Tri-axial centrifuge apparatus with electrical sensor, acoustic sensor, and X-ray instrument

1. A method of using a tri-axial centrifuge apparatus, said method comprising the steps of:

providing the tri-axial centrifuge apparatus having:

a tri-axial sample holder located within an inner bore of a cell body;

an axially oriented piston assembly with a piston stem located entirely within the inner bore of the cell body, the axially oriented piston assembly operable to apply an axial pressure on a test sample that is greater than a biaxial confining fluid pressure applied on the test sample, and operable to apply the axial pressure independent of increasing the biaxial confining fluid pressure;

a fluid sample holder, the fluid sample holder being sealingly secured to the cell body and static relative to the cell body;

a test fluid circulation system having a test sample fluid line extending between the tri-axial sample holder and the fluid sample holder and a fluid circulation line extending outside of the cell body between the fluid sample holder and the tri-axial sample holder, the test fluid circulation system providing a fluid circulation path for a test fluid sample;

a centrifuge with a window that is located on a portion of a path of the tri-axial sample holder, where the test fluid circulation system rotates with the cell body within the centrifuge;

at least one electrical sensor;

at least one acoustic sensor; and

an x-ray instrument, wherein the x-ray instrument is static and is aligned with the window of the centrifuge;

loading the test sample in the tri-axial sample holder;

loading the tri-axial sample holder within the inner bore of the cell body of a tri-axial test casing;

applying axial pressure to the test sample with the axially oriented piston assembly with the piston stem located entirely within the inner bore of the cell body;

increasing the biaxial confining fluid pressure in the tri-axial test casing, where the axial pressure is greater than the biaxial confining fluid pressure and applying the axial pressure is independent of increasing the biaxial confining fluid pressure;

equilibrating the pressure, fluid, and temperature for the test sample to a first test condition;

loading the fluid sample holder in the tri-axial test casing, the fluid sample holder being sealingly secured to the cell body and static relative to the cell body;

performing a centrifuge test on the test sample;

performing an x-ray scan of the test sample through the window of the centrifuge that is located on the path of the tri-axial sample holder with the x-ray instrument as the test sample spins past the x-ray instrument;

performing electrical analysis of the test sample; and

performing acoustic analysis of the test sample.

2. A method of using the tri-axial centrifuge apparatus of claim 1 , further comprising before performing the centrifuge test on the test sample, loading the test sample in the centrifuge in a vertical orientation that is parallel to an axis of rotation.

3. A method of using the tri-axial centrifuge apparatus of claim 1 , further comprising before performing the centrifuge test on the test sample, loading the test sample in the centrifuge in a horizontal orientation that is perpendicular to an axis of rotation.

4. A method of using the tri-axial centrifuge apparatus of claim 1 , wherein the performing electrical analysis of the test sample includes measuring at least one of the resistance, conductivity, capacitance, or impedance of the test sample.

5. A method of using the tri-axial centrifuge apparatus of claim 1 , wherein the performing acoustic analysis of the test sample includes measuring sonic velocity data of the test sample.

6. A method of using the tri-axial centrifuge apparatus of claim 1 , wherein the acoustic sensor rotates with the tri-axial test casing.

7. A method of using the tri-axial centrifuge apparatus of claim 1 , wherein the biaxial confining fluid pressure is increased after the axial pressure is applied.

8. A method of using the tri-axial centrifuge apparatus of claim 1 , further comprising providing open two way fluid communication between the tri-axial sample holder and the fluid sample holder.

9. A method of using the tri-axial centrifuge apparatus of claim 1 , where performing the centrifuge test on the test sample includes providing a capillary pressure of at least 10,000 psi.

10. A method of using the tri-axial centrifuge apparatus of claim 1 , where performing the centrifuge test on the test sample includes providing a capillary pressure of at least 20,000 psi.

11. A method of using the tri-axial centrifuge apparatus of claim 1 , where the test fluid sample is a solvent.

12. A method of using the tri-axial centrifuge apparatus of claim 1 , further including performing a saturation and a capillary pressure test at tri-axial test conditions.