IP Library › Granted Patent US 9,989,473
Granted Patent B2
US 9,989,473 · App. 14/856,671 · Granted Jun 5, 2018

Portable liquid analyzer

Inventor: Michael Callahan (Englewood, CO)
G01N21/78G01N31/22G01N31/222
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Quick Facts
Patent No.
US 9,989,473
App. No.
14/856,671
Granted
Jun 5, 2018
Kind
B2
Abstract

A system is provided for identifying the presence of a target molecule or ion. The system comprises a solid support, and at least one chemical reagent applied to the solid support. Each chemical reagent produces a presumptive color indication that identifies or excludes the presence of a target molecule or ion.

Claims (18)

1. A method for producing a test kit to identify the presence of a target molecule or ion, comprising:

providing a solid support;

providing a first chemical reagent comprising a first micronized powder, the first chemical reagent producing a presumptive color indication that identifies or excludes the presence of a first target molecule or ion;

mixing a dispersant with the first micronized powder to reduce the viscosity of the first reagent powder to a first temporary flowable liquid; and

applying the first temporary flowable liquid to the solid support using a process selected from the group consisting of letterpress, rotary gravure, screen printing, tampography, wax printing, contact dosing, ultrasonic sputter, and drop on demand printing.

2. The method of claim 1 , further comprising:

a plurality of second temporary flowable liquids, each comprising a micronized chemical reagent mixed with a dispersant and each second chemical reagent producing a presumptive color indication that identifies or excludes the presence of one of a plurality of a second target molecules or ions different from the first target molecule or ion and from each other target molecule or ion; and

applying each second temporary flowable liquid to the solid support, each spaced apart from and different from the first chemical reagent and from each other second chemical reagent.

3. The method of claim 1 , further comprising manufacturing the solid support from a material selected from the group consisting of glass, metal, paper, textiles, organic, and inorganic membranes.

4. The method of claim 1 , further comprising providing a sample collector for collection of an unknown molecule or ion and introducing the unknown molecule or ion to the first chemical reagent.

5. The method of claim 4 , wherein providing the sample collector comprises providing a swab formed from an unreactive, adsorbent fiber.

6. The method of claim 1 , further comprising sealing the solid support and first chemical reagent in a moisture and UV resistant package.

7. The method of claim 1 , wherein the dispersant comprises a material selected from the group consisting of acrylic acid, polyvinyl alcohol, amino crosslinkers, polyvinyl pyrollidinone, glycol-ethers, styrene, polyester, vinyl chloride, polyethylene, natural gums, polyether and polyamide units.

8. The method of claim 1 , further comprising drying the solid support after applying the first temporary flowable liquid.

9. The method of claim 1 , wherein the first target molecule or ion is a dissolved hydrogen ion and the first chemical reagent comprises a material selected from a group consisting of cresol red, methyl violet, crystal violet, ethyl violet, malachite green, methyl green, 2-(p-dimethylaminophenylazo)pyridine, paramethyl red, metanil yellow, 4-phenylazodiphenylamine, thymol blue, metacresol purple, orange IV, 4-o-tolylazo-o-toluidine, quinaldine red, 4,4′-bis(4-amino-1-naphthylazo)-2,2′-stilbenedisulfonic acid, p-naphtholbenzein, phenolphthalein, o-cresolphthalein, ethyl bis(2,4-dimethylphenyl)ethanoate, Thymolphthalein, alizarin yellow R, alizarin, p-(2,4-dihydroxyphenylazo) benzenesulfonic acid, sodium salt, 5,5′-indigodisulfonic acid, disodium salt, and 2,4,6-trinitrotoluene, 1,3,5-trinitrobenzene, clayton yellow.

