IP Library Granted Patent US 10,173,206
Granted Patent B2
US 10,173,206 · App. 14/647,989 · Granted Jan 8, 2019

Modified Y-zeolite/ZSM-5 catalyst for increased propylene production

Inventors: Maria Margaret Ludvig (Seabrook, TX); Erja Paivi Helena Rautiainen (Leusden, NL); Albert Carel Pouwels (Amersfoort, NL)
Assignee: ALBEMARLE EUROPE SPRL
B01J29/80B01J29/061B01J29/084B01J29/40B01J35/023C07C4/06C10G11/05C10G11/18B01J29/90B01J35/0006B01J38/06B01J38/12B01J2029/062B01J2229/186B01J2229/42C07C2529/08C07C2529/40C07C2529/80C10G2400/20
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Quick Facts
Patent No.
US 10,173,206
App. No.
14/647,989
Granted
Jan 8, 2019
Kind
B2
Abstract

Provided is a Fluid Catalytic Cracking catalyst composition having increased propylene production with respect to other Fluid Catalytic Cracking catalysts (measured at constant conversion). The catalyst composition comprises a particulate which comprises (a) non-rare earth metal exchanged Y-zeolite in an amount in the range of about 5 to about 50 wt %, based upon the weight of the particulate; and (b) ZSM-5 zeolite in an amount in the range of about 2 to about 50 wt %, based upon the weight of the particulate.

Claims (22)

1. An FCC catalyst composition comprising a particulate, said particulate comprising

catalytic components (a) and (b), wherein component (a) comprises a non-rare earth metal exchanged Y-zeolite in an amount in the range of about 5 to about 50 wt %, based upon the weight of the particulate; and component (b) consists of ZSM-5 zeolite in an amount in the range of about 2 to about 50 wt %, based upon the weight of the particulate, wherein (a) and (b) are present in the same particle, wherein the Y-zeolite:ZSM-5 weight ratio is in the range of about 1:2.5 to about 1:6, and wherein the non-rare earth metal is magnesium, calcium, or strontium.

2. An FCC catalyst composition as in claim 1 wherein said non-rare earth metal comprises magnesium.

3. An FCC catalyst composition as in claim 1 wherein the FCC catalyst composition comprises a total non-rare earth metal content in the range of about 0.2 to about 3 wt % percent.

4. An FCC catalyst composition as in claim 2 wherein said FCC catalyst composition is prepared by a process comprising magnesium/hydrogen ion exchange with an unexchanged Y-zeolite.

5. A process for producing propylene from a hydrocarbon feedstock, said process comprising the steps of:

a) providing an FCC catalyst composition comprising:

a particulate, said particulate comprising catalytic components (a) and (b), wherein component (a) comprises a non-rare earth metal exchanged Y-zeolite in an amount in the range of about 5 to about 50 wt %, based upon the weight of the particulate; and component (b) consists of ZSM-5 zeolite in an amount in the range of about 2 to about 50 wt %, based upon the weight of the particulate, wherein (a) and (b) are present in the same particle, and wherein the Y-zeolite:ZSM-5 weight ratio is in the range of about 1:2.5 to about 1:6, and wherein the non-rare earth metal is magnesium, calcium, or strontium;

b) contacting the FCC particulate catalyst composition with the hydrocarbon feedstock, at one or more temperatures in the range of about 400 to about 650° C., with a dwell time in the range of about 0.5 to about 12 seconds.

6. A process as in claim 5 wherein contacting in b) takes place in a fluidized bed reactor.

7. A process as in claim 5 wherein the non-rare earth metal comprises magnesium.

8. A process as in claim 5 , wherein the resulting yield of propylene is greater, as compared with the resulting yield of propylene of the same process but modified to use an unexchanged Y-zeolite instead of said non-rare earth metal exchanged Y-zeolite on a weight-for-weight basis, the comparison being made at a feedstock conversion in the range of about 40 to about 90 weight percent conversion.

9. A process as in claim 5 wherein the ZSM-5 is in the range of about 5 to about 35 wt %, based upon the weight of the particles in which ZSM-5 and non-rare earth metal exchanged Y-zeolite are present.

10. A process as in claim 5 wherein the non-rare earth metal exchanged Y-zeolite is in the range of about 5 to about 30 wt %, based upon the weight of the particles in which ZSM-5 and non-rare earth metal exchanged Y-zeolite are present.

11. A process as in claim 5 , wherein the FCC catalyst composition further comprises an amount of alumina in the range of 0 to about 35 wt %, an amount of silica sol in the range of 0 to about 25 wt %, and the remaining balance being clay.

12. An FCC catalyst composition as in claim 2 wherein the magnesium is in an amount measured as magnesium oxide in the range of about 0.25 to about 3.0 wt % percent.

13. An FCC catalyst composition as in claim 1 wherein the Y zeolite is an ultrastabilized faujasite Y zeolite.

14. A process as in claim 5 wherein:

the Y zeolite is an ultrastabilized faujasite Y zeolite;

and/or

propylene is formed with a conversion efficiency in the range of about 4 to about 20 wt %, based upon the weight of the hydrocarbon feedstock.

15. A process as in claim 7 wherein the FCC catalyst composition comprises a magnesium salt in an amount measured as magnesium oxide in the range of from 0.25 to 3.0 wt %.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 8, 2024
From: ALBEMARLE EUROPE SRL
To: KETJEN NETHERLANDS B.V.
Reel/Frame 067035/0015 →
CHANGE OF NAME Recorded Apr 8, 2024
From: ALBEMARLE EUROPE SPRL
To: ALBEMARLE EUROPE SRL
Reel/Frame 067040/0477 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 4, 2015
From: LUDVIG, MARIA M.; RAUTIAINEN, ERJA PAIVI HELENA; POUWELS, ALBERT CAREL
To: ALBEMARLE EUROPE SPRL
Reel/Frame 036245/0079 →
Continuity (2)
Provisional Application 61740948 · Dec 21, 2012
Related Publication 20150298107A1 · Oct 22, 2015