IP Library Granted Patent US 9,395,245
Granted Patent B2
US 9,395,245 · App. 14/603,700 · Granted Jul 19, 2016

Data knitting tandem dispersive range monochromator

Inventors: Jerome J. Workman, Jr. (Danbury, CT); Tushar Saraf (Lincoln, NE); Thomas Andrew Bennett (Brookfield, CT)
G01J3/18G01J3/0202G01J3/027G01J3/06G01J3/10G01J2003/1866
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Quick Facts
Patent No.
US 9,395,245
App. No.
14/603,700
Granted
Jul 19, 2016
Kind
B2
Abstract

Aspects of a tandem dispersive range monochromator and data knitting for the monochromator are described herein. In one embodiment, the monochromator includes a tandem diffraction grating, a grating drive motor that rotates the tandem diffraction grating to provide, by diffraction of broadband light, first dispersed wavelengths of light and second dispersed wavelengths of light, a detector that detects a first reflection from the first dispersed wavelengths of light and a second reflection from the second dispersed wavelengths of light, and processing circuitry that knits together data values from the first reflection and data values from the second reflection to provide a spectrum of combined data values. By using a tandem diffraction grating having different dispersive surfaces, measurements of relatively high precision and quality may be taken throughout a wider spectral range, and the measurements may be knitted together to provide a spectrum of combined data values.

Claims (48)

1. A monochromator, comprising:

a tandem diffraction grating including a first diffraction grating, a second diffraction grating, and a mounting assembly having a rotatable shaft to rotate the tandem diffraction grating;

a grating drive motor that rotates the tandem diffraction grating about a pivot point of the rotatable shaft to provide, by diffraction of broadband light, first dispersed wavelengths of light from the first diffraction grating and second dispersed wavelengths of light from the second diffraction grating;

a detector that detects a first reflection of at least a portion of the first dispersed wavelengths of light and a second reflection of at least a portion of the second dispersed wavelengths of light; and

processing circuitry that aligns data values from the first reflection with data values from the second reflection and smooths at least a portion of the data values from the first reflection with at least a portion of the data values from the second reflection to provide a combined spectrum of data values across the first dispersed wavelengths of light and the second dispersed wavelengths of light.

2. The monochromator of claim 1 , wherein

the first diffraction grating includes a first periodic surface structure for a first range of ultra-violet (UV) to visible (VIS) wavelengths of the broadband light; and

the second diffraction grating includes a second periodic surface structure for a second range of near-infrared (NIR) to infrared (IR) wavelengths of the broadband light.

3. The monochromator of claim 1 , wherein, to provide the combined spectrum of data values, the processing circuitry aligns the data values from the first reflection with the data values from the second reflection based on data values which overlap in spectral range among the first reflection and the second reflection.

4. The monochromator of claim 1 , wherein, to smooth the at least a portion of the data values from the first reflection with the at least a portion of the data values from the second reflection, the processing circuitry averages the at least a portion of the data values from the first reflection with the at least a portion of the data values from the second reflection.

5. The monochromator of claim 4 , wherein the portion of the data values from the first reflection and the portion of the data values from the second reflection overlap in spectral range.

6. The monochromator of claim 1 , further comprising:

a sample tray;

a sample tray drive motor; and

a sample position encoder mounted in connection with the sample tray drive motor that identifies an angular orientation of the sample tray.

7. The monochromator of claim 1 , wherein the processing circuitry further controls the grating drive motor to regulate an angular velocity of the tandem diffraction grating based on an angular orientation of the tandem diffraction grating.

8. The monochromator of claim 7 , further comprising:

a sample tray drive motor, wherein

the processing circuitry further controls the sample tray drive motor to vary an angle of incidence of at least one of the first dispersed wavelengths of light and the second dispersed wavelengths of light onto a sample while the processing circuitry controls the grating drive motor to regulate the angular velocity of the tandem diffraction grating.

9. A method of scanning, comprising:

rotating, by a grating drive motor, a tandem diffraction grating about a pivot point to provide, by diffraction of broadband light, first dispersed wavelengths of light from a first diffraction grating and second dispersed wavelengths of light from a second diffraction grating;

detecting, by a detector, a first reflection of at least a portion of the first dispersed wavelengths of light and a second reflection of at least a portion of the second dispersed wavelengths of light; and

knitting together, with processing circuitry, data values from the first reflection and data values from the second reflection to provide a combined spectrum of data values across the first dispersed wavelengths of light and the second dispersed wavelengths of light, wherein the knitting together comprises:

aligning the data values from the first reflection with the data values from the second reflection; and

smoothing at least a portion of the data values from the first reflection with at least a portion of the data values from the second reflection.

10. The method of claim 9 , wherein the tandem diffraction grating comprises:

a first diffraction grating having a first periodic surface structure for a first range of ultra-violet (UV) to visible (VIS) wavelengths of the broadband light; and

a second diffraction grating having a second periodic surface structure for a second range of near-infrared (NIR) to infrared (IR) wavelengths of the broadband light.

