IP Library Granted Patent US 10,017,813
Granted Patent B2
US 10,017,813 · App. 14/781,453 · Granted Jul 10, 2018

Differentiation of macromolecules and analysis of their internal content in solid-state nanopore devices

Inventors: Marija Drndic (Philadelphia, PA); Kimberly Elizabeth Venta (Philadelphia, PA); Gabriel Shemer (Jenkintown, PA)
Assignee: The Trustees of the University of Pennsylvania
C12Q1/6869G01N27/44743G01N27/44791G01N33/48721
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Quick Facts
Patent No.
US 10,017,813
App. No.
14/781,453
Granted
Jul 10, 2018
Kind
B2
Abstract

Provided are solid-state nanopore platforms for fast, electronic, label-free and high-resolution analysis of biomolecules.

Claims (33)

1. A system, comprising:

a membrane having a first region that defines a thickness in the range of from about 0.1 nm to about 10 nm;

a pore formed in the first region of the membrane, the pore defining a cross-sectional dimension in the range of from about 0.1 nm to about 5 nm;

a voltage source configured to, during operation, apply a voltage in the range of from about 0.1 V to about 2 V across the pore; and

the system further comprising an amplifier in electronic connection with the pore, the amplifier being configured such that the system is capable of operating at up to about 100 MHz.

2. The system of claim 1 , further comprising a device adapted to maintain the temperature in the environment proximate to the pore at less than about 25 deg. C.

3. The system of claim 1 , further comprising a species that is more hydrophilic than the membrane, the species surmounting at least a portion of the membrane.

4. The system of claim 1 , wherein at least a portion of the membrane defines a thickness in the range of from about 0.1 nm to about 100 nm.

5. The system of claim 1 , further comprising an amplifier in electronic connection with the pore, the amplifier being configured such that the system has a capacitance of less than about 50 pico-Farad.

6. The system of claim 1 , further comprising an amplifier in electronic connection with the pore, the amplifier being configured such that the system is capable of resolving the internal structure of a biomolecule.

7. The system of claim 1 , wherein the amplifier comprises a filter configured to operate at between about 100 kHz and about 100 MHz.

8. A system, comprising:

a membrane having a first region that defines a thickness in the range of from about 0.1 nm to about 10 nm;

a pore formed in the first region of the membrane, the pore defining a cross-sectional dimension in the range of from about 0.1 nm to about 5 nm; and

a voltage source configured to, during operation, apply a voltage in the range of from about 0.1 V to about 2 V across the pore,

the system further comprising an amplifier in electronic connection with the pore, the amplifier being configured such that the system is capable of resolving signals down to about 10 nano-second temporal resolution.

9. The system of claim 8 , further comprising a device adapted to maintain the temperature in the environment proximate to the pore at less than about 25 deg. C.

10. The system of claim 8 , further comprising a species that is more hydrophilic than the membrane, the species surmounting at least a portion of the membrane.

11. The system of claim 8 , wherein at least a portion of the membrane defines a thickness in the range of from about 0.1 nm to about 100 nm.

12. The system of claim 8 , further comprising an amplifier in electronic connection with the pore, the amplifier being configured such that the system is capable of resolving the internal structure of a biomolecule.

13. The system of claim 8 , wherein the amplifier comprises a filter configured to operate at between about 100 kHz and about 100 MHz.

14. The system of claim 8 , further comprising an amplifier in electronic connection with the pore, the amplifier being configured such that the system has a capacitance of less than about 50 pico-Farad.

15. A system, comprising:

a membrane having a first region that defines a thickness in the range of from about 0.1 nm to about 10 nm;

a pore formed in the first region of the membrane, the pore defining a cross-sectional dimension in the range of from about 0.1 nm to about 5 nm; and

a voltage source configured to, during operation, apply a voltage in the range of from about 0.1 V to about 2 V across the pore,

the system further comprising an amplifier in electronic connection with the pore, the amplifier being configured such that the system is capable of resolving a current difference across the pore of about 0.1 pA.

16. The system of claim 12 , further comprising a device adapted to maintain the temperature in the environment proximate to the pore at less than about 25 deg. C.

17. The system of claim 15 , further comprising a species that is more hydrophilic than the membrane, the species surmounting at least a portion of the membrane.

18. The system of claim 15 , wherein at least a portion of the membrane defines a thickness in the range of from about 0.1 nm to about 100 nm.

19. The system of claim 15 , further comprising an amplifier in electronic connection with the pore, the amplifier being configured such that the system is capable of resolving the internal structure of a biomolecule.

20. The system of claim 15 , wherein the amplifier comprises a filter configured to operate at between about 100 kHz and about 100 MHz.

21. The system of claim 15 , further comprising an amplifier in electronic connection with the pore, the amplifier being configured such that the system has a capacitance of less than about 50 pico-Farad.

Assignments (2)
CONFIRMATORY LICENSE Recorded Mar 3, 2016
From: UNIVERSITY OF PENNSYLVANIA
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 037981/0061 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 30, 2015
From: DRNDIC, MARIJA; VENTA, KIMBERLY ELIZABETH; SHEMER, GABRIEL
To: THE TRUSTEES OF THE UNIVERSITY OF PENNSYLVANIA
Reel/Frame 036694/0460 →
Continuity (2)
Provisional Application 61808459 · Apr 4, 2013
Related Publication 20160053313A1 · Feb 25, 2016