IP Library Granted Patent US 9,410,058
Granted Patent B2
US 9,410,058 · App. 14/604,960 · Granted Aug 9, 2016

Compositions and methods for water-resistant gypsum fiber products

Inventors: David R. Blackburn (Barrington, IL); Yufeng Xu (Gurnee, IL)
Assignee: UNITED STATES GYPSUM COMPANY
C09D183/04B05D3/0272C04B11/02C04B28/14C04B41/009C04B41/4927C04B41/64C04B2111/0062C04B2111/00482C04B2111/00629C04B2111/27C08K3/30C08K2003/3045
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Quick Facts
Patent No.
US 9,410,058
App. No.
14/604,960
Granted
Aug 9, 2016
Kind
B2
Abstract

A water-resistant gypsum fiber product comprising siloxane and coated with a coating comprising alkali metal organosiliconate is provided. A method of making a gypsum fiber product in which siloxane is cross-linked at the surface of the product is also provided. A fuel-efficient method for making the product and reducing the amount of siloxane dust released is provided as well.

Claims (15)

1. A method for decreasing the amount of siloxane dust generated in a kiln, the method comprising:

preparing a gypsum slurry comprising calcium sulfate dihydrate;

heating the slurry under pressure to calcine the calcium sulfate dihydrate to form alpha-calcined calcium sulfate hemihydrate;

relieving the pressure;

after the step of calcining under pressure has been completed and the pressure has been relieved, adding a siloxane dispersion to the slurry;

dewatering the slurry to form a filter cake;

forming the cake into a desired shape;

allowing the cake to set to form a product;

coating the product with a coating comprising alkali metal organosiliconate;

placing the coated product in the kiln; and

thereby decreasing the amount of siloxane dust generated in a kiln.

2. The method of claim 1 , wherein the alkali metal organosiliconate is potassium methyl siliconate.

3. The method of claim 1 , wherein the siloxane is methylhydrogensiloxane.

4. The method of claim 1 , wherein the siloxane is used in amounts of about 0.08% to about 1.0% by weight of the total amount of gypsum.

5. The method of claim 1 , wherein the alkali metal organosiliconate is used in the amount from 0.1% to 10% by weight of the coating and from 0.002% to 2% by weight of the total amount of gypsum.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 26, 2015
From: BLACKBURN, DAVID R.; XU, YUFENG
To: UNITED STATES GYPSUM COMPANY
Reel/Frame 034810/0250 →
Continuity (2)
Provisional Application 61977885 · Apr 10, 2014
Related Publication 20150291844A1 · Oct 15, 2015