11. The method of claim 9 , wherein the knitting comprises aligning the data values from the first reflection with the data values from the second reflection based on data values which overlap in spectral range among the first reflection and the second reflection.

12. The method of claim 9 , wherein the smoothing comprises averaging the at least a portion of the data values from the first reflection with the at least a portion of the data values from the second reflection.

13. The method of claim 9 , further comprising:

identifying, with a position encoder, an angular orientation of the tandem diffraction grating over an angular range; and

controlling, with processing circuitry, the grating drive motor to regulate an angular velocity of the tandem diffraction grating based on the angular orientation of the tandem diffraction grating.

14. A monochromator, comprising:

a light source that provides broadband light;

an entrance optics assembly that collimates the broadband light;

an entrance slit that passes at least a portion of the broadband light;

a tandem diffraction grating including a first diffraction grating, a second diffraction grating, and a mounting assembly having a rotatable shaft to rotate the tandem diffraction grating, the first diffraction grating including a first periodic surface structure, and the second diffraction grating including a second periodic surface structure;

a grating drive motor that rotates the tandem diffraction grating about a pivot point of the rotatable shaft to provide, by dispersion from the first diffraction grating and the second diffraction grating, first dispersed wavelengths of light and second dispersed wavelengths of light;

a detector that detects a first reflection of at least a portion of the first dispersed wavelengths of light and a second reflection of at least a portion of the second dispersed wavelengths of light; and

processing circuitry that aligns data values from the first reflection with data values from the second reflection and smooths at least a portion of the data values from the first reflection with at least a portion of the data values from the second reflection to provide a combined spectrum of data values across the first dispersed wavelengths of light and the second dispersed wavelengths of light.

15. The monochromator of claim 14 , wherein, to provide the combined spectrum of data values, the processing circuitry aligns the data values from the first reflection with the data values from the second reflection based on data values which overlap in spectral range among the first reflection and the second reflection.

16. The monochromator of claim 15 , wherein, to smooth the at least a portion of the data values from the first reflection with the at least a portion of the data values from the second reflection, the processing circuitry averages the at least a portion of the data values from the first reflection with the at least a portion of the data values from the second reflection.

17. The monochromator of claim 14 , wherein the processing circuitry further controls the grating drive motor to regulate an angular velocity of the tandem diffraction grating based on an angular orientation of the tandem diffraction grating.

18. The monochromator of claim 14 , further comprising:

a sample tray that holds a sample for evaluation; and

a sample tray drive motor, wherein

the processing circuitry further controls the sample tray drive motor to vary an angle of incidence of at least one of the first dispersed wavelengths of light and the second dispersed wavelengths of light onto the sample.

Assignments (7)
PATENT SECURITY AGREEMENT Recorded Feb 13, 2026
From: KPM ANALYTICS NORTH AMERICA CORPORATION
To: CCP AGENCY, LLC, AS ADMINISTRATIVE AGENT
Reel/Frame 074852/0543 →
RELEASE OF SECURITY INTEREST RECORDED AT REEL/FRAME 047989/0327 Recorded Jul 7, 2021
From: CRYSTAL FINANCIAL LLC
To: KPM ANALYTICS NORTH AMERICA CORPORATION (FORMERLY KNOWN AS PROCESS SENSORS CORPORATION)
Reel/Frame 057106/0699 →
SECURITY INTEREST Recorded Jul 2, 2021
From: KPM ANALYTICS NORTH AMERICA CORPORATION (FORMERLY KNOWN AS PROCESS SENSORS CORPORATION)
To: SOUND POINT AGENCY LLC
Reel/Frame 056741/0373 →
CHANGE OF NAME Recorded Jan 22, 2019
From: PROCESS SENSORS CORPORATION
To: KPM ANALYTICS NORTH AMERICA CORPORATION
Reel/Frame 049514/0312 →
MERGER AND CHANGE OF NAME Recorded Jan 22, 2019
From: WESTCO SCIENTIFIC INSTRUMENTS, INC.; PROCESS SENSORS CORPORATION
To: PROCESS SENSORS CORPORATION
Reel/Frame 048093/0794 →
PATENT SECURITY AGREEMENT Recorded Dec 28, 2018
From: KPM ANALYTICS NORTH AMERICA CORPORATION (FORMERLY KNOWN AS PROCESS SENSORS CORPORATION)
To: CRYSTAL FINANCIAL LLC, AS AGENT
Reel/Frame 047989/0327 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 26, 2015
From: WORKMAN, JEROME J., JR; SARAF, TUSHAR; BENNETT, THOMAS ANDREW
To: WESTCO SCIENTIFIC INSTRUMENTS, INC.
Reel/Frame 034807/0574 →
Continuity (3)
Continuation In Part 14213214 · Mar 14, 2014
Provisional Application 61792209 · Mar 15, 2013
Related Publication 20150138536A1 · May 21, 2015