10. The method of claim 1 , wherein the first target molecule or ion is an organic solid and the first chemical reagent comprises a material selected from a group consisting of merocyanine dyes, 4-[2-N-substituted-1,4-hydropyridin-4-ylidine)ethylidene]cyclohexa-2,5-di-en-1-one, red pyrazolone dyes, azomethine dyes, indoaniline dyes, diazamerocyanine dyes, indigoid dyes 2,6-diphenyl-4-(2,4,6-triphenylpyridinium-1-yl)phenolate, 1-ethyl-4-(methoxycarbonyl)pyridinium iodide,5-(dimethylamino)-5′-nitro-2,2′-bisthiophene, reichart's dye, (2,4,6-triphenyl-l-pyridinio)-2,6-diphenylphenolate, and 9-diethylamino-5-benzo[α]phenoxazinone.

11. The method of claim 1 , wherein the first target molecule or ion is reactive nitrogen and the first chemical reagent comprises a material selected from a group consisting of 6-amino-1-naphthol-3-sulphonic acid, zinc, diphenylbenzidine, phenylanthranilic acid, aniline sulfate, diphenylamine, ethylenediamine, N-1 naphthyl dihydrochloride, potassium iodide, bismuth nitrate, sulfamic acid, sodium hydrogen sulphate, sulfanilamide, and hexachloroplatinic(IV) acid hydrate.

12. The method of claim 1 , wherein the first target molecule or ion is a reactive halogen or free radical and the first chemical reagent comprises a material selected from a group consisting of ammonium thiocyanate, 2,2′-bipyridine (Ru complex), nitrophenanthroline (Fe complex), manganous sulphate, phenylanthranilic acid, 1,10-Phenanthroline iron(II) sulfate complex, indigo carmine, copper sulphate, N-ethoxychrysoidine, analine, 2,2′-Bipyridine (Fe complex), methylene blue, 5,6-dimethylphenanthroline (Fe complex), o-dianisidine, ferrous sulphate, p-amino-N, N-diethylaniline sulfate, sodium diphenylamine sulfonate, diphenylbenzidine, diphenylamine, and viologen.

Assignments (5)
CORRECTIVE ASSIGNMENT TO CORRECT THE CONVEYING PARTY DATA TO S2 DETECTION {NEVADA} INC. PREVIOUSLY RECORDED AT REEL: 053019 FRAME: 0821. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Oct 5, 2020
From: S2 DETECTION (NEVADA) INC.
To: VERITEQUE USA, INC.
Reel/Frame 053981/0396 →
CORRECTIVE ASSIGNMENT TO CORRECT THE RECEIVING PARTY DATA TO S2 DETECTION{NEVADA} INC. PREVIOUSLY RECORDED AT REEL: 053966 FRAME: 0693. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Oct 5, 2020
From: THREAT DETECTION TECHNOLOGIES LLC DELAWARE - D/B/A S2 THREAT DETECTION; CALLAHAN, MICHAEL D.; LOANE, CHRISTIAN
To: S2 DETECTION (NEVADA) INC.
Reel/Frame 053981/0454 →
CORRECTIVE ASSIGNMENT TO CORRECT THE RECEIVING PARTY DATA TO S2 DETECTION {NEVADA}, INC PREVIOUSLY RECORDED AT REEL: 052594 FRAME: 0945. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Oct 1, 2020
From: THREAT DETECTION TECHNOLOGIES LLC DELAWARE - D/B/A S2 THREAT DETECTION; CALLAHAN, MICHAEL D.; LOANE, CHRISTIAN
To: S2 DETECTION (NEVADA) INC.
Reel/Frame 053966/0693 →
CHANGE OF NAME Recorded Jun 23, 2020
From: S2 DETECTION {NEVADA} INC.
To: VERITEQUE USA, INC.
Reel/Frame 053019/0821 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 6, 2020
From: CALLAHAN, MICHAEL D.; LOANE, CHRISTIAN; THREAT DETECTION TECHNOLOGIES LLC DELAWARE - D/B/A S2 THREAT DETECTION
To: S2 DETECTION {NEVADA}, INC.
Reel/Frame 052594/0945 →
Continuity (1)
Related Publication 20170082550A1 · Mar 23, 2017