IP Library › Granted Patent US 9,353,078
Granted Patent B2
US 9,353,078 · App. 14/503,919 · Granted May 31, 2016

Amino, amido and heterocyclic compounds as modulators of rage activity and uses thereof

Inventors: Ann Marie Schmidt (Franklin Lakes, NJ); Ravichandran Ramasamy (Ardsley, NY); Alexander Shekhtman (Glenmont, NY); Vivek Rai (Allahabad, IN); Michaele B. Manigrasso (New York, NY)
Assignees: New York University; The Research Foundation for The State University of New York
C07D319/20C07D213/75C07D239/42C07D277/28
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Quick Facts
Patent No.
US 9,353,078
App. No.
14/503,919
Granted
May 31, 2016
Kind
B2
Abstract

Amino, amido, and heterocyclic compounds are disclosed. The compounds may be prepared as pharmaceutical compositions, and may be used for the prevention and treatment of a variety of conditions in mammals including humans, including by way of non-limiting example, diabetes complications, inflammation, and neurodegeneration, obesity, cancer, ischemia/reperfusion injury, cardiovascular disease and other diseases related to RAGE activity.

Claims (86)

1. A method for treating or ameliorating in a mammal a disease or condition that is causally related to RAGE activity in vivo, which comprises administering to the mammal an effective disease-treating or condition-treating amount of a compound according to formula B-I′:

wherein

each A 1 , A 2 , A 3 , and A 4 is independently CR 4 or N; provided that only 1 or 2 of A 1 , A 2 , A 3 , and A 4 are N at any one time;

Z is substituted amino, substituted hydroxyl, substituted or unsubstituted aryl, or substituted or unsubstituted heteroaryl;

X is CR 5a or N;

R 1 is hydroxy, substituted hydroxyl, amino, or substituted amino;

R 2 is H, alkyl or aryl;

R 3a is H, substituted or unsubstituted alkyl,substituted or unsubstituted cycloalkyl, substituted or unsubstituted aryl, halo, or cyano;

each R 4 is independently selected from H, OH, substituted or unsubstituted alkyl, substituted or unsubstituted alkoxy, substituted or unsubstituted acyl, substituted or unsubstituted acylamino, substituted or unsubstituted alkylamino, substituted or unsubstituted alkythio, substituted or unsubstituted alkoxycarbonyl, substituted or unsubstituted alkylarylamino, substituted or unsubstituted amino, substituted or unsubstituted arylalkyl, sulfo, substituted sulfo, substituted sulfonyl, substituted sulfinyl, substituted sulfanyl, substituted or unsubstituted aminosulfonyl, substituted or unsubstituted alkylsulfonyl, substituted or unsubstituted arylsulfonyl, azido, substituted or unsubstituted carbamoyl, carboxyl, cyano, substituted or unsubstituted aryl, substituted or unsubstituted heteroaryl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted heterocycloalkyl, substituted or unsubstituted dialkylamino, halo, nitro, and thiol;

R 5a is independently H, substituted or unsubstituted alkyl,substituted or unsubstituted cycloalkyl, substituted or unsubstituted aryl, halo, or cyano; or R 5a and R 3a may join together to form a substituted or unsubstituted carbocyclic or heterocyclic ring;

and each of the subscript m and n is independently 1, 2, or 3;

or a pharmaceutically acceptable salt, solvate or prodrug thereof;

or stereoisomers, isotopic variants and tautomers thereof;

wherein the disease or condition is selected from diabetes and its complications, atherosclerosis, peripheral vascular disease and associated complications, cardiovascular disease nephropathy,retinopathy, cardio- and cerebrovascular ischemia/reperfusion injury, heart attack, myocardial infarction, ischemic cardiomyopathy, cancer, tumor invasion and metastases, acute and chronic inflammation, arthritis,allergy asthma, obesity, pollution-associated tissue or organ damage, infection, sepsis, pneumonia, liver injury/damage, amyloidoses, skin disorders, colitis, lupus, and impaired wound healing.

2. The method according to claim 1 , wherein Z is

wherein B 1 , B 2 , B 3 , and B 4 is independently CR 4 or N; Y is , CR 5b or NR 5a ; R 3b is R 3a ; and R 4 are as in claim 1 ; and R 5b is independently H, substituted or unsubstituted alkyl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted aryl, halo, or cyano; or R 5b and R 3b may join together to form a substituted or unsubstituted carbocyclic or heterocyclic ring.

