IP Library Granted Patent US 9,969,903
Granted Patent B2
US 9,969,903 · App. 14/606,544 · Granted May 15, 2018

Method of applying an organosilane solution to rigid substrates and grout

Inventors: Silver Cornia (Casinalbo, IT); Curt V. Rapp (Atlanta, GA)
C09D183/08B05D1/185B05D5/00C04B41/00C04B41/009C04B41/4927C04B41/84Y10T428/23986Y10T428/31612Y10T428/31663
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Quick Facts
Patent No.
US 9,969,903
App. No.
14/606,544
Granted
May 15, 2018
Kind
B2
Abstract

A stain-treated substrate comprising an extremely thin coating for stain protection. The stain-treated substrate includes substrate material and the extremely thin coating include a molecular layer of organosilane 3-(trimethoxysilyl) propyldimethyl octadecyl ammonium chloride covalently bonded to the surface of the substrate material. The substrate material can include a wide variety of materials including tile, ceramic, glass, stone and marble and can optionally be used in conjunction with a grout mixture including a diluted organosilane mixture.

Claims (15)

1. An apparatus comprising a substrate and a coating for stain protection, the apparatus comprising:

the substrate; and

the coating comprising a molecular layer of organosilane 3-(trimethoxysilyl) propyldimethyl octadecyl ammonium chloride wherein the coating is covalently bonded to the substrate, wherein the coating is created by:

preparing a diluted solution of organosilane 3-(trimethoxysilyl) propyldimethyl octadecyl ammonium chloride in a concentration range of between 0.72% and 3.6%;

heating and maintaining the substrate to an above-room temperature comprising a temperature of between 100 degrees Celsius and 120 degrees Celsius;

applying the water-diluted solution to the substrate;

curing the substrate and water-diluted solution until dry and polymerized at the above-room temperature; and

removing excess polymerized solution from the substrate.

2. The apparatus of claim 1 , wherein the substrate comprises one of porcelain, fiberglass, a composite material, cultured marble, a bath tub, a shower tub, a ceramic tile, a porcelain tile, marble, granite, slate, natural stone, vinyl, brick, wood, engineered stone, carpet, and a rug.

3. The apparatus of claim 1 , wherein preparing the diluted solution comprises preparing the water-diluted solution at a concentration of 1.44%.

4. The apparatus of claim 1 , wherein applying the diluted solution to the substrate comprises spraying the solution upon the substrate as an atomized mist.

5. The apparatus of claim 4 , wherein the atomized mist comprises an ideal drip size of less than 50 microns.

6. The apparatus of claim 4 , wherein the atomized mist comprises an ideal drip size of 20 microns.

7. The apparatus of claim 1 , wherein preparing the water-diluted solution comprises maintain a temperature of the water-diluted solution between 25 degrees Celsius and 50 degrees Celsius.

8. The apparatus of claim 1 , wherein preparing the water-diluted solution comprises maintain an ideal temperature of the water-diluted solution between 25 degrees Celsius and 30 degrees Celsius.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 9, 2024
From: CORNIA, SILVER
To: TILE MEDIA PROPERTIES, INC.
Reel/Frame 068850/0942 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 17, 2024
From: RAPP, CURT V.
To: TILE MEDIA PROPERTIES, INC.
Reel/Frame 068974/0592 →
RELEASE OF SECURITY INTEREST Recorded Oct 28, 2018
From: GIBRALTAR BUSINESS CAPITAL, LLC
To: TILE MEDIA PROPERTIES, INC.
Reel/Frame 047727/0047 →
SECURITY INTEREST Recorded Mar 24, 2015
From: TILE MEDIA PROPERTIES, INC.
To: GIBRALTAR BUSINESS CAPITAL, LLC
Reel/Frame 035244/0083 →
Continuity (2)
Provisional Application 61932657 · Jan 28, 2014
Related Publication 20150210889A1 · Jul 30, 2015