IP Library Granted Patent US 9,878,306
Granted Patent B2
US 9,878,306 · App. 14/858,283 · Granted Jan 30, 2018

Silver nanowires, methods of making silver nanowires, core-shell nanostructures, methods of making core-shell nanostructures, core-frame nanostructures, methods of making core-frame nanostructures

Inventors: Dong Qin (Atlanta, GA); Younan Xia (Atlanta, GA); Yin Yang (Atlanta, GA); Jumei Li (Atlanta, GA); Xiaojun Sun (Atlanta, GA); Robson Rosa da Silva (Inhumas Goiás, BR); Miaoxin Yang (Atlanta, GA)
Assignee: Georgia Tech Research Corporation
B01J23/50B01J35/008B01J35/0013B01J35/023B01J35/026B01J35/06B01J37/0219B01J37/0225B01J37/16B22F1/0025B22F9/24B22F9/26B01J35/002B22F2001/0037C23F1/02C23F1/30
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Quick Facts
Patent No.
US 9,878,306
App. No.
14/858,283
Granted
Jan 30, 2018
Kind
B2
Abstract

In accordance with the purpose(s) of the present disclosure, as embodied and broadly described herein, embodiments of the present disclosure provide for silver nanowires, methods of making silver nanowires, core-shell nanostructures, methods of making core-shell nanostructures, core-frame nanostructures, methods of making core-frame nanostructures, and the like.

Claims (11)

1. A structure comprising:

a core-frame nanostructure including a frame around a hollow area within the frame, wherein the frame is a M-Ag alloy, wherein M is selected from the group consisting of Au, Pd, Pt, and Cu.

2. The structure of claim 1 , wherein the core frame nanostructure is selected from the group consisting of: a nanorod, a nanowire, a nano-sized polyhedron, and a nano-sized prism or thin plate.

3. The structure of claim 1 , wherein the nanocube has a length, a width, and a height of about 15 to 250 nm.

4. A method of making a core-frame nanostructure, comprising:

providing a silver nanostructure solution containing silver nanostructures, a reducing agent and poly(vinyl pyrrolidone);

mixing a first metal precursor solution and a second metal precursor solution with the silver nanostructure solution to produce a core-shell nanostructure; and

mixing an etchant with the core-shell nanostructure to remove the silver nanostructure to form the core-frame nanostructure, wherein the core-frame nanostructure includes a frame around a hollow area within the frame, wherein the frame is a M-Ag alloy, wherein M is selected from the group consisting of Au, Pd, Pt, and Cu.

5. The method of claim 4 , wherein the reducing agent is selected from the group consisting of: ascorbic acid, citric acid, formic acid, sodium borohydride, hydrogen gas, aldehydes, alcohols, polyols, carbohydrates, and hydrazine.

6. The method of claim 4 , wherein the etchant is selected from the group consisting of: H 2 O 2 , O 2 , FeCl 3 , Fe(NO 3 ) 3 , K 3 Fe(CN) 6 , and ammonia.

7. The method of claim 4 , wherein the core-frame nanostructure is selected from the group consisting of: a nanorod, a nanowire, a nano-sized polyhedron, and a nano-sized prism or thin plate.

Assignments (2)
CONFIRMATORY LICENSE Recorded Mar 16, 2018
From: GEORGIA INSTITUTE OF TECHNOLOGY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 045569/0208 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 25, 2016
From: QIN, DONG; XIA, YOUNAN; YANG, YIN; LI, JUMEI; SUN, XIAOJUN; DA SILVA, ROBSON ROSA; YANG, MIAOXIN
To: GEORGIA TECH RESEARCH CORPORATION
Reel/Frame 037572/0373 →
Continuity (2)
Provisional Application 62052677 · Sep 19, 2014
Related Publication 20160082418A1 · Mar 24, 2016