3. The method according to claim 1 , wherein the compound is according to formula B-I:

wherein

each A 1 , A 2 , A 3 , A 4 , B 1 , B 2 , B 3 , and B 4 is independently CR 4 or N; provided that only 1 or 2 of A 1 , A 2 , A 3 , and A 4 are N, and only 1 or 2 of B 1 , B 2 , B 3 , and B 4 are N at any one time;

X is CR 5a or N; X is CR 5b or N;

R 1 is hydroxy, substituted hydroxyl, amino, or substituted amino;

R 2 is H, alkyl or aryl;

each R 3a and R 3b is independently H, substituted or unsubstituted alkyl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted aryl, halo, or cyano;

each R 4 is independently selected from H, OH, substituted or unsubstituted alkyl, substituted or unsubstituted alkoxy, substituted or unsubstituted acyl, substituted or unsubstituted acylamino, substituted or unsubstituted alkylamino, substituted or unsubstituted alkythio, substituted or unsubstituted alkoxycarbonyl, substituted or unsubstituted alkylarylamino, substituted or unsubstituted amino, substituted or unsubstituted arylalkyl, sulfo, substituted sulfo, substituted sulfonyl, substituted sulfinyl, substituted sulfanyl, substituted or unsubstituted aminosulfonyl, substituted or unsubstituted alkylsulfonyl, substituted or unsubstituted arylsulfonyl, azido, substituted or unsubstituted carbamoyl, carboxyl, cyano, substituted or unsubstituted aryl, substituted or unsubstituted heteroaryl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted heterocycloalkyl, substituted or unsubstituted dialkylamino, halo, nitro, and thiol;

R 5a is independently H, substituted or unsubstituted alkyl,substituted or unsubstituted cycloalkyl, substituted or unsubstituted aryl, halo, or cyano; or R 5a and R 3a may join together to form a substituted or unsubstituted carbocyclic or heterocyclic ring;

R 5b is independently H, substituted or unsubstituted alkyl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted aryl, halo, or cyano; or R 5b and R 3b may join together to form a substituted or unsubstituted carbocyclic or heterocyclic ring;

and each of the subscript m and n is independently 1, 2, or 3;

or a pharmaceutically acceptable salt, solvate or prodrug thereof;

or stereoisomers, isotopic variants and tautomers thereof.

4. The method according to claim 1 , wherein the compound is according to formula B-VII:

and wherein X, Y, R 1 , R 2 , R 3a , R 3b , m, and n are as in claim 3 ;

or a pharmaceutically acceptable salt, solvate or prodrug thereof;

or stereoisomers, isotopic variants and tautomers thereof.

5. The method according to claim 1 , wherein the compound is according to formula B-VIIIa, B-VIIIb, B-VIIIc, or B-VIIId:

and wherein R 1 , R 2 , R 3a , R 3b , R 5a , R 5b , m, and n are as in claim 1 ;

or a pharmaceutically acceptable salt, solvate or prodrug thereof;

or stereoisomers, isotopic variants and tautomers thereof.

6. The method according to claim 1 , wherein the compound is according to formula B-IXa, B-IXb, or B-IXc :

and wherein R 1 , R 2 , R 3b , m, and n are as in claim 3 ;

or a pharmaceutically acceptable salt, solvate or prodrug thereof;

or stereoisomers, isotopic variants and tautomers thereof.

7. The method according to claim 1 , wherein R 1 is OH, alkoxy, or acyloxy.

8. The method according claim 1 , wherein R 2 is substituted or unsubstituted alkyl.

9. The method according to claim 1 , wherein R 2 is substituted or unsubstituted aryl.

10. The method according to claim 1 , wherein m is 1; and n is 1.

11. The method according to claim 1 , wherein the compound is according to formula B-Xa, B-Xb, B-Xc, or B-Xd :

and wherein R 3b is as in claim 3 ;

or a pharmaceutically acceptable salt, solvate or prodrug thereof;

or stereoisomers, isotopic variants and tautomers thereof.

12. The method according to claim 1 , wherein R 3b is independently H, substituted or unsubstituted alkyl,substituted or unsubstituted cycloalkyl, substituted or unsubstituted aryl, halo, or cyano.

13. The method according to claim 1 , wherein the compound is according to formula B-XIa, B-XIb, B-XIc, B-XId, B-XIe, B-XIf, B-XIg, or B-XIh:

or a pharmaceutically acceptable salt, solvate or prodrug thereof;

or stereoisomers, isotopic variants and tautomers thereof.

14. The method according to claim 1 , wherein the compound is according to formula B-XIIa, B-XIIb, B-XIIc, B-XIId, B-XIIe, or B-XIIf:

or a pharmaceutically acceptable salt, solvate or prodrug thereof;

or stereoisomers, isotopic variants and tautomers thereof.

15. The method according to claim 1 , wherein the compound is according to formula B-XIIIa, B-XIIIb, B-XIIIc, or B-XIIId:

or a pharmaceutically acceptable salt, solvate or prodrug thereof;

or stereoisomers, isotopic variants and tautomers thereof.

16. The method according to claim 1 , wherein the compound is according to formula B-XIVa, or B-XIVb:

or a pharmaceutically acceptable salt, solvate or prodrug

or stereoisomers, isotopic variants and tautomers thereof.

17. The method according to claim 1 , wherein the compound is according to formula B-XVa, B-XVb, B-XVc, or B-XVd:

or a pharmaceutically acceptable salt, solvate or prodrug

or stereoisomers, isotopic variants and tautomers thereof.

