IP Library › Granted Patent US 9,481,577
Granted Patent B2
US 9,481,577 · App. 14/520,075 · Granted Nov 1, 2016

Reactor with induction heater

Inventors: Matthew Targett (Shanghai, CN); Hani Gadalla (Madison, WI)
Assignee: LP AMINA LLC
C01B31/32C01B31/303C01B31/308
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Quick Facts
Patent No.
US 9,481,577
App. No.
14/520,075
Granted
Nov 1, 2016
Kind
B2
Abstract

A method for producing usable product in a reactor including introducing a viscous mixture including usable product and unconverted reactant into a chamber of a housing through an inlet, wherein the mixture has a temperature greater than ambient temperature when introduced into the chamber; heating the viscous mixture in the chamber using at least one of an induction heater, an exothermic reaction, a microwave heater, a radio frequency heater, an electrical resistance heater, a laser heater, a plasma heater, and a heated fluid; converting at least a portion of the unconverted reactant to usable product, wherein at least a portion of the usable product is produced in the viscous mixture; and transferring the viscous mixture including usable product from the housing through an outlet.

Claims (65)

1. A method for producing usable product in a reactor, the method comprising:

introducing a viscous mixture comprising usable product and unconverted reactant into a chamber of a housing through an inlet, wherein the mixture has a temperature greater than ambient temperature when introduced into the chamber;

heating the viscous mixture in the chamber using at least one of an induction heater, a microwave heater, a radio frequency heater, an electrical resistance heater, a laser heater, and a plasma heater;

converting at least a portion of the unconverted reactant to usable product, wherein at least a portion of the usable product is produced in the viscous mixture; and

transferring the viscous mixture including usable product from the housing through an outlet;

wherein a level of heat in the chamber is adjustable when heating the viscous mixture to control a flow of the viscous mixture through the reactor, such that the flow of the viscous mixture increases when the level of heat is increased and the flow of the viscous mixture decreases when the level of heat is decreased, and wherein the usable product comprises a carbide.

2. The method of claim 1 , wherein the carbide is selected from a group consisting of calcium carbide, lithium carbide, sodium carbide, potassium carbide, rubidium carbide, cesium carbide, francium carbide, beryllium carbide, strontium carbide, magnesium carbide, barium carbide, and radium carbide.

3. The method of claim 1 , wherein the viscous mixture is configured to solidify when the level of heat is decreased below a solidifying threshold.

4. The method of claim 1 , wherein the viscous mixture in the chamber is directly heated by heat from at least one of the microwave heater, the radio frequency heater, the laser heater, and the plasma heater.

5. The method of claim 1 , wherein the housing further includes a conductive heating element provided around an inner layer of the housing, wherein the heating element is directly heated by the at least one of the induction heater, the microwave heater, the radio frequency heater, the electrical resistance heater, the laser heater, the plasma heater, and the heated gas, and wherein the viscous mixture in the chamber is indirectly heated by the heating element.

6. The method of claim 1 , further comprising:

introducing additional raw reactant into the chamber when introducing the viscous mixture, wherein at least a portion of the additional raw reactant is converted to usable product in the chamber.

7. The method of claim 1 , further comprising:

removing off gases from the reactor for use in a downstream device.

8. The method of claim 1 , wherein transferring the viscous mixture including the usable product from the housing includes transferring the viscous mixture from the housing to a collection device, wherein the collection device is detachably coupled to the housing.

9. A method for producing usable product in a reactor, the method comprising:

introducing a viscous mixture comprising usable product and unconverted reactant into a chamber of a housing through an inlet, wherein the mixture has a temperature greater than ambient temperature when introduced into the chamber;

heating the viscous mixture in the chamber using at least one of an induction heater, an exothermic reaction, a microwave heater, a radio frequency heater, an electrical resistance heater, a laser heater, a plasma heater, and a heated fluid;

converting at least a portion of the unconverted reactant to usable product, wherein at least a portion of the usable product is produced in the viscous mixture; and

transferring the viscous mixture including usable product from the housing through an outlet;

wherein a level of heat in the chamber is adjustable when heating the viscous mixture to control a flow of the viscous mixture through the reactor, such that the flow of the viscous mixture increases when the level of heat is increased and the flow of the viscous mixture decreases when the level of heat is decreased, and wherein the usable product comprises a carbide;

wherein the viscous mixture in the chamber is directly heated by heat from at least one of the exothermic reaction, the microwave heater, the radio frequency heater, the laser heater, the plasma heater, the heated fluid, and the heated gas; and

wherein the heat is produced by microwaves, radio-waves, or a combination of microwaves and radio-waves from a dielectric heater.

10. The method of claim 9 , wherein the housing further includes a conductive heating element provided around an inner layer of the housing, wherein the heating element is directly heated by the microwaves, radio-waves, or a combination of microwaves and radio-waves from a dielectric heater, and wherein the viscous mixture in the chamber is indirectly heated by the heating element.

11. The method of claim 9 , wherein the carbide is selected from a group consisting of calcium carbide, lithium carbide, sodium carbide, potassium carbide, rubidium carbide, cesium carbide, francium carbide, beryllium carbide, strontium carbide, magnesium carbide, barium carbide, and radium carbide.

