IP Library Granted Patent US 9,266,078
Granted Patent B2
US 9,266,078 · App. 14/641,662 · Granted Feb 23, 2016

Cloud mixer of minimizing agglomeration of particulates

Inventors: Scott Murray (Lansing, MI); Michael Knox (Lansing, MI)
B01F15/0254B01F3/12B01F3/1271B01F5/106B01F5/205B01F2003/125B01F2215/0032
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Quick Facts
Patent No.
US 9,266,078
App. No.
14/641,662
Granted
Feb 23, 2016
Kind
B2
Abstract

An apparatus and a method for dispersing particulate materials prone to agglomeration, in a liquid. Particulate materials are exposed to a liquid and put into that liquid to form a suspension or a dispersion in a controlled method thereby minimizing agglomerates. The method uses mechanical/hydro mixing that prevents the physical deterioration of the particulate material and inhibits agglomeration of the particles. In many cases, these materials may be nanomaterials. Almost all particulate materials, can be handled in this manner. This method has been found to be especially useful for preparing solutions of exfoliated graphene and certain drugs.

Claims (27)

1. A apparatus for dispersing a particulate material in a liquid, said apparatus comprising:

i. a hollow tubular chamber having an open top, an open bottom, and a side wall;

ii. said open top having surmounted therein, a feed tube entry component having a feed tube throat smaller in diameter than said open top of said hollow tubular chamber;

iii. a series of misting nozzles located through said side wall of said hollow tubular chamber to create a wet zone;

iv. a plurality of transfer lines for distribution of said liquid from,

v. a manifold to said nozzles;

vi. an output of a high pressure pump connected to said manifold, and the input from,

vii. a storage tank for said liquid;

viii. a drain funnel having an open bottom end and being attached to the open bottom of said hollow tubular chamber;

ix. a mixing chamber having an inlet port;

x. a chamber drain attached to said open bottom end of said drain funnel, said chamber drain surrounded by a cylindrical covering having an outside wall connecting to a holding tank;

xi. there being a support plate surrounding said cylindrical covering and attached thereto;

xii. a holding tank

xiii. a high volume pump, said holding tank being connected to said inlet port via said high volume pump.

2. An apparatus for dispersing a particulate material in a liquid, said apparatus comprising:

i. a hollow tubular chamber having an open top, an open bottom; and a side wall;

ii. said open top having surmounted therein, a feed tube entry component having a feed tube throat smaller in diameter than the open top of said hollow tubular chamber;

iii. a series of misting nozzles located through said site wall of the hollow tubular chamber to create a wet zone;

iv. a plurality of transfer lines for distribution of said liquid from,

v. a manifold to said misting nozzles;

vi. the output of a high pressure pump connected to said manifold and said input from,

vii. a storage tank for said liquid;

viii. a drain funnel having an open bottom end and being attached to the open bottom of said hollow tubular chamber;

ix. there being a support plate surrounding a cylindrical covering and attached thereto;

x. an eductor having an inlet pipe from said open bottom of said drain funnel, an inlet port, and an outlet port;

xi. a holding tank connected to said outlet port;

xii. a high volume pump, said holding tank being connected to said inlet port via said high volume pump.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 26, 2023
From: XGS HOLDINGS LLC (ON BEHALF OF XG SCIENCES, INC. PURSUANT TO THE UCC)
To: NANOXPLORE INC.
Reel/Frame 063446/0841 →
SECURITY INTEREST Recorded Apr 28, 2020
From: XG SCIENCES IP, LLC; XG SCIENCES, INC.
To: XGS COLLATERAL AGENT, LLC
Reel/Frame 052512/0860 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 22, 2018
From: MURRAY, SCOTT; KNOX, MICHAEL
To: XG SCIENCES, INC.
Reel/Frame 046660/0120 →
CORRECTIVE ASSIGNMENT TO CORRECT THE APPLICATION NO. 15155558 PREVIOUSLY RECORDED ON REEL 040639 FRAME 0592. ASSIGNOR(S) HEREBY CONFIRMS THE SECURITY INTEREST. Recorded Jan 18, 2017
From: XG SCIENCES IP, LLC; XG SCIENCES, INC.
To: THE DOW CHEMICAL COMPANY
Reel/Frame 041437/0504 →
SECURITY INTEREST Recorded Dec 16, 2016
From: XG SCIENCES IP, LLC; XG SCIENCES, INC.
To: THE DOW CHEMICAL COMPANY
Reel/Frame 040639/0592 →
Continuity (4)
Division 14215356 · Mar 17, 2014
Division 13610934 · Sep 12, 2012
Provisional Application 61573897 · Sep 14, 2011
Related Publication 20150174543A1 · Jun 25, 2015