IP Library Granted Patent US 11,142,812
Granted Patent B2
US 11,142,812 · App. 14/801,836 · Granted Oct 12, 2021

Multicaloric MnNiSi alloys

Inventors: Tapas Samanta (Baton Rouge, LA); Shane Stadler (Baton Rouge, LA); Naushad Ali (Carbondale, IL)
C22C30/00H01F1/015C22C19/005C22C22/00
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Quick Facts
Patent No.
US 11,142,812
App. No.
14/801,836
Granted
Oct 12, 2021
Kind
B2
Abstract

A multicaloric alloy material combines two isostructural compounds, the first compound being MnNiSi and the second compound being either MnFeGe or CoFeGe, each such compound having extremely different magnetic and thermo-structural properties. The resulting alloy material (MnNiSi) 1-x (MnFeGe) x or (MnNiSi) 1-x (CoFeGe) x possesses extraordinary magnetocaloric and/or barocaloric properties with an acute sensitivity to applied pressure and no appreciable magnetic hysteresis losses.

Claims (22)

1. An alloy consisting of:

a first compound, said first compound comprising Mn 1±α Ni 1±β Si 1±γ , wherein α≤0.25, γ≤0.25, and γ≤0.25;

a second compound, said second compound isostructurally substituting the first compound, and said second compound comprising one of Fe 1±λ Mn 1±μ Ge 1±ν wherein λ≤0.25, μ≤0.25, and ν≤0.25 and Co 1±λ Fe 1±μ Ge 1±ν wherein λ≤0.25, μ≤0.25, and ν≤0.25;

where the ratio of the first compound to the second compound is 1-x to x; and

where when the second compound comprises Co 1±λ Fe 1±μ Ge 1±ν then x is from 0.30 to 0.50, and when the second compound is Fe 1±λ Mn 1±μ Ge 1±ν then x is from 0.40 to 0.65.

2. An alloy consisting of:

a first compound, said first compound comprising Mn 1±α Ni 1±β Si 1±γ , wherein α≤0.25, β≤0.25, and γ≤0.25;

a second compound, said second compound isostructurally substituting the first compound, and said second compound comprising one of Fe 1±λ Mn 1±μ Ge 1±ν wherein λ≤0.25, μ≤0.25, and ν≤0.25 and Co 1±λ Fe 1±μ Ge 1±ν wherein λ≤0.25, μ≤0.25, and ν≤0.25;

where the ratio of the first compound to the second compound is 1-x to x; and

where when the second compound comprises Co 1±λ Fe 1±μ Ge 1±ν then x is from 0.30 to 0.50, and when the second compound is Fe 1±λ Mn 1±μ Ge 1±ν then x is from 0.40 to 0.65 and further comprising an element from the group consisting of B, C, N, P, S, As and H, the element from the group consisting of B, C, N, P, S, As and H comprising not more than 15% by mass of the alloy.

3. An alloy consisting of

a first compound, said first compound comprising Mn 1±α Ni 1±β Si 1±γ , wherein α≤0.25, β≤0.25, and γ≤0.25; and

a second compound, said second compound isostructurally substituting the first compound, and said second compound comprising Fe 1±λ Mn 1±μ Ge 1±ν , wherein λ≤0.25, μ≤0.25, and ν≤0.25.

4. An alloy consisting of

a first compound, said first compound comprising Mn 1±α Ni 1±β Si 1±γ , wherein α≤0.25, β≤0.25, and γ≤0.25; and

a second compound, said second compound isostructurally substituting the first compound, and said second compound comprising Fe 1±λ Mn 1±μ Ge 1±ν , wherein λ≤0.25, μ≤0.25, and ν≤0.25 and further comprising an element from the group consisting of B, C, N, P, S, As and H, the element from the group consisting of B, C, N, P, S, As and H comprising not more than 15% by mass of the alloy.

5. An alloy consisting of

a first compound, said first compound comprising Mn 1±α Ni 1±β Si 1±γ , wherein α≤0.25, β≤0.25, and γ≤0.25; and

a second compound, said second compound isostructurally substituting the first compound, and said second compound comprising Co 1±λ Fe 1±μ Ge 1±ν wherein λ≤0.25, μ≤0.25, and ν≤0.25.

6. An alloy consisting of

a first compound, said first compound comprising Mn 1±α Ni 1±β Si 1±γ , wherein α≤0.25, β≤0.25, and γ≤0.25; and

a second compound, said second compound isostructurally substituting the first compound, and said second compound comprising Co 1±α Fe 1±μ Ge 1±ν wherein λ≤0.25, μ≤0.25, and ν≤0.25 and further comprising an element from the group consisting of B, C, N, P, S, As and H, the element from the group consisting of B, C, N, P, S, As and H comprising not more than 15% by mass of the alloy.

Assignments (3)
CONFIRMATORY LICENSE Recorded Dec 13, 2021
From: LOUISIANA STATE UNIV A&M COL BATON ROUGE
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 058495/0387 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 17, 2015
From: SAMANTA, TAPAS, DR; STADLER, SHANE, DR
To: BOARD OF SUPERVISORS OF LOUISIANA STATE UNIVERSITY AND AGRICULTURAL AND MECHANICAL COLLEGE
Reel/Frame 036121/0362 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 17, 2015
From: ALI, NAUSHAD, DR
To: BOARD OF TRUSTEES OF SOUTHERN ILLINOIS UNIVERSITY
Reel/Frame 036121/0408 →
Continuity (2)
Provisional Application 62026091 · Jul 18, 2014
Related Publication 20160017462A1 · Jan 21, 2016