18. The method according to claim 1 , wherein the compound is according to formula B-XId, or B-XIIIa.

19. The method of any one of claim 1 , 2 , or 3 , wherein each R 4 is independently selected from H, OH, substituted or unsubstituted alkyl, substituted or unsubstituted alkoxy, substituted or unsubstituted acyl, substituted or unsubstituted acylamino, substituted or unsubstituted alkylamino, substituted or unsubstituted alkythio, substituted or unsubstituted alkoxycarbonyl, substituted or unsubstituted alkylarylamino, substituted or unsubstituted amino, substituted or unsubstituted arylalkyl, sulfo, substituted sulfo, substituted sulfonyl, substituted sulfinyl, substituted sulfanyl, substituted or unsubstituted aminosulfonyl, substituted or unsubstituted alkylsulfonyl, substituted or unsubstituted arylsulfonyl, azido, substituted or unsubstituted carbamoyl, carboxyl, cyano, substituted or unsubstituted aryl, substituted or unsubstituted heteroaryl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted heterocycloalkyl, substituted or unsubstituted dialkylamino, Cl, F, nitro, and thiol.

20. A method for treating or ameliorating in a mammal a disease or condition that is causally related to RAGE activity in vivo, which comprises administering to the mammal an effective disease-treating or condition-treating amount of a compound according to formula B-I′:

wherein

each A 1 , A 2 , A 3 , and A 4 is independently CR 4 or N; provided that only 1 or 2 of A 1 , A 2 , A 3 , and A 4 are N at any one time;

Z is

B 1 , B 2 , B 3 , and B 4 is independently CR 4 or N; Y is CR 5b or NR 5a ; R 3b is R 3a ; R 5b is independently H, substituted or unsubstituted alkyl,substituted or unsubstituted cycloalkyl, substituted or unsubstituted aryl, halo, or cyano; or R 5b and R 3b may join together to form a substituted or unsubstituted carbocyclic or heterocyclic ring;

X is CR 5a or N;

R 1 is hydroxy, substituted hydroxyl, amino, or substituted amino;

R 2 is H, alkyl or aryl;

R 3a is H, substituted or unsubstituted alkyl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted aryl, halo, or cyano;

each R 4 is independently selected from H, OH, substituted or unsubstituted alkyl, substituted or unsubstituted alkoxy, substituted or unsubstituted acyl, substituted or unsubstituted acylamino, substituted or unsubstituted alkylamino, substituted or unsubstituted alkythio, substituted or unsubstituted alkoxycarbonyl, substituted or unsubstituted alkylarylamino, substituted or unsubstituted amino, substituted or unsubstituted arylalkyl, sulfo, substituted sulfo, substituted sulfonyl, substituted sulfinyl, substituted sulfanyl, substituted or unsubstituted aminosulfonyl, substituted or unsubstituted alkylsulfonyl, substituted or unsubstituted arylsulfonyl, azido, substituted or unsubstituted carbamoyl, carboxyl, cyano, substituted or unsubstituted aryl, substituted or unsubstituted heteroaryl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted heterocycloalkyl, substituted or unsubstituted dialkylamino, F, Cl, nitro, and thiol;

R 5a is independently H, substituted or unsubstituted alkyl,substituted or unsubstituted cycloalkyl, substituted or unsubstituted aryl, halo, or cyano; or R 5a and R 3a may join together to form a substituted or unsubstituted carbocyclic or heterocyclic ring;

and each of the subscript m and n is independently 1, 2, or 3;

or a pharmaceutically acceptable salt, solvate or prodrug thereof;

or stereoisomers, isotopic variants and tautomers thereof;

wherein the disease or condition is selected from diabetes and its complications, atherosclerosis, peripheral vascular disease and associated complications, cardiovascular disease, nephropathy, retinopathy, cardio- and cerebrovascular ischemia/reperfusion injury, heart attack, stroke, myocardial infarction, ischernic cardiomyopathy, cancer, tumor invasion and metastases, acute and chronic inflammation, arthritis, allergy, asthma, obesity, pollution-associated tissue or organ damage, infection, sepsis, pneumonia, liver injury/damage, amyloidoses, skin disorders, skin aging, colitis, lupus, and impaired wound healing.

21. The method according to claim 20 , wherein the compound is according to formula B-I:

wherein

each A 1 , A 2 , A 3 , A 4 , B 1 , B 2 , B 3 , B 4 , R 1 , R 2 , R 3a , R 3b , R 4 , R 5a , R 5a , m, and n are as in claim 20 ;

or a pharmaceutically acceptable salt, solvate or prodrug thereof; or stereoisomers, isotopic variants and tautomers thereof.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 8, 2015
From: SHEKHTMAN, ALEXANDER
To: THE RESEARCH FOUNDATION OF STATE UNIVERSITY OF NEW YORK
Reel/Frame 035803/0895 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 8, 2015
From: SCHMIDT, ANN MARIE; RAMASAMY, RAVICHANDRAN; MANIGRASSO, MICHAELE B.; RAI, VIVEK
To: NEW YORK UNIVERSITY
Reel/Frame 035856/0454 →
Continuity (3)
Provisional Application 61885183 · Oct 1, 2013
Provisional Application 61885176 · Oct 1, 2013
Related Publication 20150094307A1 · Apr 2, 2015