IP Library Granted Patent US 9,297,762
Granted Patent B2
US 9,297,762 · App. 14/827,545 · Granted Mar 29, 2016

Spatial positioning of spectrally labeled beads

Inventors: Stephen Empedocles (Mountain View, CA); Andrew Watson (Lexington, MA); Jian Jin (Berkeley, CA)
Assignee: Life Technologies Corporation
G01N21/6428B01L3/5025B01L3/5085B01L3/502715B01L3/502761G01N21/25G01N21/253G01N21/272G01N21/274G01N21/278G01N21/6452G01N21/6486G01N21/6489G01N33/54373B01J2219/005B01J2219/00317B01J2219/00432B01J2219/00574B01J2219/00576B01J2219/00578B01J2219/00585B01J2219/00596B01J2219/00648B01J2219/00657B01J2219/00659B01J2219/00677B01J2219/00707B01J2219/00722B01J2219/00743B01L3/545B01L2200/0668B01L2300/021B01L2300/0819B01L2300/0829B01L2400/0454B01L2400/0457B82Y30/00C40B40/06C40B60/14G01N21/6456G01N2015/0092G01N2015/1472G01N2015/1497G01N2021/6441G01N2021/6482G01N2035/00158G01N2035/00742G01N2035/00752G01N2201/04G01N2201/06113
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Quick Facts
Patent No.
US 9,297,762
App. No.
14/827,545
Granted
Mar 29, 2016
Kind
B2
Abstract

Devices, systems, kits, and methods for detecting and/or identifying a plurality of spectrally labeled bodies well-suited for performing multiplexed assays. By spectrally labeling the beads with materials which generate identifiable spectra, a plurality of beads may be identified within the fluid. Reading of the beads is facilitated by restraining the beads in arrays, and/or using a focused laser.

Claims (36)

1. A multiplex assay detection apparatus, comprising:

a plurality of spectrally labeled bodies bound to a surface of a solid support,

wherein the spectrally labeled bodies are spatially resolved and each comprise a plurality of different fluorescent labels used to encode discrete and different emission spectra wherein each emission spectrum has a plurality of signals at differing wavelengths;

an excitation energy source configured to excite the plurality of spectrally labeled bodies;

a sensor configured to detect the emission spectrum of each spectrally labeled body; and

a processor configured to utilize machine-readable code including a library of identifiable substances and their associated emission spectra to identify the identifiable substance associated with each spectrally labeled body.

2. The apparatus of claim 1 , wherein each of the plurality of spectrally labeled bodies includes a capture moiety that has an affinity for a particular identifiable substance.

3. The apparatus claim of 2 , wherein the identifiable substance is a biomolecule.

4. The apparatus claim of 3 , wherein the biomolecule is an oligonucleotide.

5. The apparatus of claim 1 , wherein the surface of the solid support is substantially planar.

6. The apparatus of claim 1 , wherein the solid support is a bead.

7. The apparatus of claim 6 , wherein the bead is comprised of spectrally labeled bodies with the same emission spectrum.

8. The apparatus of claim 6 , wherein the bead is comprised of spectrally labeled bodies with two or more emission spectra.

9. The apparatus of claim 1 , wherein the solid support is an assay plate.

10. The apparatus of claim 1 , wherein the processor is configured to provide a count of the detected spectrally labeled bodies.

11. An assay detection system, comprising:

an assay detection apparatus, comprising:

a plurality of spectrally labeled bodies bound to a surface of a solid support, wherein the spectrally labeled bodies are spatially resolved and each comprise a plurality of different fluorescent labels used to encode discrete and different emission spectra wherein each emission spectrum has a plurality of signals at differing wavelengths;

an excitation energy source configured to excite the plurality of spectrally labeled bodies; and

a sensor configured to detect the emission spectra of each spectrally labeled body;

a computing device in communication with the assay detection apparatus, comprising:

a memory for storing machine-readable code including a library of identifiable substances and their associated spectral barcodes, and

a processor in communication with the memory and configured to utilize the machine-readable code to identify the identifiable substances associated with the spectrally labeled bodies.

12. The system of claim 11 , wherein each of the plurality of spectrally labeled bodies includes a capture moiety that has an affinity for a particular identifiable substance.

13. The system claim of 12 , wherein the identifiable substance is a biomolecule.

14. The system claim of 13 , wherein the biomolecule is an oligonucleotide.

15. The system of claim 11 , wherein the surface of the solid support is substantially planar.

16. The apparatus of claim 11 , wherein the solid support is a bead.

17. The apparatus of claim 11 , wherein the solid support is an assay plate.

18. The apparatus of claim 11 , wherein the processor is configured to provide a count of the detected spectrally labeled bodies.

19. An assay detection method, comprising:

exciting a plurality of spectrally labeled bodies with an energy source, wherein the spectrally labeled bodies are bound to a surface of a solid support in a spatially resolved configuration and each comprise a plurality of different fluorescent labels used to encode discrete and different emission spectra wherein each emission spectrum has a plurality of signals at differing wavelengths;

detecting emission spectra with a sensor;

providing a memory for storing machine-readable code including a library of identifiable substances and their associated emission spectra; and

identifying identifiable substances from the emission spectra using a processor, wherein the processor is in communication with the memory and configured to utilize the machine-readable code to identify the identifiable substances associated with the spectrally labeled bodies.

20. The method of claim 19 , further comprising the step of counting the detected spectrally labeled bodies using the processor.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 23, 2016
From: QUANTUM DOT CORPORATION
To: INVITROGEN CORPORATION
Reel/Frame 037798/0123 →
MERGER Recorded Feb 23, 2016
From: INVITROGEN CORPORATION
To: LIFE TECHNOLOGIES CORPORATION
Reel/Frame 037798/0209 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 2, 2015
From: EMPEDOCLES, STEPHEN A.; WATSON, ANDREW R.; JIN, JIAN
To: QUANTUM DOT CORP.
Reel/Frame 036478/0142 →
MERGER Recorded Sep 2, 2015
From: QUANTUM DOT CORPORATION
To: LIFE TECHNOLOGIES CORPORATION
Reel/Frame 036479/0289 →
Continuity (7)
Division 14608350 · Jan 29, 2015
Continuation 13777032 · Feb 26, 2013
Continuation 12620475 · Nov 17, 2009
Continuation 11425851 · Jun 22, 2006
Continuation 09827256 · Apr 5, 2001
Provisional Application 60195520 · Apr 6, 2000
Related Publication 20150355079A1 · Dec 10, 2015