IP Library Granted Patent US 9,816,952
Granted Patent B2
US 9,816,952 · App. 14/632,201 · Granted Nov 14, 2017

Method and apparatus for implementing material thermal property measurement by flash thermal imaging

Inventor: Jiangang Sun (Westmont, IL)
Assignee: UChicago Argonne, LLC
G01N25/18
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Quick Facts
Patent No.
US 9,816,952
App. No.
14/632,201
Granted
Nov 14, 2017
Kind
B2
Abstract

A method and apparatus are provided for implementing measurement of material thermal properties including measurement of thermal effusivity of a coating and/or film or a bulk material of uniform property. The test apparatus includes an infrared camera, a data acquisition and processing computer coupled to the infrared camera for acquiring and processing thermal image data, a flash lamp providing an input of heat onto the surface of a two-layer sample with an enhanced optical filter covering the flash lamp attenuating an entire infrared wavelength range with a series of thermal images is taken of the surface of the two-layer sample.

Claims (219)

1. A method for implementing measurement of material thermal properties including measurement of thermal effusivity of a coating and/or film or a bulk material of uniform property comprising:

providing an infrared camera,

providing a data acquisition and processing computer coupled to the infrared camera for acquiring and processing thermal image data,

providing a flash lamp providing an input of heat onto the surface of a two-layer sample;

providing an optical filter covering the flash lamp for attenuating an entire infrared wavelength range of thermal images taken of the surface of a sample, providing said optical filter including a pair of glass plates enclosing a water layer; and

performing a measurement solution to determine material thermal properties including thermal effusivity of the sample.

2. The method as recited in claim 1 , includes providing two-layer sample, and measuring thermal effusivity of each of the two layers without requiring other material information.

3. The method as recited in claim 1 , wherein the measurement solution to determine material thermal properties including thermal effusivity of the sample is represented by:

T

f

(

t

)

=

Q

·

f

1

(

e

1

2

t

)

·

f

3

(

e

1

e

2

,

α

1

L

1

2

,

t

)

,

(

1

)

T

f

(

t

)

=

Q

ρ

1

c

1

L

1

+

ρ

2

c

2

L

2

·

f

4

(

e

1

e

2

,

α

1

L

1

2

,

α

2

L

2

2

,

t

)

,

(

2

)

where T ƒ (t) represents a front surface temperature, where t is time and Q is the total amount of absorbed energy (heat) on surface for the two-layer sample of materials of uniform properties with an instantaneous heat impulse for the cases of a semi-infinite and a finite substrate thickness material, respectively; where L represents sample thickness, e represents thermal effusivity and ρc represents heat capacity; where the subscripts 1 and 2 denote the first-layer or shallow layer material and a second-layer or deep layer material, respectively.

4. The method as recited in claim 1 , wherein performing a measurement solution to determines material thermal properties including thermal effusivity of the sample includes providing a measurement accuracy of <2% absolute errors.

5. The method as recited in claim 1 , wherein performing a measurement solution to determine material thermal properties including thermal effusivity of the sample includes measuring coating and/or film thermal effusivity with known substrate effusivity.

6. The method as recited in claim 1 , wherein performing a measurement solution to determines material thermal properties including thermal effusivity of the sample includes measuring thermal diffusivity of a bulk plate material with known plate thickness.

7. A method for implementing measurement of material thermal properties including measurement of thermal effusivity of a coating and/or film or a bulk material of uniform property comprising:

providing an infrared camera,

providing a data acquisition and processing computer coupled to the infrared camera for acquiring and processing thermal image data,

providing a flash lamp providing an input of heat onto the surface of a two-layer sample;

providing an optical filter covering the flash lamp for attenuating an entire infrared wavelength range of thermal images taken of the surface of a sample; and

performing a measurement solution to determine material thermal properties including thermal effusivity of the sample includes measuring thermal effusivity of a bulk material by bonding a calibrated film on a material surface of the bulk material.

8. A system for implementing measurement of material thermal properties including measurement of thermal effusivity of a coating and/or film or a bulk material of uniform property comprising:

an infrared camera,

a data acquisition and processing computer coupled to the infrared camera for acquiring and processing thermal image data,

a flash lamp providing an input of heat onto the surface of a two-layer sample;

an optical filter covering the flash lamp for attenuating an entire infrared wavelength range of thermal images taken of the surface of a sample, said optical filter including a pair of glass plates enclosing a water layer; and

said data acquisition and processing computer performing a measurement solution to determine material thermal properties including thermal effusivity of the sample.

9. The system as recited in claim 8 , wherein the sample includes a two-layer sample, and thermal effusivity of each of the two layers is measured without requiring other material information.

10. The system as recited in claim 9 , wherein the measurement solution to determine material thermal properties including thermal effusivity of the sample is represented by:

T

f

(

t

)

=

Q

·

f

1

(

e

1

2

t

)

·

f

3

(

e

1

e

2

,

α

1

L

1

2

,

t

)

,

(

1

)

T

f

(

t

)

=

Q

ρ

1

c

1

L

1

+

ρ

2

c

2

L

2

·

f

4

(

e

1

e

2

,

α

1

L

1

2

,

α

2

L

2

2

,

t

)

,

(

2

)

where T ƒ (t) represents a front surface temperature, where t is time and Q is the total amount of absorbed energy (heat) on surface for the two-layer sample of materials of uniform properties with an instantaneous heat impulse for the cases of a semi-infinite and a finite substrate thickness material, respectively; where L represents sample thickness, e represents thermal effusivity and ρc represents heat capacity; where the subscripts 1 and 2 denote the first-layer or shallow layer material and a second-layer or deep layer material, respectively.

11. The system as recited in claim 8 , wherein said data acquisition and processing computer performing a measurement solution to determine material thermal properties including thermal effusivity of the sample provides a measurement accuracy of <2% absolute errors.

12. The system as recited in claim 8 , wherein said data acquisition and processing computer performing a measurement solution to determine material thermal properties including thermal effusivity of the sample includes said data acquisition and processing computer measuring coating and/or film thermal effusivity with known substrate effusivity.

13. The system as recited in claim 8 , wherein said data acquisition and processing computer performing a measurement solution to determine material thermal properties including thermal effusivity of the sample includes said data acquisition and processing computer measuring thermal effusivity of a bulk material by bonding a calibrated film on a material surface of the bulk material.

14. The system as recited in claim 8 , wherein said data acquisition and processing computer performing a measurement solution to determine material thermal properties including thermal effusivity of the sample includes said data acquisition and processing computer measuring thermal diffusivity of a bulk plate material with known plate thickness.

Assignments (2)
CONFIRMATORY LICENSE Recorded Aug 11, 2015
From: UCHICAGO ARGONNE, LLC
To: ENERGY, UNITED STATES DEPARTMENT OF
Reel/Frame 036353/0431 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 11, 2015
From: SUN, JIANGANG
To: UCHICAGO ARGONNE, LLC
Reel/Frame 035140/0846 →
Continuity (1)
Related Publication 20160252399A1 · Sep 1, 2016