IP Library Granted Patent US 9,981,202
Granted Patent B2
US 9,981,202 · App. 14/774,965 · Granted May 29, 2018

Rotary evaporator with mechanical foam breaker

Inventors: Joachim Carl (Stein, DE); Patrick Nico Jost (Steinheim am Albuch, DE)
Assignee: HANS HEIDOLPH GMBH
B01D3/085B01B1/02B01D1/222B01D1/223B01D3/02B01D19/02
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Quick Facts
Patent No.
US 9,981,202
App. No.
14/774,965
Granted
May 29, 2018
Kind
B2
Abstract

A rotary evaporator for the vacuum distillation of a liquid is disclosed. The rotary evaporator contains an evaporator flask and a vapor feeder with an interior volume connected downstream of the evaporator flask. The rotary evaporator further contains a rotor that has a mechanical foam breaker within the interior volume of the vapor feeder. Further, a cooler is connected downstream of the vapor feeder.

Claims (15)

1. A rotary evaporator for the vacuum distillation of a liquid comprising an evaporator flask, a vapor feeder connected downstream of the evaporator flask and having an interior volume, a rotor having a mechanical foam breaker being disposed in the interior volume of the vapor feeder, and a cooler connected downstream of the vapor feeder.

2. The rotary evaporator in accordance with claim 1 , wherein the rotor is contactlessly driven by a drive device arranged outside of the vapor feeder or by a battery formed integrally with the rotor.

3. The rotary evaporator in accordance with claim 1 , wherein a drive of the rotor takes place electromagnetically by means of a stator which is arranged outside of the vapor feeder.

4. The rotary evaporator in accordance with claim 3 , wherein the stator comprises a plurality of coils which are arranged around a circumference of a coil body and which are controlled such that a magnetic rotary field is generated and/or such that the stator has a plurality of magnetic poles arranged in the peripheral direction.

5. The rotary evaporator in accordance with claim 1 , wherein the rotor comprises an even number of permanent magnet poles arranged around a circumference of a coil body or a short-circuit ring.

6. The rotary evaporator in accordance with claims 3 , wherein the stator comprises a plurality of coils arranged around a circumference of a coil body and having radially or tangentially oriented axes.

7. The rotary evaporator in accordance with claim 1 , wherein the vapor feeder has an insertion point for the rotor at which two mutually separate vapor feeder sections of the vapor feeder are connected to one another in a hermetically sealed and releasable manner.

8. The rotary evaporator in accordance with claim 7 , wherein a spacing is formed between the two vapor feeder sections, with the spacing being bridged by an insertion piece.

9. The rotary evaporator in accordance with claim 1 , further comprising a support device having a bearing for the rotor.

10. The rotary evaporator in accordance with claim 9 , wherein the support device is supported at inner walls of the vapor feeder or is formed integrally with an insertion piece.

11. The rotary evaporator in accordance with claim 9 , wherein the support device comprises a plurality of webs extending radially and arranged around a circumference of a coil body of the vapor feeder or comprises a funnel section connected upstream of the rotor and tapering in the direction of flow of the vapor.

12. The rotary evaporator in accordance with claim 1 , wherein the mechanical foam breaker is configured as a foam centrifuge or as a stirring member.

13. The rotary evaporator in accordance with claim 1 , wherein the vapor feeder has an expansion vessel and the rotor is arranged in the interior of the expansion vessel.

14. The rotary evaporator in accordance with claim 1 , further comprising a foam sensor arranged within the vapor feeder for the detection of foam present in the vapor feeder.

15. The rotary evaporator in accordance with claim 14 , wherein the rotary evaporator is configured to set the rotor into rotation automatically when it is detected by the foam sensor that foam present in the vapor feeder exceeds a predefined measure.

Assignments (2)
CHANGE OF NAME Recorded Mar 23, 2017
From: HANS HEIDOLPH GMBH & CO. KG
To: HANS HEIDOLPH GMBH
Reel/Frame 042076/0506 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 10, 2015
From: CARL, JOACHIM; JOST, PATRICK NICO
To: HANS HEIDOLPH GMBH & CO. KG
Reel/Frame 037262/0799 →
Priority Claims (1)
DE 10 2013 204 459 · Mar 14, 2013 · national
Continuity (1)
Related Publication 20160136539A1 · May 19, 2016