

37. A method of using an electron microscope, the method comprising:

(a) receiving a shaped laser beam in an upstream radio frequency cavity;

(b) super-cooling the upstream cavity to a temperature less than or equal to 10 Kelvin;

(c) generating an electron beam in the upstream cavity;

(d) bunching the electron beam in a downstream radio frequency cavity; and

(e) using the electron beam to create a specimen image.

38. The method of claim 37 , further comprising using the downstream cavity to bunch a pulse of at least 10 5 electrons of the electron beam with a time resolution of less than 1 picosecond.

39. The method of claim 37 , further comprising using a radio frequency wave of 500 MHz-3 GHz and 100 W-5 kW inside the downstream cavity.

40. The method of claim 37 , further comprising receiving the shaped femtosecond laser pulse in a specimen chamber downstream of the cavities.

41. The method of claim 37 , further comprising varying the electron beam with at least one condenser lens between the cavities, and varying the electron beam with an objective lens after the downstream cavity.

42. The method of claim 37 , further comprising creating the magnified image with scanning electron microscopy.

43. The method of claim 37 , further comprising creating the magnified image with transmission electron microscopy.

44. The method of claim 37 , further comprising shaping pulses of the laser beam with a computer-controlled pulse shaper.

45. The method of claim 37 , further comprising retrofitting the cavities onto a previously assembled microscope.

Assignments (2)
CONFIRMATORY LICENSE Recorded Apr 7, 2015
From: MICHIGAN STATE UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 035386/0128 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 7, 2014
From: RUAN, CHONG-YU; BERZ, MARTIN; TAO, ZHENSHENG
To: BOARD OF TRUSTEES OF MICHIGAN STATE UNIVERSITY
Reel/Frame 033488/0732 →
Continuity (3)
Continuation PCTUS2013024860 · Feb 6, 2013
Provisional Application 61595725 · Feb 7, 2012
Related Publication 20140346355A1 · Nov 27, 2014