12. The method of claim 9 , wherein the viscous mixture is configured to solidify when the level of heat is decreased below a solidifying threshold.

13. The method of claim 9 , wherein the housing further includes a conductive heating element provided around an inner layer of the housing, wherein the heating element is directly heated by the at least one of the induction heater, the electrical resistance heater, the laser heater, the plasma heater, the heated fluid, and the heated gas, and wherein the viscous mixture in the chamber is indirectly heated by the heating element.

14. The method of claim 9 , further comprising:

introducing additional raw reactant into the chamber when introducing the viscous mixture, wherein at least a portion of the additional raw reactant is converted to usable product in the chamber; and

removing off gases from the reactor for use in a downstream device.

15. A method for producing usable product in a reactor, the method comprising:

introducing a viscous mixture comprising usable product and unconverted reactant into a chamber of a housing through an inlet, wherein the mixture has a temperature greater than ambient temperature when introduced into the chamber;

heating the viscous mixture in the chamber using at least one of an induction heater, an exothermic reaction, a microwave heater, a radio frequency heater, an electrical resistance heater, a laser heater, a plasma heater, and a heated fluid;

converting at least a portion of the unconverted reactant to usable product, wherein at least a portion of the usable product is produced in the viscous mixture; and

transferring the viscous mixture including usable product from the housing through an outlet;

wherein a level of heat in the chamber is adjustable when heating the viscous mixture to control a flow of the viscous mixture through the reactor, such that the flow of the viscous mixture increases when the level of heat is increased and the flow of the viscous mixture decreases when the level of heat is decreased;

wherein the usable product comprises a carbide;

wherein the housing further includes a conductive heating element provided around an inner layer of the housing;

wherein the viscous mixture in the chamber is indirectly heated by the heating element;

wherein the heating element is directly heated by the induction heater;

wherein the induction heater comprises a power supply and an electrically conductive coil configured to receive electric power from the power supply;

wherein the coil is provided around the heating element and produces an induced oscillating magnetic field when electric power is passed through the coil; and

wherein the oscillating magnetic field induces eddy currents in the conductive heating element generating heat that is transferred to the inner layer via conduction.

16. The method of claim 15 , wherein the carbide is selected from a group consisting of calcium carbide, lithium carbide, sodium carbide, potassium carbide, rubidium carbide, cesium carbide, francium carbide, beryllium carbide, strontium carbide, magnesium carbide, barium carbide, and radium carbide.

17. The method of claim 15 , wherein the viscous mixture is configured to solidify when the level of heat is decreased below a solidifying threshold.

18. The method of claim 15 , further comprising:

introducing additional raw reactant into the chamber when introducing the viscous mixture, wherein at least a portion of the additional raw reactant is converted to usable product in the chamber; and

removing off gases from the reactor for use in a downstream device.

19. A method for producing usable product in a reactor, the method comprising:

introducing a viscous mixture comprising usable product and unconverted reactant into a chamber of a housing through an inlet, wherein the mixture has a temperature greater than ambient temperature when introduced into the chamber;

heating the viscous mixture in the chamber using at least one of an induction heater, an exothermic reaction, a microwave heater, a radio frequency heater, an electrical resistance heater, a laser heater, a plasma heater, and a heated fluid;

converting at least a portion of the unconverted reactant to usable product, wherein at least a portion of the usable product is produced in the viscous mixture; and

transferring the viscous mixture including usable product from the housing through an outlet;

wherein a level of heat in the chamber is adjustable when heating the viscous mixture to control a flow of the viscous mixture through the reactor, such that the flow of the viscous mixture increases when the level of heat is increased and the flow of the viscous mixture decreases when the level of heat is decreased;

wherein the usable product comprises a carbide;

wherein the housing further includes a conductive heating element provided around an inner layer of the housing;

wherein the viscous mixture in the chamber is indirectly heated by the heating element;

wherein the heating element is directly heated by the electrical resistance heater; and

wherein the electrical resistance heater comprises a power supply electrically connected to the heating element to pass electric power through the heating element generating heat that is transferred to the inner layer via conduction.

20. The method of claim 19 , wherein the carbide is selected from a group consisting of calcium carbide, lithium carbide, sodium carbide, potassium carbide, rubidium carbide, cesium carbide, francium carbide, beryllium carbide, strontium carbide, magnesium carbide, barium carbide, and radium carbide.

21. The method of claim 19 , wherein the viscous mixture is configured to solidify when the level of heat is decreased below a solidifying threshold.

22. The method of claim 19 , further comprising:

introducing additional raw reactant into the chamber when introducing the viscous mixture, wherein at least a portion of the additional raw reactant is converted to usable product in the chamber; and

removing off gases from the reactor for use in a downstream device.

23. The method of claim 19 , wherein transferring the viscous mixture including the usable product from the housing includes transferring the viscous mixture from the housing to a collection device, wherein the collection device is detachably coupled to the housing.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 3, 2014
From: TARGETT, MATTHEW; GADALLA, HANI
To: LP AMINA LLC
Reel/Frame 034361/0457 →
Continuity (2)
Provisional Application 61893978 · Oct 22, 2013
Related Publication 20150110703A1 · Apr 23, 2015