IP Library Granted Patent US 10,092,654
Granted Patent B2
US 10,092,654 · App. 14/795,569 · Granted Oct 9, 2018

Coacervate micro and/or nano droplets and hydrogels

Inventors: Eben Alsberg (Cleveland, OH); Oju Jeon (Cleveland, OH); David Wolfson (Cleveland, OH)
Assignee: Case Western Reserve University
A61K47/36A61K9/00A61K31/727A61K35/28A61K38/1875A61K47/00A61K47/42A61L27/26A61L27/38A61L27/3834A61L27/52A61L27/54C12N5/0662A61L2300/414A61L2430/02C12N2533/54C12N2533/74C12N2537/00C12N2537/10
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Quick Facts
Patent No.
US 10,092,654
App. No.
14/795,569
Granted
Oct 9, 2018
Kind
B2
Abstract

A composition includes a plurality of coacervate micro and/or nanodroplets of oxidized alginate and a methacrylated gelatin.

Claims (21)

1. A composition comprising:

a plurality of coacervate microdroplets and/or nanodroplets that include an oxidized alginate and a methacrylated gelatin, and at least one bioactive agent incorporated in the plurality of coacervate microdroplets and/or nanodroplets, wherein the oxidized alginate has an oxidation percentage of at least 10% of uronic acid units of alginate and the methacrylated gelatin has a methacrylation percentage of about 10% to about 99% of amine groups of gelatin.

2. The composition of claim 1 , wherein the oxidized alginate has an oxidation percentage up to 50% of uronic acid units of alginate.

3. The composition of claim 2 , wherein the oxidized alginate is methacrylated and has a methacrylation percentage up to 45% of alginate carboxylic acid reactive groups.

4. The composition of claim 1 , further comprising a cytocompatible hydrogel matrix in which the coacervate microdroplets and/or nanodroplets are suspended.

5. The composition of claim 4 , wherein the hydrogel matrix is cross-linked.

6. The composition of claim 4 , wherein the hydrogel matrix includes a plurality of cells and the plurality of coacervate microdroplets and/or nanodroplets provide controlled release of the bioactive agent to the plurality of cells.

7. The composition of claim 6 , wherein the bioactive agent comprises BMP-2 and the cells comprise progenitor cells.

8. The composition of claim 4 , wherein the hydrogel further includes photocrosslinkable heparin.

9. A coacervate hydrogel comprising:

crosslinked oxidized alginate and methacrylated gelatin that form a hydrogel matrix and a plurality of coacervate microdroplets and/or nanodroplets suspended in the matrix, wherein the oxidized alginate has an oxidation percentage of at least 10% of uronic acid units of alginate and the methacrylated gelatin has a methacrylation percentage of about 10% to about 99% of amine groups of gelatin.

10. The hydrogel of claim 9 , wherein at least one bioactive agent is incorporated in the coacervate microdroplets and/or nanodroplets and/or matrix.

11. The hydrogel of claim 9 , wherein the oxidized alginate has an oxidation percentage up to 50% of uronic acid units of alginate.

12. The hydrogel of claim 10 , wherein the oxidized alginate is methacrylated and has a methacrylation percentage up to 45% of alginate carboxylic acid reactive groups.

13. The hydrogel of claim 10 , wherein the hydrogel matrix includes a plurality of cells and the plurality of coacervate microdroplets and/or nanodroplets provide controlled release of the bioactive agent to the plurality of cells.

14. The hydrogel of claim 13 , wherein the bioactive agent comprises BMP-2 and the cells comprise hMSCs.

15. A coacervate hydrogel comprising:

a crosslinked oxidized methacrylated alginate and a methacrylated gelatin that form a hydrogel matrix and a plurality of coacervate microdroplets and/or nanodroplets, wherein the oxidized methacrylated alginate has an oxidation percentage of 10% up to 50% of uronic acid units and a methacrylation percentage up to 45% of carboxylic acid reactive groups of alginate, the methacrylated gelatin has a methacrylation percentage of at least about 10% to about 99% of amine groups of alginate.

16. The hydrogel of claim 15 , further comprising at least one bioactive agent incorporated in the microdroplets and/or nanodroplets and/or matrix.

17. The hydrogel of claim 16 , wherein the hydrogel matrix includes a plurality of cells and the plurality of coacervate microdroplets and/or nanodroplets provide controlled release of the bioactive agent to the plurality of cells.

18. The hydrogel of claim 17 , wherein the bioactive agent comprises BMP-2 and the cells comprise hMSCs.

Assignments (2)
CONFIRMATORY LICENSE Recorded Jul 8, 2016
From: CASE WESTERN RESERVE UNIVERSITY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 039289/0456 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 15, 2015
From: ALSBERG, EBEN; JEON, OJU; WOLFSON, DAVID
To: CASE WESTERN RESERVE UNIVERSITY
Reel/Frame 036802/0553 →
Continuity (2)
Provisional Application 62022343 · Jul 9, 2014
Related Publication 20160008475A1 · Jan 14, 2016