IP Library Granted Patent US 9,837,486
Granted Patent B2
US 9,837,486 · App. 14/854,125 · Granted Dec 5, 2017

Method for oxidizing a substrate surface using oxygen

Inventors: Pekka Laukkanen (Turku, FI); Jouko Lang (Lieto, FI); Marko Punkkinen (Turku, FI); Marjukka Tuominen (Turku, FI); Veikko Tuominen (Turku, FI); Johnny Dahl (Turku, FI); Juhani Vayrynen (Kaarina, FI)
Assignee: Comptek Solutions Oy
H01L29/02H01L21/02046H01L21/02109H01L21/02172H01L21/02241H01L21/28264H01L21/31666H01L21/3245H01L29/1054H01L29/20H01L29/201H01L29/205
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Quick Facts
Patent No.
US 9,837,486
App. No.
14/854,125
Granted
Dec 5, 2017
Kind
B2
Abstract

A method for treating a compound semiconductor substrate, in which method in vacuum conditions a surface of an In-containing III-As, III-Sb or III-P substrate is cleaned from amorphous native oxides and after that the cleaned substrate is heated to a temperature of about 250-550° C. and oxidized by introducing oxygen gas onto the surface of the substrate. The invention relates also to a compound semiconductor substrate, and the use of the substrate in a structure of a transistor such as MOSFET.

Claims (16)

1. A method for producing a crystalline oxide layer on an In-containing III-As, III-Sb or III-P compound semiconductor substrate, comprising in vacuum conditions

providing an In-containing III-As, III-Sb or III-P substrate having a substrate surface which is clean from amorphous native oxides, and

heating said substrate having a clean surface to a temperature of about 250-550° C., and oxidizing it at said temperature of about 250-550° C. by introducing oxygen gas onto the surface of the substrate,

wherein said method produces a compound semiconductor substrate comprising at least

an In-containing III-As, III-Sb or III-P base material having a first side and a second side, and

a crystalline (3×1)-O, c(4×2)-O, (1×2)-O, (2×3)-O, (3×1)-SnO, (3×3)-SnO, or (1×1)-SnO oxide layer being formed on at least a part of the first side of the base material.

2. The method according to claim 1 , wherein the In-containing III-As, III-Sb or III-P substrate is made of InAs, InSb, InP, InGaAs or InGaSb.

3. The method according to claim 1 , wherein the substrate is cleaned by argon-ion sputtering and post heating in ultra-high-vacuum (UHV) conditions at least to 400° C., or by pure heating in UHV at around 400-550° C.

4. The method according to claim 1 , wherein the cleaned substrate is covered by a tin (Sn) layer.

5. The method according to claim 1 , wherein the cleaned In-containing III-As substrate is heated to a temperature of about 340-400° C.

6. The method according to claim 1 , wherein the cleaned In-containing III-Sb substrate is heated to a temperature of about 340-450° C.

7. The method according to claim 1 , wherein the cleaned In-containing III-P substrate is heated to a temperature of about 450-500° C.

8. The method according to claim 1 , wherein the heating and the oxidation of the substrate are carried out simultaneously.

9. The method according to claim 1 , wherein the substrate is oxidized for 15 to 45 minutes.

10. The method according to claim 9 , wherein the substrate is oxidized for 15 to 30 minutes.

11. The method according to claim 1 , wherein the oxygen gas pressure is between 5×10 −7 and 5×10 −5 mbar.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 4, 2017
From: TURUN YLIOPISTO
To: COMPTEK SOLUTIONS OY
Reel/Frame 042248/0799 →
Priority Claims (1)
FI 20106181 · Nov 11, 2010 · national
Continuity (2)
Division 13881420
Related Publication 20160049295A1 · Feb 18, 2016