Process for hot application of a silylated adhesive composition
A process for hot application of an adhesive composition ( 80 ) on a support ( 96 ), by means of a nozzle ( 50 ) applying the adhesive composition ( 80 ), a line ( 88 ) supplying the nozzle ( 50 ) with the adhesive composition ( 80 ) to be applied in fluid form, a mixer ( 30 ) positioned in the line ( 88 ) for the homogeneous mixture of the main components of the adhesive composition before its application; the applied adhesive composition ( 80 ) including a silylated prepolymer, a compatible tackifying resin; the adhesive composition having a cross-linking catalyst; the process involving: supplying the line ( 88 ) with the silylated prepolymer separated from the cross-linking catalyst, the mixing of the cross-linking catalyst with the main components by the mixer ( 30 ), the hot application of the mixed adhesive composition ( 80 ) onto a support ( 96 ).
1. A process for hot application of an adhesive composition on a support, comprising employing a hot application system comprising:
an application nozzle applying the adhesive composition,
a supply line supplying the application nozzle with the adhesive composition to be applied in fluid form,
a mixer positioned in the supply line homogeneously mixing main components of the adhesive composition before its application, wherein the mixer comprises, at an injection point of a cross-linking catalyst, a part reducing the free passage for said cross-linking catalyst to locally increase the flow rate of said cross-linking catalyst upon mixing;
wherein the mixer further comprises at least one mixing element having deflective surfaces positioned downstream from said injection point of the cross-linking catalyst,
the applied adhesive composition including as main components:
from 20% to 85% by weight of silylated pre-polymer,
from 15 to 80% by weight of compatible tackifying resin; and further comprising the cross-linking catalyst from 0.01 to 3% by weight;
the process comprising:
supplying the supply line with said at least silylated pre-polymer, separate from the cross-linking catalyst,
injecting the cross-linking catalyst in the supply line at the injection point in the mixer, wherein the cross-linking catalyst is in intermediate or turbulent conditions upon passing through the part reducing its free passage at the injection point,
wherein the mixture of the at least silylated pre-polymer and the cross-linking catalyst is in laminar flow in the mixer downstream from the injection point of the cross-linking catalyst,
mixing the cross-linking catalyst with the at least silylated pre-polymer in the mixer, to form a mixed adhesive composition, heating the mixed adhesive composition, and
applying the heated mixed adhesive composition on a support by the application nozzle.
2. The hot application process according to claim 1 , wherein, upon supplying the supply line, the cross-linking catalyst is separated from the whole of the main components of the adhesive composition.
3. The hot application process according to claim 2 , wherein the mixer is a static mixer.
4. The hot application process according to claim 3 , wherein the static mixer includes an electrically conducting material, the hot application system comprising an in-line heating device, including an inductive coil surrounding a portion of the static mixer, the process comprising, prior to the hot application, heating of the adhesive composition up to the application temperature, by electrically powering the inductive coil of the in-line heating device.
5. The hot application process according to claim 4 , wherein the adhesive composition is applied at a temperature comprised between 50° C. and 140° C.
6. The hot application process according to claim 2 , wherein the adhesive composition to be applied cross-links with humidity.
7. The hot application process according to claim 2 , wherein the adhesive composition is applied at a temperature comprised between 50° C. and 140° C.
8. The hot application process according to claim 1 , wherein the mixer is a static mixer.
9. The hot application process according to claim 8 , wherein the static mixer includes an electrically conducting material, the hot application system comprising an in-line heating device, including an inductive coil surrounding a portion of the static mixer, the process comprising, prior to the hot application, heating of the adhesive composition up to the application temperature, by electrically powering the inductive coil of the in-line heating device.
10. The hot application process according to claim 9 , wherein the adhesive composition is applied at a temperature comprised between 50° C. and 140° C.
11. The hot application process according to claim 1 , wherein the adhesive composition to be applied cross-links with humidity.
12. The hot application process according to claim 11 , wherein the adhesive composition is applied at a temperature comprised between 50° C. and 140° C.
13. The hot application process according to claim 1 , wherein the system comprises heater able to be positioned at a storage reservoir comprising at least one of the separate main components for raising said at least one main component to a pumping temperature.
14. The hot application process according to claim 13 , wherein said at least one separate main component is raised to a pumping temperature comprised between 50° C. and 140° C.
15. The hot application process according to claim 1 , wherein the adhesive composition is applied at a temperature comprised between 50° C. and 140° C.