IP Library › Granted Patent US 9,663,376
Granted Patent B2
US 9,663,376 · App. 14/734,400 · Granted May 30, 2017

Xerogel production method

Inventors: Kazuma Oikawa (Osaka, JP); Shigeaki Sakatani (Osaka, JP); Kei Toyota (Osaka, JP)
Assignee: PANASONIC INTELLECTUAL PROPERTY MANAGEMENT CO., LTD.
C01B33/16B01J13/0091
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Quick Facts
Patent No.
US 9,663,376
App. No.
14/734,400
Granted
May 30, 2017
Kind
B2
Abstract

A xerogel production method includes: adding, to water glass, a basic silicic acid solution having a sol with a particle size between a particle size of the water glass and a particle size of colloidal silica, to acidify and solate the water glass, and polycondensing the solated water glass at 20° C. to 90° C., to obtain a hydrogel; growing the hydrogel by leaving the hydrogel for a certain time period at a constant temperature; hydrophobizing the hydrogel; and drying the hydrophobized hydrogel.

Claims (19)

1. A xerogel production method comprising:

adding, to water glass, a basic silicic acid solution having a sol with a particle size between a particle size of the water glass and 30 nm, to acidify and solate the water glass, and polycondensing the solated water glass at 20° C. to 90° C., to obtain a hydrogel;

growing the hydrogel by leaving the hydrogel for a certain time period at a constant temperature;

hydrophobizing the hydrogel; and

drying the hydrophobized hydrogel.

2. The xerogel production method according to claim 1 ,

wherein the water glass is acidified to a pH ranging from 5.0 to 8.0.

3. The xerogel production method according to claim 1 ,

wherein the particle size of the sol ranges from 1 nm to 30 nm.

4. The xerogel production method according to claim 1 ,

wherein the basic silicic acid solution has a concentration of silicic acid ranging from 13 wt % to 20 wt %.

5. The xerogel production method according to claim 1 ,

wherein the basic silicic acid solution has a pH ranging from 8.0 to 11.0.

6. The xerogel production method according to claim 1 ,

wherein when the hydrogel is hydrophobized, at least one of hexamethyldisiloxane, octamethyltrisiloxane, decamethyltetrasiloxane, trimethylchlorosilane, hexamethyldisilazane, or methyltrimethoxysilane is used.

7. The xerogel production method according to claim 1 ,

wherein when the hydrogel is hydrophobized, at least one of methanol, ethanol, 2-propanol, tert-butanol, or ethylene glycol is used.

8. The xerogel production method according to claim 1 ,

wherein when the hydrophobized hydrogel is dried, the hydrophobized hydrogel is dried at 100° C. to 200° C.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 3, 2015
From: OIKAWA, KAZUMA; SAKATANI, SHIGEAKI; TOYOTA, KEI
To: PANASONIC INTELLECTUAL PROPERTY MANAGEMENT CO., LTD.
Reel/Frame 036234/0134 →
Priority Claims (1)
JP 2014-124008 · Jun 17, 2014 · national
Continuity (1)
Related Publication 20150360961A1 · Dec 17, 2015