IP Library Granted Patent US 9,522,115
Granted Patent B2
US 9,522,115 · App. 14/733,659 · Granted Dec 20, 2016

Pharmaceutical formulation containing gelling agent

Inventors: Curtis Wright (Rockport, MA); Benjamin Oshlack (Boca Raton, FL); Christopher Breder (Bethesda, MD)
Assignees: Purdue Pharma L.P.; The P.F. Laboratories, Inc.; Purdue Pharmaceuticals L.P.
A61K9/1641A61J3/10A61K9/0002A61K9/006A61K9/0053A61K9/06A61K9/08A61K9/1635A61K9/1652A61K9/205A61K9/2009A61K9/2013A61K9/2018A61K9/2027A61K9/2031A61K9/2054A61K9/2095A61K9/28A61K9/284A61K9/2806A61K9/2846A61K9/2866A61K9/2893A61K9/485A61K9/4808A61K9/4833A61K9/4858A61K9/4866A61K9/4891A61K9/5047A61K9/5078A61K9/5089A61K9/70A61K31/137A61K31/167A61K31/192A61K31/439A61K31/4458A61K31/48A61K31/485A61K45/06A61K47/08A61K47/10A61K47/12A61K47/14A61K47/26A61K47/32A61K47/34A61K47/36A61K47/38
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Quick Facts
Patent No.
US 9,522,115
App. No.
14/733,659
Granted
Dec 20, 2016
Kind
B2
Abstract

Disclosed in certain embodiments is a controlled release oral dosage form comprising a therapeutically effective amount of a drug susceptible to abuse together with one or more pharmaceutically acceptable excipients; the dosage form further including a gelling agent in an effective amount to impart a viscosity unsuitable for administration selected from the group consisting of parenteral and nasal administration to a solubilized mixture formed when the dosage form is crushed and mixed with from about 0.5 to about 10 ml of an aqueous liquid; the dosage form providing a therapeutic effect for at least about 12 hours when orally administered to a human patient.

Claims (25)

1. A controlled release oral dosage form comprising:

a matrix comprising a mixture of (i) hydrocodone or a pharmaceutically acceptable salt thereof; and

(ii) a gelling agent comprising polyethylene oxide, the gelling agent is in an effective amount to impart a viscosity of about 10 cP or more when the dosage form is subjected to tampering by dissolution in from about 0.5 ml to about 10 ml of an aqueous liquid;

a coating comprising a hydrophobic material, the coating applied on the matrix and comprising one or more passageways through the coating;

the dosage form providing a therapeutic effect for about 12 hours or longer when orally administered to a human patient.

2. The controlled release oral dosage form of claim 1 , comprising from about 750 ng to about 750 mg hydrocodone or a pharmaceutically acceptable salt thereof.

3. The controlled release oral dosage form of claim 1 , comprising from about 2 mg to about 50 mg hydrocodone or a pharmaceutically acceptable salt thereof.

4. The controlled release oral dosage form of claim 1 , wherein the hydrocodone or pharmaceutically acceptable salt thereof is hydrocodone bitartrate.

5. The controlled release oral dosage form of claim 1 , wherein the aqueous liquid is water.

6. The controlled release oral dosage form of claim 1 , wherein the viscosity is imparted when the dosage form is subjected to tampering by dissolution in about 1 ml to about 3 ml of aqueous liquid.

7. The controlled release oral dosage form of claim 1 , wherein the viscosity is imparted when the dosage form is subjected to tampering by crushing and dissolution in the aqueous liquid.

8. The controlled release oral dosage form of claim 1 , wherein the viscosity is imparted when the dosage form is subjected to tampering by dissolution in the aqueous liquid at ambient temperature.

9. The controlled release oral dosage form of claim 1 , wherein the viscosity is imparted when the dosage form is subjected to tampering by dissolution in the aqueous liquid with heating greater than 45° C.

10. The controlled release oral dosage form of 1 , wherein the hydrophobic material comprises a cellulosic polymer.

11. The controlled release oral dosage form of claim 1 , wherein the cellulosic polymer comprises ethylcellulose.

12. The controlled release dosage form of claim 1 , wherein the polyethylene oxide has a weight average molecular weight from about 100,000 daltons to about 1,000,000 daltons.

13. The controlled release dosage form of claim 1 , wherein the polyethylene oxide has a weight average molecular weight from about 1,000,000 daltons to about 10,000,000 daltons.

14. The controlled release dosage form of claim 1 , wherein the ratio of gelling agent to hydrocodone or pharmaceutically acceptable salt thereof is from about 40:1 to about 1:40.

15. The controlled release dosage form of claim 1 , wherein the ratio of gelling agent to hydrocodone or pharmaceutically acceptable salt thereof is from about 1:1 to about 30:1.

16. A controlled release oral dosage form comprising:

a matrix comprising a mixture of (i) from about 750 ng to about 750 mg hydrocodone or a pharmaceutically acceptable salt thereof; and

(ii) a gelling agent comprising polyethylene oxide, the gelling agent is in an effective amount to impart a viscosity of at least 10 cP when the dosage form is subjected to tampering by dissolution in from about 0.5 ml to about 10 ml of an aqueous liquid;

the dosage form having a ratio of gelling agent to hydrocodone or pharmaceutically acceptable salt thereof from about 40:1 to about 1:40;

a coating comprising ethylcellulose, the coating applied on the matrix and comprising one or more passageways through the coating;

the dosage form providing a therapeutic effect for about 12 hours or longer when orally administered to a human patient.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 17, 2019
From: THE P.F. LABORATORIES, INC.; PURDUE PHARMA TECHNOLOGIES, INC.
To: PURDUE PHARMA L.P.
Reel/Frame 048932/0651 →
Continuity (8)
Continuation 14730017 · Jun 3, 2015
Continuation 14243580 · Apr 2, 2014
Continuation 13726324 · Dec 24, 2012
Continuation 13349449 · Jan 12, 2012
Continuation 12653115 · Dec 8, 2009
Continuation 10214412 · Aug 6, 2002
Provisional Application 60310534 · Aug 6, 2001
Related Publication 20150265607A1 · Sep 24, 2015