IP Library Granted Patent US 9,512,094
Granted Patent B2
US 9,512,094 · App. 14/566,827 · Granted Dec 6, 2016

C17-heteroaryl derivatives of oleanolic acid and methods of use thereof

Inventors: Xin Jiang (Coppell, TX); Christopher F. Bender (Garland, TX); Melean Visnick (Irving, TX)
Assignee: REATA PHARMACEUTICALS, INC.
C07D271/10C07D271/06C07J63/008
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Quick Facts
Patent No.
US 9,512,094
App. No.
14/566,827
Granted
Dec 6, 2016
Kind
B2
Abstract

Disclosed herein are novel C17-heteroaryl derivatives of oleanolic acid, including those of the formula: wherein the variables are defined herein. Also provided are pharmaceutical compositions, kits and articles of manufacture comprising such compounds. Methods and intermediates useful for making the compounds, and methods of using the compounds, for example, as antioxidant inflammation modulators, and compositions thereof are also provided.

Claims (21)

1. A compound of the formula:

wherein:

n is 0-3;

Ar is heteroarenediyl (C≦8) or a substituted version thereof; and

Y is:

hydrogen, hydroxy, halo, amino, or cyano or —NCO; or

alkyl (C≦8) , alkenyl (C≦8) , alkynyl (C≦8) , aryl (C≦12) , aralkyl (C≦12) , heteroaryl (C≦8) , heterocycloalkyl (C≦12) , acyl (C≦12) , alkoxy (C≦8) , aryloxy (C≦12) , acyloxy (C≦8) , alkylamino (C≦8) , dialkylamino (C≦8) , arylamino (C≦8) , aralkylamino (C≦8) , alkylthio (C≦8) , acylthio (C≦8) , alkylsulfonylamino (C≦8) , or substituted versions of any of these groups;

or a pharmaceutically acceptable salt thereof.

2. The compound of claim 1 , wherein Y is —H.

3. The compound of claim 1 , wherein Y is alkyl (C≦4) .

4. The compound of claim 3 , wherein Y is methyl, n-propyl, isopropyl or cyclopropyl.

5. The compound of claim 1 , wherein Y is substituted alkyl (C≦4) .

6. The compound of claim 5 , wherein Y is methoxymethyl.

7. The compound of claim 1 , wherein Ar is

8. The compound of claim 1 , wherein n=0.

9. The compound of claim 1 , wherein n=1.

10. The compound of claim 1 , further defined as:

or a pharmaceutically acceptable salt thereof.

11. A pharmaceutical composition comprising:

a) the compound of claim 1 ; and

b) an excipient.

Assignments (7)
RELEASE OF SECURITY INTEREST Recorded Apr 9, 2025
From: BIOPHARMA CREDIT PLC
To: REATA PHARMACEUTICALS HOLDINGS, LLC; REATA PHARMACEUTICALS GLOBAL, INC.; REATA PHARMACEUTICALS, INC.
Reel/Frame 070793/0228 →
RELEASE OF SECURITY INTEREST Recorded Apr 9, 2025
From: BIOPHARMA CREDIT PLC
To: REATA PHARMACEUTICALS HOLDINGS, LLC; REATA PHARMACEUTICALS GLOBAL, INC.; REATA PHARMACEUTICALS, INC.
Reel/Frame 070793/0130 →
AMENDED AND RESTATED PATENT SECURITY AGREEMENT Recorded Jul 12, 2023
From: REATA PHARMACEUTICALS HOLDINGS, LLC; REATA PHARMACEUTICALS GLOBAL, INC.; REATA PHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 064264/0557 →
PATENT SECURITY AGREEMENT Recorded May 18, 2023
From: REATA PHARMACEUTICALS HOLDINGS, LLC; REATA PHARMACEUTICALS GLOBAL, INC.; REATA PHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 063697/0461 →
RELEASE OF SECURITY INTEREST Recorded Jun 24, 2020
From: OXFORD FINANCE LLC, AS COLLATERAL AGENT
To: REATA PHARMACEUTICALS, INC.
Reel/Frame 053034/0018 →
SECURITY INTEREST Recorded Jun 14, 2018
From: REATA PHARMACEUTICALS, INC.
To: OXFORD FINANCE LLC, AS COLLATERAL AGENT
Reel/Frame 046357/0605 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 22, 2015
From: JIANG, XIN; BENDER, CHRISTOPHER F.; VISNICK, MELEAN
To: REATA PHARMACEUTICALS, INC.
Reel/Frame 034789/0913 →
Continuity (3)
Continuation In Part 14022843 · Sep 10, 2013
Provisional Application 61699199 · Sep 10, 2012
Related Publication 20150152071A1 · Jun 4, 2015