IP Library Granted Patent US 9,901,295
Granted Patent B2
US 9,901,295 · App. 14/488,040 · Granted Feb 27, 2018

Near infrared fluorescent single walled carbon nanotubes as tissue localizable biosensors

Inventors: Nicole M. Iverson (Boston, MA); Michael S. Strano (Lexington, MA); Nigel F. Reuel (Cambridge, MA); Thomas P. McNicholas (Cambridge, MA)
Assignee: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
A61B5/14556A61B5/1459A61B5/14552B82Y15/00B82Y30/00A61B5/14532A61B2562/0285A61B2562/12G01N2021/6432G01N2021/7723G01N2021/7786
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Quick Facts
Patent No.
US 9,901,295
App. No.
14/488,040
Granted
Feb 27, 2018
Kind
B2
Abstract

A nanosensor for detecting an analyte can include a substrate, a photoluminescent nanostructure, and a polymer interacting with the photoluminescent nanostructure. The nanosensor can be used in in vivo for biomedical applications.

Claims (54)

1. A nanosensor for detecting an analyte, comprising:

a substrate hydrogel arranged on a support;

a sensor hydrogel arranged on the substrate hydrogel;

a photoluminescent nanostructure embedded in the sensor hydrogel; and

a polymer interacting with the photoluminescent nanostructure,

wherein the polymer is ligated with the sensor hydrogel.

2. The nanosensor of claim 1 , wherein the analyte has a molecule weight of less than 100 g/mol.

3. The nanosensor of claim 2 , wherein the analyte is nitric oxide.

4. The nanosensor of claim 1 , wherein the photoluminescent nanostructure comprises a carbon nanotube.

5. The nanosensor of claim 4 , wherein the carbon nanotube is a single-walled carbon nanotube.

6. The nanosensor of claim 5 , wherein the single-walled carbon nanotube is a semiconductive single-walled carbon nanotube.

7. The nanosensor of claim 1 , wherein the polymer includes an oligonucleotide or a polynucleotide.

8. The nanosensor of claim 7 , wherein the oligonucleotide includes ds(AAAT) 7 (SEQ ID NO: 1).

9. The nanosensor of claim 1 , wherein the photoluminescent nanostructure emits near-infrared radiation in the absence of the analyte.

10. The nanosensor of claim 1 , wherein the photoluminescent nanostructure emits near-infrared radiation in the presence of the analyte.

11. The nanosensor of claim 1 , wherein the polymer includes polyvinyl alcohol, poly(acrylic acid), poly(ethylene oxide), poly(vinyl pyrrolidinone), poly(allyl amine), poly(2-vinylpyridine), or poly(maleic acid).

12. The nanosensor of claim 1 , wherein the concentration of the analyte is less than 1 micromolar.

13. The nanosensor of claim 1 , wherein the interaction between the analyte and the nanosensor includes an interaction between the analyte and the photoluminescent nanostructure.

14. The nanosensor of claim 1 , wherein the substrate hydrogel includes alginate hydrogel.

15. The nanosensor of claim 1 , wherein the sensor hydrogel includes alginate hydrogel.

16. The nanosensor of claim 1 , wherein the polymer includes a copolymer of a hydrophilic polymer and an oligonucleotide.

17. The nanosensor of claim 16 , wherein the hydrophilic polymer is poly(ethylene oxide).

18. The nanosensor of claim 16 , wherein the oligonucleotide is ds(AAAT) 7 (SEQ ID NO: 1) .

19. The nanosensor of claim 16 , wherein the copolymer includes poly(ethylene oxide) and ds(AAAT) 7 (SEQ ID NO: 1).

20. The nanosensor of claim 1 , wherein the substrate hydrogel includes polyethylene glycol.

21. The nanosensor of claim 1 , wherein the sensor hydrogel includes polyethylene glycol.

22. A method of detecting an analyte in a subject, comprising:

introducing a sensor into a subject, wherein the sensor includes:

a substrate hydrogel arranged on a support;

a sensor hydrogel arranged on the substrate hydrogel;

a photoluminescent nanostructure embedded in the sensor hydrogel; and

a polymer interacting with the photoluminescent nanostructure, wherein the polymer is ligated with the sensor hydrogel; and

monitoring emission of radiation from the sensor in the subject.

23. The method of claim 22 , further comprising detecting photoluminescence from the photoluminescent nanostructure.

24. The method of claim 22 , wherein introducing the sensor includes injecting the sensor into a tissue of the subject.

25. The method of claim 22 , wherein the substrate hydrogel includes alginate hydrogel.

26. The method of claim 22 , wherein the sensor hydrogel includes alginate hydrogel.

27. The method of claim 22 , wherein the analyte has a molecule weight of less than 100 g/mol.

28. The method of claim 27 , wherein the analyte is nitric oxide.

29. The method of claim 22 , wherein the photoluminescent nanostructure comprises a carbon nanotube.

30. The method of claim 29 , wherein the carbon nanotube is a single-walled carbon nanotube.

31. The method of claim 30 , wherein the single-walled carbon nanotube is a semiconductive single-walled carbon nanotube.

32. The method of claim 22 , wherein the polymer includes an oligonucleotide or a polynucleotide.

33. The method of claim 32 , wherein the oligonucleotide includes ds(AAAT) 7 (SEQ ID NO: 1).

34. The method of claim 22 , wherein the polymer includes polyvinyl alcohol, poly(acrylic acid), poly(ethylene oxide), poly(vinyl pyrrolidinone), poly(allyl amine), poly(2-vinylpyridine), or poly(maleic acid).

35. The method of claim 22 , wherein the polymer includes a copolymer of a hydrophilic polymer and an oligonucleotide.

36. The method of claim 35 , wherein the hydrophilic polymer is poly(ethylene oxide).

37. The method of claim 35 , wherein the oligonucleotide is ds(AAAT) 7 (SEQ ID NO: 1).

38. The method of claim 35 , wherein the copolymer includes poly(ethylene oxide) and ds(AAAT) 7 (SEQ ID NO: 1).

39. The method of claim 22 , wherein the photoluminescent nanostructure emits near-infrared radiation in the absence of the analyte.

40. The method of claim 22 , wherein the photoluminescent nanostructure emits near-infrared radiation in the presence of the analyte.

41. The method of claim 22 , wherein the concentration of the analyte is less than 1 micromolar.

42. The method of claim 22 , wherein the substrate hydrogel includes polyethylene glycol.

43. The method of claim 22 , wherein the sensor hydrogel includes polyethylene glycol.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 23, 2015
From: IVERSON, NICOLE M.; STRANO, MICHAEL S.; REUEL, NIGEL F.; MCNICHOLAS, THOMAS P.
To: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
Reel/Frame 036630/0746 →
CONFIRMATORY LICENSE Recorded Jun 19, 2015
From: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 035976/0666 →
Continuity (2)
Provisional Application 61878303 · Sep 16, 2013
Related Publication 20150133752A1 · May 14, 2015