IP Library Granted Patent US 9,719,908
Granted Patent B1
US 9,719,908 · App. 14/625,287 · Granted Aug 1, 2017

Electrofracturing test system and method of determining material characteristics of electrofractured material samples

Inventors: Stephen J. Bauer (Albuquerque, NM); Steven F. Glover (Albuquerque, NM); Tom Pfeifle (Albuquerque, NM); Jiann-Cherng Su (Albuquerque, NM); Kenneth Martin Williamson (Albuquerque, NM); Scott Thomas Broome (Santa Fe, NM); William Payton Gardner (Albuquerque, NM); Gary Pena (Albuquerque, NM)
Assignee: Sandia Corporation
G01N15/082G01N1/28G01N2001/1062
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Quick Facts
Patent No.
US 9,719,908
App. No.
14/625,287
Granted
Aug 1, 2017
Kind
B1
Abstract

A device for electrofracturing a material sample and analyzing the material sample is disclosed. The device simulates an in situ electrofracturing environment so as to obtain electrofractured material characteristics representative of field applications while allowing permeability testing of the fractured sample under in situ conditions.

Claims (32)

1. A device for electrofracturing a material sample, comprising:

a pressure vessel comprising an internal cavity;

a pressurized fluid supply system fluidly coupled to the internal cavity;

a material sample disposed within the internal cavity;

a voltage source electrically coupled to the material sample to provide a voltage pulse across the material sample; and

a gas measurement system fluidly coupled to the material sample;

wherein the voltage source provides a pulse of between 150 kv and 1 MV.

2. The device of claim 1 , wherein the pressurized fluid system is capable of pressurizing the internal cavity up to 20,000 psi.

3. The device of claim 1 , wherein the voltage source provides a pulse of 1 MV.

4. The device of claim 1 , wherein the voltage source provides a pulse of 200 kV.

5. The device of claim 1 , wherein the voltage source is capable of providing a pulse having a pulse width of between 100 picoseconds (ps) and 1 day.

6. The device of claim 1 , wherein the gas measurement system comprises a mass spectrometer.

7. The device of claim 1 , wherein the gas measurement system comprises a flow meter.

8. The device plate of claim 1 , wherein the material sample is shale.

9. The device of claim 1 , wherein the material sample is disposed with a test assembly disposed within the internal cavity, the test assembly comprising:

a first nonconductive end cap on a first surface of the material sample;

a second nonconductive end cap on a second surface of the material sample opposite the first surface;

a first and second conductors passing through the first and second nonconductive end caps, respectively, and contacting the material sample; and

a jacketing material sealing the material sample between the first and second nonconductive end caps.

10. A method of electrofracturing a material sample, comprising:

providing a material sample;

subjecting the material sample to an external pressure;

subjecting the material sample to a voltage potential;

flowing a test fluid across the material sample; and

measuring the amount of test gas that flows from the material sample;

wherein the voltage potential is between 150 kv and 1 MV.

11. The method of claim 10 , further comprising:

determining the permeability of the material sample.

12. The method of claim 10 , wherein the external pressure is between 2,000 psi and 20,000 psi.

13. The method of claim 10 , wherein the voltage potential is capable of fracturing the material sample.

14. The method of claim 10 , wherein the voltage potential is pulsed two or more times and the time between pulses is 100 μs to 1 day.

15. The method of claim 10 , wherein the voltage potential has a pulse width of between 100 picoseconds (ps) and 1 day.

Assignments (3)
CHANGE OF NAME Recorded Aug 3, 2017
From: SANDIA CORPORATION
To: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
Reel/Frame 043431/0734 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 7, 2016
From: BAUER, STEPHEN J.; GLOVER, STEVEN F.; PFEIFLE, TOM; SU, JIANN-CHERNG; WILLIAMSON, KENNETH MARTIN; BROOME, SCOTT THOMAS; GARDNER, WILLIAM PAYTON; PENA, GARY
To: SANDIA CORPORATION
Reel/Frame 039097/0446 →
CONFIRMATORY LICENSE Recorded May 18, 2016
From: SANDIA CORPORATION
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 038742/0477 →
Continuity (1)
Provisional Application 61941258 · Feb 18, 2014